94-31815. Regulation of Fuels and Fuel Additives: Standards for Deposit Control Gasoline Additives  

  • [Federal Register Volume 59, Number 248 (Wednesday, December 28, 1994)]
    [Unknown Section]
    [Page ]
    From the Federal Register Online via the Government Publishing Office [www.gpo.gov]
    [FR Doc No: 94-31815]
    
    
    [Federal Register: December 28, 1994]
    
    
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    40 CFR Part 60
    40 CFR Part 80
    
    [AMS-FRL-5128-9]
    
    
    Regulation of Fuels and Fuel Additives: Standards for Deposit 
    Control Gasoline Additives
    
    AGENCY: Environmental Protection Agency (EPA).
    
    ACTION: Proposed rule; reopening of comment period.
    
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    SUMMARY: On December 6, 1993, EPA published a Notice of Proposed 
    Rulemaking (NPRM) to require the use of deposit control (detergent) 
    additives in all gasoline used in the United States. The NPRM contained 
    a proposed interim program which would take effect beginning January 1, 
    1995, as well as a proposed performance-based detergent additive 
    certification program to be implemented at a later date. The interim 
    program was finalized on October 14, 1994. The detergent certification 
    program is expected to be finalized by June 30, 1995, and to take 
    effect a year later.
        As proposed, the detergent certification program was concerned 
    specifically with the control of port fuel injector deposits (PFID) and 
    intake valve deposits (IVD). While also acknowledging the potential 
    importance of combustion chamber deposits (CCD), EPA did not propose 
    any requirements for CCD control because of uncertainty regarding the 
    scope of the problem and the current lack of suitable performance test 
    procedures and standards. Subsequently, some commenters expressed 
    concern that a federal requirement for PFID and IVD control might 
    encourage detergent overuse, which could potentially exacerbate CCD 
    concerns. These commenters suggested that, as a temporary measure, 
    until CCD performance tests become available, EPA should cap detergent 
    use by implementing standards to limit the level of unwashed gums in 
    additized gasoline. However, other commenters disagreed with this 
    suggestion. This document discusses the CCD issue and requests comments 
    on alternative approaches for addressing it. Additional comment is also 
    sought in regard to selected issues related to the proposed detergent 
    certification program and the enforcement provisions of the detergents 
    program.
    
    DATES: Written comments on the specific issues discussed in this 
    document will be accepted until January 27, 1995. EPA is not soliciting 
    new comments on aspects of the original proposed rule that are not 
    specifically addressed in this document.
    
    ADDRESSES: Comments on this notice should be submitted in duplicate to: 
    EPA Air Docket Section (LE-131); Attention: Public Docket No. A-91-77; 
    Room M-1500, 401 M Street S.W., Washington, DC 20460. (Phone 202-260-
    7548; FAX 202-260-4000). This docket also contains all other materials 
    relevant to this rulemaking. The docket is open for public inspection 
    from 8:00 a.m. until 4:00 p.m., except on government holidays. As 
    provided in 40 CFR part 2, a reasonable fee may be charged for copying 
    docket materials.
        Electronic copies of this and other documents related to this 
    rulemaking are available through the Office of Air Quality Planning and 
    Standards (OAQPS) Technology Transfer Network Bulletin Board System 
    (TTNBBS). Details on how to access this bulletin board are included in 
    Section VII of this notice.
    
    FOR FURTHER INFORMATION CONTACT: For general information and 
    information related to technical issues contact: Mr. Jeffrey A. Herzog, 
    U.S. EPA (RDSD-12), Regulation Development and Support Division, 2565 
    Plymouth Road, Ann Arbor, MI 48105; Telephone: (313) 668-4227, Fax: 
    (313) 741-7816. For information on enforcement related issues contact: 
    Judith Lubow, U.S. EPA, Office of Enforcement and Compliance Assurance, 
    Western Field Office, 12345 West Alameda Parkway, Suite 300, Lakewood, 
    CO 80228; Telephone: (303) 969-6483, FAX: (303) 969-6490.
    
    SUPPLEMENTAL INFORMATION:
    
    I. Introduction
    
        Section 211(l) of the Clean Air Act (CAA) specifies that, beginning 
    January 1, 1995, all gasoline shall contain additives to prevent the 
    accumulation of deposits in engines or fuel supply systems. Such 
    deposits can have adverse effects on the emissions of a vehicle as well 
    as its fuel economy and driveability. As part of the CAA mandate, EPA 
    was tasked with the promulgation of rules establishing specifications 
    for such additives.
        In response to these statutory requirements, on December 6, 1993, 
    (59 FR 64213) EPA published a Notice of Proposed Rulemaking (NPRM) 
    requiring that gasolines contain detergents to control port fuel 
    injector deposits (PFID) and intake valve deposits (IVD). The rule was 
    proposed to be implemented in two phases. The first phase was an 
    interim program focused on registration and record-keeping requirements 
    which would apply for the first year. The second phase, to apply 
    thereafter, was a certification program requiring detergents to be 
    evaluated in a matrix of test fuels using national consensus test 
    procedures and prescribed standards for IVD and PFID control.
        The detergents rule is being finalized in two parts. The interim 
    program was promulgated October 14, 1994, and appeared in the Federal 
    Register on November 1, 1994 (59 FR 54678). Promulgation of the full 
    detergent certification program is expected to occur by June 30, 1995. 
    This second phase of the rule was delayed for two reasons. First, the 
    national consensus procedure EPA proposed for use in testing PFID 
    control was not finalized by the American Society for Testing and 
    Materials (ASTM) in time to be incorporated into the rule. Since an 
    interim program had already been proposed for 1995, EPA saw little 
    value in abandoning reliance on the ASTM procedure solely for the sake 
    of promulgating the entire rule at once. Second, issues were raised in 
    the comments regarding the possible impact of IVD and PFID control 
    requirements on combustion chamber deposits (CCD).
        While the NPRM also contained a substantial discussion on CCD, it 
    did not propose specific CCD control measures due to a lack of national 
    consensus test procedures and performance standards as well as 
    uncertainty as to the scope of the CCD problem. Given the need for a 
    slight delay in the final rulemaking schedule to allow completion of 
    the test procedure development, EPA believed it was important to 
    further evaluate the CCD issue prior to finalization of the 
    certification program.
        As part of that evaluation effort, this notice seeks public comment 
    on concerns raised by auto industry commenters that the gum levels in 
    gasoline will increase as a result of the use of IVD and PFID detergent 
    additives and that these gums will increase CCD. This could have an 
    adverse effect on emissions and vehicle driveability. Additional 
    comment is also sought on several points raised in the comments 
    regarding the proposed implementation and enforcement schemes under the 
    detergent certification program. Each of these areas is discussed 
    below.
    
