2024-22966. Addition of Certain Per- and Polyfluoroalkyl Substances (PFAS) to the Toxics Release Inventory (TRI)
Table 1 to Paragraph ( a )(1)
Chemical name CAS No. Reporting threshold (in pounds) * * * * * * * Per- and polyfluoroalkyl substances (Individually listed chemicals added by 15 U.S.C. 8921(b)(1) and (c)(1) and pursuant to 42 U.S.C. 11023(d)(2)). (EPA periodically updates the lists of covered chemicals at § 372.65(d) and (e) to reflect chemicals that have been added by 15 U.S.C. 8921) see § 372.65(d) and (e). 100 * * * * * * * (2) * * *
Table 2 to Paragraph ( a )(2)
Category name Reporting threshold (in pounds) * * * * * * * Per- and polyfluoroalkyl substances (Chemical categories added by 15 U.S.C. 8921 (b)(1) and (c)(1) and pursuant to 42 U.S.C. 11023(d)(2)). (EPA periodically updates the lists of covered chemicals at § 372.65(f) to reflect chemical categories that have been added by 15 U.S.C. 8921) 100 * * * * * * * 3. Amend § 372.65 by:
a. Revising the introductory text;
b. In table 4 to paragraph (d):
i. Removing the entries for “Ammonium perfluorobutanoate”; “Ammonium perfluorooctanoate”; “Chromium(III) perfluorooctanoate”; “Ethanaminium, N,N,N-triethyl-, salt with 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-1-octanesulfonic acid (1:1)”; “Hexafluoropropylene oxide dimer acid”; “Hexafluoropropylene oxide dimer acid ammonium salt”; “1-Hexanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,6-tridecafluoro-, ammonium salt”; “1-Hexanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,6-tridecafluoro-, potassium salt”; “1-Hexanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,6-tridecafluoro-, compd. with 2,2'-iminobis[ethanol] (1:1)”; “Lithium (perfluorooctane)sulfonate”; “1-Octanesulfonic acid, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-, ammonium salt”; “Octanoyl fluoride, pentadecafluoro-”; “Perfluorobutane sulfonic acid”; “Perfluorobutanesulfonate”; “Perfluorobutanoate”; “Perfluorobutanoic acid”; “Perfluorodecanoic acid”; “Perfluorododecanoic acid”; “Perfluorohexanesulfonic acid”; “Perfluorononanoic acid”; “Perfluorooctane sulfonic acid”; and “Perfluorooctanoic acid”; “Perfluorooctylsulfonyl fluoride”; “Potassium heptafluorobutanoate”; “Potassium perfluorobutane sulfonate”; “Potassium perfluorooctanesulfonate”; “Potassium perfluorooctanoate”; “Silver(I) perfluorooctanoate”; “Sodium perfluorobutanoate”; and “Sodium perfluorooctanoate”;
ii. Adding, in alphabetical order, entries for “Broflanilide”; “1-Butanesulfonamide, 1,1,2,2,3,3,4,4,4-nonafluoro-N-(2-hydroxyethyl)-N-methyl-”; “1-Butanesulfonamide, 1,1,2,2,3,3,4,4,4-nonafluoro-N-methyl-”; “Cyclopentene, 1,3,3,4,4,5,5-heptafluoro-”; “Ethanesulfonamide, 1,1,2,2,2-pentafluoro-N-[(pentafluoroethyl)sulfonyl]-, lithium salt”; “6:2 Fluorotelomer alcohol”; “Fulvestrant”; “Hexaflumuron”; “Pentane, 1,1,1,2,2,3,4,5,5,5-decafluoro-3-methoxy-4-(trifluoromethyl)-”; “Perfluorotridecanoic acid”; “Perfluoro(2-ethoxy-2-fluoroethoxy)acetic acid ammonium salt”; “2-Propenoic acid, 2-[methyl[(nonafluorobutyl)sulfonyl]amino]ethyl ester”; “Pyrifluquinazon”; “Tetraconazole”; “Triethoxy(3,3,4,4,5,5,6,6,7,7,8,8,8-tri-deca-fluorooctyl)silane”; and “Trifluoro(trifluoromethyl) oxirane”;
c. In table 5 to paragraph (e):
i. Removing the entries for “307-35-7”; “307-55-1”; “335-66-0”; “335-67-1”; “335-76-2”; “335-93-3”; “335-95-5”; “355-46-4”; “375-22-4”; “375-73-5”; “375-95-1”; “1763-23-1”; “2218-54-4”; “2395-00-8”; “2795-39-3”; “2966-54-3”; “3825-26-1”; “3871-99-6”; “10495-86-0”; “13252-13-6”; “29081-56-9”; “29420-49-3”; “29457-72-5”; “45048-62-2”; “45187-15-3”; “56773-42-3”; “62037-80-3”; “68141-02-6”; “68259-08-5”; and “70225-16-0”;
ii. Adding, in numerical order, the entries for “428-59-1”; “647-42-7”; “1892-03-1”; “34454-97-2”; “51851-37-7”; “67584-55-8”; “68298-12-4”; “72629-94-8”; “86479-06-3”; “112281-77-3”; “129453-61-8”; “132182-92-4”; “132843-44-8”; “337458-27-2”;“908020-52-0”; and “1207727-04-5”; and
d. Adding paragraph (f).