    II. Combustion Chamber Deposit Control
    
    A. Background
    
        CCDs are composed of fuel and other material which enter the 
    combustion chamber, are not fully burned, and are deposited in various 
    portions of the engine's combustion chamber rather than leaving the 
    chamber with other exhaust products. The formation of CCD is governed 
    by the combustion process, combustion temperatures, and the design of 
    the combustion chamber itself. Other factors influencing CCD formation 
    include fuel and oil composition, engine design/technology and 
    operating conditions (e.g., speed, load, coolant temperature), engine 
    oil consumption, and fuel/oil additive usage. The technical literature 
    indicates that CCD potentially have three effects on engine operations: 
    an adverse effect on emission rates, an increase in engine octane 
    requirements, and an impact on fuel economy. Additional background 
    information on CCD is provided in the NPRM as well as a memorandum to 
    the docket entitled, ``Summary Discussion of Combustion Chamber 
    Deposits'' (Docket Item IV-B-04).
        Based on the incomplete information available in the literature and 
    the lack of available consensus test procedures or standards, EPA did 
    not propose a requirement for CCD control related to emissions or 
    octane requirement increase (ORI) effects. EPA received comments both 
    supporting and opposing this position.
        Vehicle manufacturers expressed concern that the proposed rule, 
    which contained IVD/PFID performance standards but no requirements to 
    control CCD, may have an adverse impact on vehicle performance. They 
    stated that the use of excessive quantities of some types of detergent 
    additives, which provide an acceptable level of IVD/PFID control, tend 
    to incrementally contribute to CCD. They further held that EPA's rule, 
    by requiring a consistent level of IVD/PFID control additives in all 
    gasoline, may exacerbate this incremental additive contribution to CCD, 
    since there would be at least a slight incentive to over- additize fuel 
    to assure compliance. An adverse impact on vehicle NOx and HC emissions 
    performance and durability would result.
        Vehicle manufacturers also stated that CCD can cause ORI, and that 
    higher engine octane demand might limit future attempts to achieve fuel 
    economy improvements through the design of engines with higher 
    compression ratios. Concerns regarding the potential impact of CCD on 
    vehicle driveability and durability centered around reports that 
    detergent additive overuse could result in valve sticking and 
    combustion chamber deposit interference (CCDI). These commenters stated 
    that CCDI results from the accumulation of CCD on the top of the piston 
    and combustion chamber, which causes mechanical interference during 
    engine operation.
        Vehicle manufacturers urged EPA to investigate the potential 
    adverse impact of some IVD/PFID additives on CCD as soon as possible, 
    with the ultimate goal of a standardized CCD control test. As an 
    interim measure, until such a performance test is available, several 
    commenters urged EPA to, in effect, adopt a cap on additive 
    concentration, by setting a maximum unwashed gum level in additized 
    gasoline as measured by ASTM test D381. Two vehicle manufacturers 
    recommended an unwashed gum standard of 20 mg/100 ml, based on the 
    allowable limit for Japanese gasoline. They stated that CCD problems 
    are not present in vehicles in Japan and this may be due in large part 
    to the unwashed gum standard of 20 mg/100 ml. The American Automobile 
    Manufacturers Association (AAMA) recommended an unwashed gum limit of 
    70 mg/100 ml, and stated that this value would act as a cap and not 
    create a large burden since it exceeds the levels found in most 
    gasolines today. These commenters supported their position by stating 
    that a relationship exists between the increased use of IVD detergent 
    additives, an increase in unwashed gum levels in gasoline, and an 
    increased incidence of CCD-related customer complaints.
        One vehicle manufacturer recommended that, as a condition for 
    detergent certification, data should be required demonstrating that the 
    additive does not increase CCD relative to base gasoline. This 
    commenter further stated that it would be appropriate in the interim to 
    allow each additive manufacturer to use its own CCD control test 
    methods. The commenter stated that, because these test procedures would 
    be expected to vary from manufacturer to manufacturer, this approach 
    was recommended only as an interim solution until a standardized CCD 
    performance test and standard is developed.
        In contrast to the vehicle manufacturers, the petroleum and 
    additive industries contended that regulatory control of CCD was not 
    appropriate at this time because of a lack of data on the effects of 
    CCD and the lack of an adequate performance test and standard. They 
    stated that data suggesting a link between additive use and increased 
    CCD with associated increased emissions and ORI is too sparse to reach 
    sound conclusions. These commenters also stated that engine 
    manufacturing tolerances may play a greater role than fuel properties 
    in determining the onset and occurrence of CCDI. Commenters from the 
    petroleum industry stated that, while negative impacts from 
    overtreatment exist, including valve sticking, these occurrences have 
    been very rare and usually result from an accidental overtreatment. In 
    summary, API stated that there is no immediate, growing CCD-related 
    problem in the field, and EPA's planned IVD/PFID control requirements 
    are not likely to cause one. They stated that regulatory control of CCD 
    should not be attempted until the Coordinating Research Council (CRC) 
    has had an opportunity to investigate potential adverse effects of CCD 
    and to gain an understanding of all of the factors which can affect 
    CCD, including hardware, lubricant, fuel and additive effects.
        Commenters from the petroleum industry all agreed that, even if the 
    need to control CCD were demonstrated, setting a cap on the unwashed 
    gum level in additized gasoline would not be an appropriate control 
    measure. They argued that the data offered to support a correlation 
    between unwashed gum levels and CCD formation is unreliable. 
    Furthermore, they claimed that the unwashed gum test is highly 
    unrepeatable and cannot differentiate different sources of the gum 
    content in the gasoline. They also noted that, since many current IVD/
    PFID detergents have varying levels of dispersant and carrier oils 
    (some having no carrier oil), the unwashed gum level in gasoline can be 
    highly misleading as a measure of the amount of additive present.
        Given the disparity in these positions, EPA requested additional 
    input from the affected industries. Additional comment was received 
    from AAMA, API, Shell Development Company, and the Chemical 
    Manufacturer's Association (CMA)\1\ Two technical papers were also 
    published in this time frame that presented additional useful data on 
    CCD related issues.\2\
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        \1\See the memorandum to the docket entitled ``Summary of 
    Additional Comments on Combustion Chamber Deposits'', Docket Item 
    IV-E-35. Discussion of additional comments on CCD is also contained 
    in the following docket items: IV-E-12, IV-E-27, IV-E-29, IV-E-33, 
    IV-E-36, IV-G-37, and IV-E-38.
        \2\``Effects of Gasoline and Gasoline Detergents on Combustion 
    Chamber Deposit Formation'', Yasunori Takei et. al., SAE Technical 
    Paper Series No. 941893. ``Effects of Fuel and Additives on 
    Combustion Chamber Deposits,'' Mitchell Jackson and Sara Pocinki, 
    SAE Technical Paper Series No. 941890.
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    B. Considerations for Determining a Course of Action
    
        EPA is considering the implementation of a CCD control measure at 
    this time in view of auto industry concerns that, absent such a 
    measure, EPA's planned detergent certification program might contribute 
    to CCD-related vehicle performance problems. Any CCD control measure 
    which EPA might require must be based on EPA's belief that such a 
    measure would prevent a future CCD problem or solve one which now 
    exists. In addition, it would have to be practical to implement and be 
    founded on a sound understanding of its impacts. If a control program 
    is found to be needed, it would preferably be based on a national 
    consensus test procedure and performance standard. Because several 
    years may be required to develop such a test procedure and standard, 
    however, a cap on unwashed gums has been suggested as a surrogate CCD 
    control strategy. Thus, to determine whether it is appropriate for EPA 
    to implement an unwashed gum standard for additized gasoline as an 
    interim measure to control the potential additive contribution to CCD, 
    EPA must assess the following questions:
        1. To what extent do some or all IVD/PFID detergents contribute to 
    unwashed gum levels in gasoline? Which, if any, classes/types of 
    additives are of concern? Under what conditions and how substantial is 
    this contribution?
        2. To what extent do gums added to gasoline as part of the 
    detergent additive package correlate or contribute to CCD formation?
        3. To what extent is there now a CCD problem associated with the 
    voluntary use of IVD/PFID detergents? Will mandatory use of these 
    detergents exacerbate the potential concerns?
        4. To what extent do CCD cause vehicle emission and performance 
    problems?
        The information found in the literature and presented by the 
    industry either in their written comments or in response to EPA follow-
    up is helpful in answering these questions. However, more information 
    is needed. These points are discussed below, followed by a discussion 
    of various alternatives that EPA could adopt regarding CCD control. EPA 
    encourages public comment that would help to further the understanding 
    of these issues.
    1. Additive Contribution to Gasoline Unwashed Gum Levels
        The data summarized in the previous section indicate a trend toward 
    increased unwashed gum levels with increased detergent additive use and 
    concentration. Public comment is sought on the unwashed gum levels in 
    additized gasoline for both the various classes/types of detergent 
    additives and individual detergent products. Information is also sought 
    on the relative contribution of various detergent additive package 
    components to unwashed gums. In addition, EPA is also interested in 
    more detail and public comment on claims that some detergents with 
    superior CCD control performance cause relatively high unwashed gum 
    levels in gasoline.
    2. Gum/Additive Package Contribution to CCDs
        The information available seems to support the view that some 
    detergent additives contribute to CCD more than others. However, the 
    significance of this contribution relative to the potential adverse 
    impacts of CCD remains unclear. It is also not completely clear what 
    fraction of the additive types currently used contribute to CCD. This 
    may be a significant concern if a CCD control measure were considered 
    that would preclude the use of a significant fraction of the detergents 
    currently being used. EPA understands that PIBA type detergent 
    additives that use a mineral-based carrier oil predominate in the 
    market. EPA requests comment on several points. First, more data is 
    requested on the relationship between gums, the additive packages, and 
    CCD. Second, EPA is interested in information on which classes/types of 
    additives contribute to this concern more than others and market share 
    and cost information on each type. Third, EPA requests comment on 
    whether the use of a synthetic-based carrier oil rather than a mineral-
    based carrier oil in PIBA detergents would decrease the gum levels and 
    improve the CCD impacts of these additives and the economic impacts 
    which might result from such a change.
    3. Prevalence of CCD-Related Problems Due to Detergent Use and the 
    Effect of IVD Control Requirements on CCD
        More information is needed to quantify the scope of the current CCD 
    problem as it relates to detergent additives. Additional information is 
    needed on the fraction of vehicles with CCD-related performance 
    problems as well as estimates of how the problem could grow with 
    federal detergent requirements. Some public comment presented the 
    viewpoint that the planned IVD/PFID control requirements would not 
    result in over-additization because the primary result would be the use 
    of deposit control additives by all fuel marketers at levels that are 
    currently achieved in the majority of gasoline sold within the U.S. 
    However, this comment neglects concerns about possible over-
    additization to assure compliance during field enforcement as well as 
    for marketing/advertising purposes. EPA encourages additional comment 
    on this issue.
    4. Potential CCD-Related Vehicle Emissions and Performance Impacts
        A review of the available data on the potential impact of CCD on 
    exhaust emissions is suggestive of a potentially significant impact. 
    However, in addition to the prevalence issue discussed above, comment 
    is requested in a number of areas relative to this point. First, 
    comment is requested regarding the role of vehicle technology on the 
    sensitivity to CCD. Second, more information is requested regarding a 
    potential for threshold effect(s). Is there a level below which no CCD 
    effect occurs for emissions, CCDI, ORI, or fuel economy? If thresholds 
    exist, do they vary for the different impacts? In what relative order? 
    Is there a CCD level above which the level of CCD no longer exacerbates 
    the impact? If such thresholds exist, any potential control measure 
    would ideally need to result in the reduction of CCD beyond this 
    threshold to ensure any meaningful emissions benefit. Since there may 
    be a threshold effect for the impact of CCD on fuel economy, the 
    relationship of this threshold to the possible threshold for exhaust 
    emissions and other impacts would also need to be considered in 
    evaluating the overall impact of a CCD control measure. Third, data is 
    needed relating these threshold effects to the amount of detergent 
    additive used. EPA welcomes the submission of any data which might help 
    to clarify these issues.
        The data on CCDI is also not conclusive as to whether this problem 
    is related to fuel quality or vehicle manufacturing problems. EPA 
    encourages the submission of additional data to further evaluate this 
    issue. Of particular value would be data illustrating the extent to 
    which out-of-tolerance engine manufacture may play a role.
        The commenters agreed that problems with intake valve sticking 
    sometimes result from detergent additive overtreatment. However, 
    opinions differed as to the extent of these problems and their 
    relevance to the possible necessity of a standard to limit detergent 
    additive concentration. The data currently available is limited and EPA 
    encourages the submission of additional data to help determine the 
    prevalence of this problem. The data on the potential impact on vehicle 
    performance associated with oil viscosity increase (OVI) from the use 
    of detergent additives is likewise very limited and more data is 
    requested in this area.
    