The revisions and additions read as follows:
Chemicals and chemical categories to which this part applies.The requirements of this part apply to the chemicals and chemical categories listed in this section. This section contains six listings. Paragraph (a) of this section is an alphabetical order listing of those chemicals that have an associated Chemical Abstracts Service (CAS) Registry number. Paragraph (b) of this section contains a CAS number order list of the same chemicals listed in paragraph (a) of this section. Paragraph (c) of this section contains the chemical categories for which reporting is required. These chemical categories are listed in alphabetical order and do not have CAS numbers. Paragraph (d) of this section is an alphabetical order listing of the per- and polyfluoroalkyl substances and their associated CAS Registry number. Paragraph (e) of this ( print page 81811) section contains a CAS number order list of the same chemicals listed in paragraph (d) of this section. Each listing identifies the effective date for reporting under § 372.30. Paragraph (f) of this section is an alphabetical order listing of the per- and polyfluoroalkyl substances chemical categories for which reporting is required. Per- and polyfluoroalkyl substances automatically added to the list of chemicals for which reporting is required pursuant to the Fiscal Year 2020 National Defense Authorization Act, section 7321(c), shall be incorporated as chemical categories to include the acid and associated salts, acyl/sulfonyl halides, and anhydride of that acid if added pursuant to a published final toxicity value that provides toxicity values for an acid and associated salts and/or acyl/sulfonyl halides and/or anhydride.
* * * * *(d) * * *
Table 4 to Paragraph ( d )
Chemical name CAS No. Effective date * * * * * * * Broflanilide 1207727-04-5 1/1/2025 * * * * * * * 1-Butanesulfonamide, 1,1,2,2,3,3,4,4,4-nonafluoro-N-(2-hydroxyethyl)-N-methyl- 34454-97-2 1/1/2025 * * * * * * * 1-Butanesulfonamide, 1,1,2,2,3,3,4,4,4-nonafluoro-N-methyl- 68298-12-4 1/1/2025 * * * * * * * Cyclopentene, 1,3,3,4,4,5,5-heptafluoro- 1892-03-1 1/1/2025 * * * * * * * Ethanesulfonamide, 1,1,2,2,2-pentafluoro-N-[(pentafluoroethyl)sulfonyl]-, lithium salt 132843-44-8 1/1/2025 * * * * * * * 6:2 Fluorotelomer alcohol 647-42-7 1/1/2025 * * * * * * * Fulvestrant 129453-61-8 1/1/2025 * * * * * * * Hexaflumuron 86479-06-3 1/1/2025 * * * * * * * Pentane, 1,1,1,2,2,3,4,5,5,5-decafluoro-3-methoxy-4-(trifluoromethyl)- 132182-92-4 1/1/2025 * * * * * * * Perfluorotridecanoic acid 72629-94-8 1/1/2025 * * * * * * * Perfluoro(2-ethoxy-2-fluoroethoxy)acetic acid ammonium salt 908020-52-0 1/1/2025 * * * * * * * 2-Propenoic acid, 2-[methyl[(nonafluorobutyl)sulfonyl]amino]ethyl ester 67584-55-8 1/1/2025 * * * * * * * Pyrifluquinazon 337458-27-2 1/1/2025 * * * * * * * Tetraconazole 112281-77-3 1/1/2025 * * * * * * * Triethoxy(3,3,4,4,5,5,6,6,7,7,8,8,8-tri-deca-fluorooctyl)silane 51851-37-7 1/1/2025 * * * * * * * Trifluoro(trifluoromethyl) oxirane 428-59-1 1/1/2025 * * * * * * * (e) * * *
( print page 81812)Table 5 to Paragraph ( e )