    C. Alternative Actions Which EPA Could Adopt
    
        Based on the information already available and any additional 
    information received in response to this notice, several options will 
    be considered. Each of these is discussed below.
    1. Option 1: Follow Approach Proposed in NPRM
        The first approach to the CCD issue that EPA is considering is to 
    follow the basic strategy outlined in the NPRM. Under this option, EPA 
    would defer action on CCD pending the gathering of more data, while 
    encouraging responsible actions by industry to develop an industry 
    consensus test procedure and standard. The CRC CCD panel may be in the 
    best position to lead development of national consensus test procedures 
    and standards for CCDs. However, EPA is aware of the disagreement among 
    members of the industry regarding the current direction of the CRC CCD 
    panel's work. Thus, there is considerable uncertainty as to the 
    viability of this option. Members of the CRC's panel from the 
    automobile industry have expressed reservations about whether the 
    investigative work of the CRC CCD panel will proceed rapidly enough to 
    address their concerns regarding the potential impact of CCD on vehicle 
    driveability and on in-use emissions. EPA requests comment on whether 
    it is appropriate to allow industry to evaluate CCD related issues 
    further prior to initiating any potential regulatory action regarding 
    CCD control, or if more immediate intervention on the part of the 
    Agency is necessary.
    2. Option 2: Consideration of a CCD Performance Standard
        As discussed above, the Agency concluded in the proposal that the 
    lack of adequate data relating CCD to emissions, ORI, or other engine 
    performance indicators, as well as the lack of a suitable test 
    procedure, precluded the Agency from proposing a CCD-related detergent 
    additive performance standard at that time. However, the Agency stated 
    that it may, at a later time, propose test procedures and performance 
    standards for the control of CCD (among other deposit-related 
    phenomena).
        In light of recent events (e.g., receipt by EPA of written and 
    verbal comments concerning issues not considered previously), the 
    Agency is again considering the issue of whether or not EPA should 
    pursue such a combustion chamber deposit control performance standard 
    at this time. A discussion of specific issues related to the 
    development of a CCD performance standard is provided in a memorandum 
    to the docket entitled, ``Consideration of a Combustion Chamber Deposit 
    Control Performance Standard'' (Docket Item IV-B-05).
    3. Option 3: Require Data Submission on Unwashed Gums
        As an intermediate measure, EPA could require that data on the 
    unwashed gum levels of additized gasoline be submitted as part of 
    detergent certification. Under this option, the detergent certifier 
    would be required to measure the unwashed gum levels in their 
    certification test fuel using the ASTM D-381 test procedures (see next 
    section). The only requirement would be that these measurements be 
    reported to EPA. Using these data, EPA could assess the difference in 
    unwashed gum levels relative to the chemistry of the detergent additive 
    package to evaluate whether a correlation exists. This information 
    would also be useful in determining what fraction of gasoline is 
    treated using additives that cause high unwashed gum levels for the 
    purposes of evaluating the potential effect on industry of implementing 
    an unwashed gum standard or CCD control program in the future.
        This option would also be beneficial in that it would encourage 
    continued industry focus on CCD-related issues and may encourage the 
    use of additives with better CCD control performance or less of an 
    impact on unwashed gum levels. An unwashed gum reporting requirement 
    would have little economic impact on industry, since the testing would 
    be conducted concurrent with detergent certification testing, would not 
    require a separate submittal to the Agency, and would be of minimal 
    cost. EPA requests comments on the potential benefits and usefulness of 
    this option in responding to current CCD concerns, and on any 
    additional data that EPA should require to be submitted during 
    detergent certification to help evaluate whether a CCD control measure 
    based on an unwashed gum specification is appropriate.
    4. Option 4: Implement an Unwashed Gum Standard
        As a measure to address concerns that detergent over-additization 
    would contribute to CCDs, EPA requests comment on whether it would be 
    appropriate to implement a limit on the unwashed gum level in additized 
    gasoline as part of the requirements for detergent certification. As 
    previously discussed, questions remain regarding the need for a full 
    regulatory program to control CCD effects, and the potential associated 
    impacts on emissions, fuel economy and vehicle driveability. While some 
    public comments suggest that limiting the additive contribution to 
    unwashed gums would not necessarily always result in a reduction in 
    CCD, it is possible that an intermediate measure such as this would 
    address the most significant concerns raised by the auto industry 
    commenters without levying large direct compliance costs on the fuel 
    and detergent additive industries. As perceived by the regulated 
    industry the benefits may be very small, but, as discussed below, costs 
    would also be very small. On the other hand, this requirement could 
    make detergent packages with higher gum levels less attractive and 
    could act as a disincentive for research on detergent additive packages 
    with high gum levels. If an unwashed gum standard is established, EPA 
    asks comment on whether such a standard should only be implemented for 
    an interim period, assuming a CCD test procedure/ standard is 
    established by regulation.
        a. Unwashed Gum Test Procedure. If an unwashed gum standard is 
    adopted, it would likely need to be implemented by requiring testing of 
    unwashed gum levels in detergent-additized gasoline using the ASTM D381 
    procedure or a derivation of this procedure. Concerns have been raised 
    about the repeatability and reproducibility reported for this procedure 
    in the ASTM D381 document, and EPA believes it would be useful to 
    further explore the reasons for the reproducibility and repeatability 
    performance cited in the procedure. In discussions with industry 
    experts regarding the ASTM D381 procedure, one member of the panel 
    which originally developed the procedure suggested the possibility that 
    greater precision might be expected in measuring the unwashed gum 
    levels of modern gasoline. The repeatability/reproducibility data in 
    the ASTM procedure is based on gasolines of the 1960s and 1970s.\3\ EPA 
    requests comment on the extent to which gasoline composition can effect 
    the precision that can be achieved in the ASTM test.
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        \3\Memorandum to the docket entitled, ``Phone Call with Leo 
    Stavinola of Southwest Research Institute (SwRI), Regarding the 
    Applicability of the Unwashed Gum Test to Modern Gasoline'', Docket 
    Item IV-E-33.
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        EPA's analysis of 1993-94 unwashed gum data collected under ASTM's 
    Interlaboratory Crosscheck Program suggests that the current 
    reproducibility of the procedure may be somewhat better than that 
    reported in the D381 document.\4\ However, the limited range of 
    unwashed gum values represented in the test samples prevents an 
    accurate assessment of test variability over the range of unwashed gum 
    values likely to be encountered in use.
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        \4\Report to EPA from George Hoffman, CSC, entitled ``Sample 
    Sizes for Unwashed Gums Measurements''.
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        Not all laboratories using the D381 unwashed gum procedure 
    encounter the variability discussed in the ASTM document. EPA contacted 
    Southwest Research Institute (SwRI) to further evaluate the suitability 
    of the unwashed gum test from the standpoint of repeatability and 
    reproducibility.\5\ SwRI stated that the unwashed gum test is used 
    routinely by their laboratory to determine whether or not gasoline had 
    been detergent additized. In addition, SwRI related that not only was 
    this test a useful predictor of additive presence, but it could also 
    distinguish additive concentration fairly well. SwRI stated that, in 
    their considerable experience in performing the unwashed gums test, 
    they have achieved significantly better repeatability than that 
    reported in the ASTM procedure. For example, at an unwashed gum level 
    of 60 mg/100 ml, they commonly achieve repeatability of results within 
    5 mg/100 ml, as compared to the 25 mg/100 ml 
    reported in the ASTM procedure. A round robin program conducted by AAMA 
    using three fuels and four labs also indicated good reproducibility 
    (coefficients of variation of 6 percent, 12 percent, and 2 percent) for 
    the three fuels tested. (See memo in public docket at IV-G-39).
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        \5\Memorandum to the docket entitled ``Phone Call with Karen 
    Kohl of Southwest Research Institute (SwRI) Regarding the Unwashed 
    Gums Test,'' Docket Item IV-E-32.
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        SwRI stated that they are aware of several potential problems that 
    may partially account for the poor reproducibility reported by ASTM. 
    SwRI related that the temperature of the evaporation bath and the flow 
    of air to the airjet apparatus must be carefully controlled to limit 
    the variability in results. SwRI also related that another potential 
    problem which can introduce variability in test results is 
    contamination of the oil from the supply pumps. If the repeatability 
    reported by SwRI and the reproducibility achieved in the AAMA study 
    could also be achieved at other laboratories, it might be possible to 
    achieve adequate test precision while minimizing the required number of 
    repeat tests.
        EPA requests comment on ways in which the ASTM D381 procedure could 
    be modified to limit test variability. In particular, EPA requests 
    comment on whether additional specifications are required regarding 
    control of the evaporation bath temperature, flow of air to the air jet 
    apparatus, and prevention of oil contamination of the fuel sample from 
    the supply pumps. Specifically, EPA is considering tighter 
    specifications on several elements of the test including the air jet 
    apparatus to 600mL/s 30 mL/s, the steam jet apparatus to 
    1000 mL/s 50 mL/s, and the evaporation bath well 
    temperature to 155 deg.C 2  deg.C. Use of a temperature 
    measuring approach other than a thermometer (e.g., thermocouple with 
    digital readout) is also being considered. Other similar modifications 
    to test specifications will also be considered to the degree that they 
    would reduce variability. The submission of test data from the ASTM 
    D381 procedure would also be useful in assisting further evaluation 
    evaluating test repeatability and reproducibility.
        b. Unwashed Gum Limit. If an unwashed gum standard for additized 
    gasoline is adopted, it must be carefully selected based on the 
    consideration of several factors. First, the available data suggests 
    that the contribution to unwashed gums from sources other than 
    detergent additives is generally under 10 mg/100 ml per the ASTM test. 
    This consideration is important because the focus of an unwashed gum 
    standard must be on the additive contribution to gums. EPA believes 
    that it may be reasonable to assume that the base fuel contribution to 
    gasoline unwashed gum levels does not exceed 10 mg/100 ml. EPA requests 
    data to further evaluate whether this assumption is appropriate.
        Second, the choice of an unwashed gum cap should be based on an 
    understanding that such a cap would result in an appropriate level of 
    CCD control. This involves consideration of the possible threshold 
    effects of CCD-related emissions, fuel economy, and vehicle 
    driveability impacts. EPA requests comments on what would be an 
    appropriate unwashed gum cap given these considerations.
        There were two separate suggestions in the public comment regarding 
    the choice of an appropriate unwashed gum cap. The first suggestion was 
    to adopt the unwashed gum cap already in place for Japanese gasoline of 
    20 mg/100 ml.\6\ This suggestion was based on the premise that the 20 
    mg/100 ml cap has been in force for Japanese gasoline for some time, 
    that industry has been able to comply with this cap while meeting other 