CAS No. Chemical name Effective date * * * * * * * 428-59-1 Trifluoro(trifluoromethyl) oxirane 1/1/2025 * * * * * * * 647-42-7 6:2 Fluorotelomer alcohol 1/1/2025 * * * * * * * 1892-03-1 Cyclopentene, 1,3,3,4,4,5,5-heptafluoro- 1/1/2025 * * * * * * * 34454-97-2 1-Butanesulfonamide, 1,1,2,2,3,3,4,4,4-nonafluoro-N-(2-hydroxyethyl)-N-methyl- 1/1/2025 * * * * * * * 51851-37-7 Triethoxy(3,3,4,4,5,5,6,6,7,7,8,8,8-trideca-fluorooctyl)silane 1/1/2025 * * * * * * * 67584-55-8 2-Propenoic acid, 2-[methyl[(nonafluorobutyl)sulfonyl]amino]ethyl ester 1/1/2025 * * * * * * * 68298-12-4 1-Butanesulfonamide, 1,1,2,2,3,3,4,4,4-nonafluoro-N-methyl- 1/1/2025 * * * * * * * 72629-94-8 Perfluorotridecanoic acid 1/1/2025 * * * * * * * 86479-06-3 Hexaflumuron 1/1/2025 * * * * * * * 112281-77-3 Tetraconazole 1/1/2025 * * * * * * * 129453-61-8 Fulvestrant 1/1/2025 * * * * * * * 132182-92-4 Pentane, 1,1,1,2,2,3,4,5,5,5-decafluoro-3-methoxy-4-(trifluoromethyl)- 1/1/2025 * * * * * * * 132843-44-8 Ethanesulfonamide, 1,1,2,2,2-pentafluoro-N-[(pentafluoroethyl)sulfonyl]-, lithium salt 1/1/2025 * * * * * * * 337458-27-2 Pyrifluquinazon 1/1/2025 * * * * * * * 908020-52-0 Perfluoro(2-ethoxy-2-fluoroethoxy)acetic acid ammonium salt 1/1/2025 * * * * * * * 1207727-04-5 Broflanilide 1/1/2025 * * * * * * * (f) Per- and polyfluoroalkyl chemical category listing.
Table 6 to Paragraph ( f )
Category name Effective date 9-chlorohexadecafluoro-3-oxanone-1-sulfonic acid (9Cl-PF3ONS) (CASRN 756426-58-1), salts, sulfonyl halides, and anhydride (includes all associated salts and sulfonyl halides, including the following): 1/1/2025 73606-19-6: potassium 9-chlorohexadecafluoro-3-oxanonane-1 sulfonate 11-chloroeicosafluoro-3-oxaundecane-1-sulfonic acid (11Cl-PF3OUdS) (CASRN 763051-92-9), salts, sulfonyl halides, and anhydride (includes all associated salts and sulfonyl halides, including the following): 1/1/2025 83329-89-9: potassium 11-chloroeicosafluoro-3-oxaundecane-1-sulfonate Hexafluoropropylene oxide dimer acid (HFPO-DA, GenX) (CASRN 13252-13-6), salts, and acyl halides (includes all associated salts and acyl halides, including the following): 1/1/2025 2062-98-8: propanoyl fluoride, 2,3,3,3-tetrafluoro-2 (heptafluoropropoxy)-] 62037-80-3: ammonium perfluoro-2-methyl-3-oxahexanoate 67118-55-2: potassium 2,3,3,3-tetrafluoro-2- (heptafluoropropoxy)propanoate ( print page 81813) 67963-75-1: sodium 2,3,3,3-tetrafluoro-2(heptafluoropropoxy)propanoate Perfluorobutanesulfonic acid (PFBS), salts, sulfonyl halides, and anhydride (CASRN 375-73-5) (includes all associated salts and sulfonyl halides, including the following): 1/1/2025 375-72-4: perfluorobutanesulfonyl fluoride 29420-49-3: potassium perfluorobutane sulfonate 36913-91-4: perfluorobutanesulfonic anhydride 60453-92-1: sodium nonafluorobutane-1-sulfonate 68259-10-9: ammonium perfluorobutanesulfonate 70225-18-2: bis(2-hydroxyethyl)ammonium perfluorobutanesulfonate 131651-65-5: lithium nonafluorobutane-1-sulfonate 220689-12-3: tetrabutylphosphonium perfluorobutanesulfonate 507453-86-3: magnesium nonafluorobutanesulfonate Perfluorobutanoic acid (PFBA) (CASRN 375-22-4), salts, acyl halides, and anhydride (includes all associated salts and acyl halides, including the following): 1/1/2025 335-42-2: perfluorobutanoyl fluoride 336-59-4: perfluorobutanoic anhydride 375-16-6: heptafluorobutyryl chloride 2218-54-4: sodium perfluorobutanoate 2966-54-3: potassium perfluorobutanoate 3794-64-7: silver heptafluorobutyrate 10495-86-0: ammonium perfluorobutanoate 73755-28-9: rhodium(II) perfluorobutyrate dimer Perfluorodecanoic acid (PFDA) (CASRN 335-76-2), salts, acyl halides, and anhydride (includes all associated salts and acyl