    deposit control performance needs, and that the presence of such a cap 
    might be credited for the absence of CCD-related problems in Japan. EPA 
    is concerned about setting a potential standard at this level, because 
    it would prevent the use of many current IVD/PFID detergents. Assuming 
    absolute precision in unwashed gum measurement, a 20 mg cap would limit 
    the additive contribution to unwashed gums to about 10 mg. The 
    available data indicates that this is significantly less than the 
    contribution to unwashed gums for IVD/PFID detergents currently used in 
    the U.S. which typically appears to be between 20 and 60 mg/100 ml and 
    can be considerably higher.\7\ EPA's review of AAMA gasoline survey 
    data reveals that less than 40 percent of U.S. gasoline samples tested 
    had an unwashed gum level below 20 mg/100 ml.\8\ One explanation for 
    the apparent large difference in unwashed gum levels in Japanese and 
    U.S. gasolines might be that Japanese gasoline tends to require less 
    detergent for adequate IVD control. EPA requests comment that would 
    help explain the difference between the unwashed gum levels in Japanese 
    and U.S. gasoline.
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        \6\Written comments on the NPRM from Mazda Motor Corporation, 
    Docket Item IV-G-17, and from Toyota Motors Inc., Docket Item IV-G-
    25.
        \7\Letter to Glenn Passavant, Office of Mobile Sources, from 
    James Williams, American Petroleum Institute, Docket Item IV-G-36.
        \8\AAMA unleaded gasoline survey data, 1991-1993, California 
    gasoline excluded.
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        AAMA suggested a significantly higher unwashed gum cap than that 
    observed in Japan. AAMA contended that their suggested cap of 70 mg/100 
    ml took into account the base gasoline contribution to gums and the 
    variability in the ASTM test procedure, and would allow the use of 
    detergents capable of IVD, PFID and CCD control. They further stated 
    that compliance with this cap could be achieved using current additive 
    technology that results in unwashed gum levels of 35 to 40 mg/100 ml. 
    AAMA's suggestion is based on the premise that an appropriate level of 
    control of the detergent additive contribution to CCD can be achieved 
    by preventing the use of the highest concentrations of detergent 
    additives and unnecessary over-additization. EPA's review of AAMA 
    gasoline survey data reveals that more than 90 percent of U.S. gasoline 
    samples analyzed had unwashed gum levels below 70 mg/100 ml. A review 
    of the same data also showed that approximately 35 percent of U.S. 
    gasoline had unwashed gum levels in excess of 40 mg/100 ml. Thus, 
    depending on the precision of the unwashed gum test, a 70 mg/100 ml 
    unwashed gum cap could result in disqualification for use of detergent 
    packages/concentrations used in approximately 10 to 35 percent of 
    gasoline in the U.S.
        EPA requests comment on the suitability of an unwashed gum cap of 
    70 mg/100 ml. In particular, EPA requests comment on the potential 
    benefit of implementing such a standard, and the ability of industry to 
    meet IVD/PFID deposit control requirements with additives that comply 
    with a 70 mg/100 ml unwashed gum standard.
        Given concerns expressed by some commenters about variability, EPA 
    proposes that certification or data submission requirements be based on 
    the average of five unwashed gum tests (ASTM D381). With regard to an 
    unwashed gum standard, EPA asks for comment on the minimum number of 
    unwashed gums tests which should be specified to demonstrate compliance 
    and, as an option to industry, the maximum number which could be 
    allowed.
        c. Incorporation of Unwashed Gum Standard Into the Detergent 
    Certification Program. If EPA adopts an unwashed gum standard or 
    requires submission of unwashed gum levels, the primary compliance 
    focus would be placed on unwashed gum testing of the properly additized 
    test fuel(s) used during detergent certification. One option would be 
    to require the measurement of the unwashed gum level of a test fuel 
    blended with the minimum treatment rate of the detergent package as 
    determined by certification testing for IVD/PFID control. To limit 
    variability in the base fuel contribution to unwashed gums, the test 
    fuel would be required to comply with other specifications regarding 
    gasoline composition (i.e., aromatic, olefin, T-90 and oxygenate 
    content) prescribed for detergent certification testing. For the 
    detergent additive to be certified, the unwashed gum level in this test 
    (or the average for a series of tests) would need to be below the 
    unwashed gum standard.
        One of the major issues raised by the auto industry commenters was 
    concern that over-additization could lead to increased gum levels and 
    CCD-related problems. While there may be no economic incentive to over-
    additize, it is likely to occur. It may occur accidentally, some fuel 
    manufacturers may choose to slightly over-additize to ensure compliance 
    with the volume accounting reconciliation requirements of EPA's 
    enforcement program, or it may occur for other reasons such as 
    advertising. One way to accommodate these possibilities and yet also 
    address the concerns of auto makers is to set the concentration of the 
    additive in the test fuel during testing for unwashed gums at a level 
    higher than the certified treat rate. For example, requiring 
    certification to the unwashed gum standard (or testing of unwashed gums 
    under Option 3) at a level of 110 percent of the certified treat rate 
    would allow the assessment of the impact of a slight over-additization 
    without creating an unreasonable obstacle to compliance. This would 
    also allow for some variation in the unwashed gum level of the 
    unadditized gasoline. Yet another approach with a similar effect would 
    be to reduce the proposed standard by 10 percent. That is, instead of 
    20 mg/100 ml or 70 mg/100 ml, the standard would be set at 18 mg/100 ml 
    or 63 mg/100 ml with testing conducted at the certified treat rate.
        The detergent registration and certification programs require that 
    each gasoline contain detergent in an amount at least equivalent to the 
    minimum certified treat rate. No maximum limit is anticipated. While 
    testing at 110 percent of the minimum certified treat rate would 
    address slight over-additization when the minimum treat rate is the 
    actual target concentration, it will not be representative for fuels 
    additized at even higher rates. EPA, therefore, asks comment on an 
    option which would require those fuel manufacturers who add detergent 
    at greater than 110 percent of the minimum treat rate to pass the 
    unwashed gum standard using fuel treated at the rate actually being 
    used.
        As an ancillary enforcement tool, EPA might also require the 
    submission of test data on the unwashed gum levels of in-use fuels from 
    detergent additive blenders. In-use testing of unwashed gum levels 
    might also be conducted by EPA. EPA does not anticipate that such in-
    use testing would be conducted routinely, but rather that it would be 
    used in cases where there was a suspicion of violation, or would be 
    conducted randomly to encourage compliance. Penalties for noncompliance 
    with an unwashed gum standard would be similar to those for 
    noncompliance with minimum concentration requirements. EPA requests 
    comments on the potential certification and enforcement requirements 
    described above as well as input on other options.
        d. Costs and Benefits. The potential economic impacts of 
    implementing an unwashed gum standard or data submission requirement 
    vary with the provisions of the potential program, but in general would 
    be similar. First, EPA needs to further evaluate the number of unwashed 
    gum tests that would be required for each detergent certification. If a 
    single unwashed gum test was performed during certification testing, 
    the additional cost for each certification would be approximately $100 
    for a total cost to industry of approximately $40,000 for the 
    approximately 400 detergents certified in the first year of the 
    program. (This assumes that these tests are not already conducted for 
    other reasons. If multiple tests are used to reduce variability 
    concerns raised in association with the ASTM D381 test, the total cost 
    would be somewhat higher. If, for example, five tests were conducted as 
    proposed above, the total cost for all detergents would be $200,000 in 
    the first year. Recurring annual costs would vary between $6,000 and 
    $30,000 assuming 15 percent new certifications per year.
        While it may be difficult to quantify the emission benefits, it is 
    possible to estimate whether such a program could be cost effective. 
    One approach would be to calculate the amount of emissions that would 
    need to be prevented by an unwashed gum standard for the control 
    measure to be cost-effective. If the costs were low, the amount of 
    emissions that would need to be prevented could be relatively small and 
    yet the program could still be quite cost effective. Using the first 
    year cost of $200,000 discussed above, only 200 tons of HC/NOx emission 
    reductions would be required to achieve a nominal cost effectiveness of 
    $1,000 per ton. Given the large number of miles travelled per year by 
    gasoline-fueled vehicles, only a tiny fraction of the fleet would have 
    to get a tiny benefit for this level of benefits to be achieved. For 
    example, less than a hundredth of one percent of vehicles would have to 
    achieve a 0.01 g/mi benefit in order to achieve this benefit. This 
    level of benefits and more appears quite conceivable. The potential 
    negative impact of fuel economy that may accompany a reduction in CCDs 
    complicates consideration of the potential economic impact of the 
    program, as do potential adverse impacts on companies manufacturing 
    detergent additives with high unwashed gum levels. EPA requests comment 
    on the approach to determine the cost- effectiveness of CCD control 
    outlined above and on a method by which any potential negative impact 
    on fuel economy might be accounted for. EPA also asks comment on 
    whether it is possible to reduce emissions or prevent emission problems 
    without adversely affecting fuel economy. It should be noted that 
    section 211(l) of the CAA does not require EPA to justify deposit 
    control measures on a cost-effectiveness basis. However, EPA will give 
    the costs and benefits of any potential CCD control measure due 
    consideration.
    5. Other Options
        a. Use of a Standard Based on Thermogravimetric Analysis of 
    Detergent Additives as an Interim CCD Control Measure. EPA requests 
    comment on whether a standard based on thermogravimetric analysis (TGA) 
    of detergent additives could be used as an interim measure to limit the 
    additive contribution to CCD. Such a standard would be based on the 
    premise that, to limit the additive contribution to CCD, a detergent 
    additive must decompose at temperatures encountered in the combustion 
    chamber. Any additive which does not decompose and burn in the 
    combustion chamber may provide material for the formation of CCD. 
    Thermogravimetric analysis is one method of determining the thermal 
    characteristics of materials, and might be useful in determining what 
    portion of detergent additive packages remain unburned and may 
    contribute to the formation of CCD.
        One potential TGA-based standard would require that, as part of 
    detergent certification testing, a TGA analysis would be performed on 
    the detergent additive package. For a detergent to be certified, the 
    residue of the detergent package left at the specified temperature 
    would be required to not exceed a specified fraction by weight of the 
    original sample. Specifying a testing temperature is a critical element 
    in a potential TGA-based CCD control standard. Recent research 
    indicates that the surface temperature in the combustion chamber may be 
    the most important physical parameter in the formation of CCD.\9\ This 
    research indicates that, with high surface temperatures, CCD will reach 
    stabilized levels earlier and the total amount of deposits will be 
    lower. It further indicates that the critical surface temperature 
    beyond which no additional fuel-derived CCD form is 310  deg.C, and the 
    critical surface temperature beyond which no oil-derived deposits form 
    is approximately 60  deg.C higher. This research may be useful in 
    helping to determine the proper test temperature specification for a 
    TGA-based CCD control standard. EPA requests comment on an appropriate 
    temperature specification.
    ---------------------------------------------------------------------------
    