halides, including the following): 1/1/2025 307-38-0: perfluorodecanoyl chloride 3108-42-7: ammonium Perfluorodecanoate 3830-45-3: sodium Perfluorodecanoate 942199-24-8: perfluorodecanoic anhydride Perfluorododecanoic acid (PFDoA) (CASRN 307-55-1), salts, acyl halides, and anhydride (includes all associated salts and acyl halides, including the following): 1/1/2025 3793-74-6: ammonium tricosafluorododecanoate 1456735-80-0: perfluorododecanoic anhydride Perfluorohexanesulfonic acid (PFHxS) (CASRN 355-46-4), salts, sulfonyl halides, and anhydride (includes all associated salts and sulfonyl halides, including the following): 1/1/2025 423-50-7: perfluorohexanesulfonyl fluoride 3871-99-6: potassium perfluorohexanesulfonate 55120-77-9: lithium perfluorohexanesulfonate 68259-08-5: ammonium perfluorohexanesulfonate 70225-16-0: bis(2-hydroxyethyl)ammonium perfluorohexanesulfonate 82382-12-5: sodium perfluorohexanesulfonate 109065-55-6: perfluorohexanesulfonic anhydride Perfluorohexanoic acid (PFHxA) (CASRN 307-24-4), salts, acyl halides, and anhydride (includes all associated salts and acyl halides, including the following): 1/1/2025 308-13-4: perfluorohexanoic anhydride 336-02-7: silver perfluorohexanoate 355-38-4: perfluorohexanoyl fluoride 335-53-5: perfluorohexanoyl chloride 2923-26-4: sodium perfluorohexanoate 3109-94-2: potassium undecafluorohexanoate 21615-47-4: ammonium perfluorohexanoate Perfluorononanoic acid (PFNA) (CASRN 375-95-1), salts, acyl halides, and anhydride (includes all associated salts and acyl halides, including the following): 1/1/2025 558-95-2: heptadecafluorononanoyl fluoride 4149-60-4: ammonium perfluorononanoate 21049-38-7: potassium perfluorononanoate 21049-39-8: sodium heptadecafluorononanoate 52447-23-1: heptadecafluorononanoyl chloride 228407-54-3: perfluorononanoic anhydride 1H,1H, 2H, 2H-Perfluorooctane sulfonic acid (6:2 FTS) (CASRN 27619-97-2), salts, sulfonyl halides, and anhydride (includes all associated salts and sulfonyl halides, including the following): 1/1/2025 2043-57-4: 1H,1H,2H,2H-Perfluorooctyl iodide 27619-89-2: 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctanesulphonyl chloride 27619-94-9: sodium 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctane-1-sulfonate 59587-38-1: potassium 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctanesulfonate 59587-39-2: 6:2 fluorotelomer sulfonate ammonium 1807944-82-6: 1-octanesulfonic acid, 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-, barium salt (2:1) Perfluorooctanoic acid (PFOA) (CASRN 335-67-1), salts, acyl halides, and anhydride (includes all associated salts and acyl halides, including the following): 1/1/2025 335-64-8: pentadecafluorooctanoyl chloride 335-66-0: pentadecafluorooctanoyl fluoride 335-93-3: silver perfluorooctanoate 335-95-5: sodium perfluorooctanoate ( print page 81814) 2395-00-8: potassium perfluorooctanoate 3825-26-1: ammonium perfluorooctanoate 17125-58-5: lithium perfluorooctanoate 17125-60-9: cesium perfluorooctanoate 33496-48-9: perfluorooctanoic anhydride 68141-02-6: chromium perfluorooctanoate 98065-31-7: potassium pentadecafluorooctanoate—water (1:1:2) Perfluorooctanesulfonic acid (PFOS) (CASRN 1763-23-1), salts, sulfonyl halides, and anhydride (includes all associated salts and sulfonyl halides, including the following): 1/1/2025 307-35-7: perfluorooctylsulfonyl fluoride 423-92-7: perfluorooctanesulfonic anhydride 2795-39-3: potassium perfluorooctanesulfonate 4021-47-0: sodium perfluorooctanesulfonate 29081-56-9: ammonium perfluorooctanesulfonate 29457-72-5: lithium perfluorooctanesulfonate 56773-42-3: tetraethylammonium perfluorooctanesulfonate 70225-14-8: 1-octanesulfonic acid,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-heptadecafluoro-, compd with 2,2'-iminobis[ethanol] (1:1) 91036-71-4: magnesium bis(heptadecafluorooctanesulfonate) 111873-33-7: tetrabutylammonium perfluorooctanesulfonate Perfluoropropanoic acid (PFPrA) (CASRN 422-64-0), salts, acyl halides, and anhydride (includes all associated salts and acyl halides, including the following): 1/1/2025 356-42-3: pentafluoropropanoic anhydride 378-76-7: potassium perfluoropropanoate 378-77-8: sodium perfluoropropanoate 422-59-3: perfluoropropanoyl chloride 422-61-7: perfluoropropanoyl fluoride Perfluoroundecanoic acid (PFUnA) (CASRN 2058-94-8), salts, acyl halides, and anhydride (includes all associated salts and acyl halides, including the following): 1/1/2025 4234-23-5: ammonium perfluoroundecanoate 30377-53-8: potassium perfluoroundecanoate 60871-96-7: sodium perfluoroundecanoate 97163-17-2: calcium perfluoroundecanoate 942199-03-3: perfluoroundecanoic anhydride
Document Information
- Published:
- 10/08/2024
- Department:
- Environmental Protection Agency
- Entry Type:
- Proposed Rule
- Action:
- Proposed rule.
- Document Number:
- 2024-22966
- Dates:
- Comments must be received on or before December 9, 2024. Comments on the information collection provisions submitted to the Office of Management and Budget (OMB) under the Paperwork Reduction Act (PRA) are best assured of consideration by OMB if OMB receives a copy of your comments on or before November 7, 2024.
- Pages:
- 81776-81814 (39 pages)
- Docket Numbers:
- EPA-HQ-OPPT-2023-0538, FRL-9313-01-OCSPP
- RINs:
- 2070-AL03: Addition of Certain Per- and Polyfluoroalkyl Substances (PFAS) to the Toxics Release Inventory (TRI)
- RIN Links:
- https://www.federalregister.gov/regulations/2070-AL03/addition-of-certain-per-and-polyfluoroalkyl-substances-pfas-to-the-toxics-release-inventory-tri-
- Topics:
- Environmental protection, Reporting and recordkeeping requirements
- PDF File:
- 2024-22966.pdf
- Supporting Documents:
- » PFAS Explained US EPA website
- » Health Effects Support Document for Perfluorooctane Sulfonate (PFOS)
- » The ECOTOXicology Knowledgebase: A Curated Database of Ecologically Relevant Toxicity Tests to Support Environmental Research and Risk Assessment
- » Human Health Hazard TRI Listing Support Document for Perfluoroundecanoic Acid (PFUnA; CASRN 2058-94-8)
- » Chronic exposure to 6:2 chlorinated polyfluorinated ether sulfonate acid (F-53B) induced hepatotoxic effects in adult zebrafish and disrupted the PPAR signaling pathway in their offspring
- » Yi et al. Probing the Hepatotoxicity Mechanisms of Novel Chlorinated Polyfluoroalkyl Sulfonates to Zebrafish Larvae: Implication of Structural Specificity
- » Prediction of Aqueous Solubility, Vapor Pressure and Critical Micelle Concentration for Aquatic Partitioning of Perfluorinated Chemicals
- » Japanese patent
- » Background document to the Opinion on the Annex XV dossier proposing restrictions on Perfluorooctanoic acid (PFOA), PFOA salts and PFOA-related substances
- » A Review of bioconcentration and bioaccumulation assessments for organic chemicals in aquatic organisms