        \9\``A Physical Mechanism for Deposit Formation in a Combustion 
    Chamber'', Society of Automotive Engineers (SAE) Technical Paper 
    Series No. 941892.
    ---------------------------------------------------------------------------
    
        Comment is also requested on the allowable fraction of the additive 
    package which could remain as residue after the completion of the TGA 
    analysis. EPA believes that, for a TGA-based standard to provide a 
    meaningful measure of CCD control, the specification on the allowable 
    amount of residue would need to be set in the range of 2 percent of the 
    original sample. EPA requests comment on whether, alternately, it would 
    be more appropriate to place an absolute specification on the allowed 
    weight of detergent residue for a given quantity of additized gasoline, 
    and what an appropriate specification would be. Comment is also 
    requested on what procedural guidelines EPA should implement for the 
    TGA test.
        The detergent additive package on which a TGA analysis was 
    performed would be required to contain the maximum concentration of the 
    detergent-active components covered under a registration. Use of these 
    components at higher concentrations to fulfill gasoline detergency 
    requirements would be prohibited. To enforce such a requirement, EPA 
    could require that samples of detergent additive be tested by the 
    additive manufacturer or submitted by the additive manufacturer for 
    analysis by EPA. A violation would occur if this sample failed to 
    satisfy the specified TGA-based limit. Alternately, a violation would 
    occur if, through fourier transform infrared spectroscopy (FTIR) 
    analysis, a sample was found to contain higher concentrations of 
    detergent-active components than those specified in the registration.
        b. Use of Existing CCD Control Performance Data. One commenter 
    suggested that, as an interim measure, EPA require vehicle/engine CCD 
    control test data to be submitted by each detergent certifier without 
    detailing any requirements regarding the acceptability of the data. EPA 
    believes that such a requirement, while potentially encouraging 
    responsible consideration of CCD control by industry, would not provide 
    a meaningful measure of an additive's CCD control performance. EPA 
    believes that CCD control performance testing is too ill defined to 
    allow EPA to implement guidelines regarding its acceptability. The 
    Agency encourages public comment on this and other options that EPA 
    might adopt to control the potential adverse impacts of detergent 
    additive overuse.
    
    D. Relationship to California Detergent Additive Program
    
        Under EPA's proposed detergent certification requirements, a 
    detergent certified for use under the state of California's detergent 
    program (Title 13, section 2257 of the California Code of Regulations) 
    could be used to satisfy federal detergency requirements for gasoline 
    sold in California. The detergent additive certification requirements 
    currently implemented by the state of California include IVD/PFID 
    control requirements but do not include any unwashed gums or other CCD 
    control provisions. Therefore, if EPA were to implement an unwashed gum 
    standard or reporting requirement, a detergent certified by the 
    California Air Resources Board (CARB) would need to satisfy these 
    requirements in addition to complying with CARB's detergent 
    certification program in order to be eligible for use in complying with 
    federal detergency requirements in the state of California.
    
    III. Other Issues for Additional Comment
    
    A. Formulation of Certification Test Fuels
    
        The discussion in this notice regarding the formulation of 
    certification test fuels pertains specifically to measures which EPA 
    might take to account for yet-to-be-identified nonoxygenate fuel 
    severity factors. Also discussed is the potential difference in the 
    deposit forming tendency of ethanol produced by different processes, 
    and measures that EPA might take to account for this variability. Other 
    issues related to test fuel definition will be addressed in the 
    detergent certification final rule.
    1. Accounting for Unidentified Nonoxygenate Fuel Severity Factors
        a. Approach Proposed in the NPRM. Under the proposed requirements, 
    certification testing for IVD/PFID control would normally be conducted 
    using a matrix of four test fuels, although testing in as few as two 
    fuels would be allowed under certain circumstances. Test fuels would be 
    required to meet or exceed minimum specifications regarding the levels 
    of the following four nonoxygenate fuel parameters which EPA believes 
    affect the deposit forming tendency of gasoline (referred to as fuel 
    severity factors): olefins, sulfur, aromatics, and T-90 distillation 
    point. To account for the deposit forming tendency of oxygenates, one 
    fuel would be required to contain 10 percent ethanol, and another would 
    be required to contain 15 percent MTBE. The NPRM included provisions 
    allowing other fuel parameters to be used to define certification test 
    fuels if their effect on IVD/PFID fuel severity could be demonstrated.
        In the NPRM, EPA discussed concerns that specifications on these 
    fuel severity factors may not completely define a gasoline's deposit 
    forming severity. If this were the case, detergent certifiers might be 
    able to locate or specially blend certification test fuels that meet 
    the proposed compositional requirements but are still inappropriately 
    mild in their deposit forming tendency. To help account for unknown 
    factors in gasoline composition that may affect fuel severity, EPA 
    proposed that gasoline samples for certification testing must be drawn 
    from normal production gasoline stock (finished commercial gasoline) 
    taken from normally operating refinery and/or terminal facilities. In 
    addition, the multiple test fuels were to be drawn from separate 
    production/distribution facilities. This requirement would increase the 
    certainty that unknown severity factors will be represented by ensuring 
    that various refinery stocks are tested. It would also tend to limit 
    the opportunity to select test fuels from refineries that, for 
    unidentified reasons, tend to produce gasoline with a relatively low 
    deposit forming tendency.
        b. Public Comment on the Proposal. Comments submitted by API and 
    CMA stated that requiring commercial fuels for testing would be 
    extremely burdensome and would have impractical consequences with 
    regard to the logistics and mechanics of obtaining non-additized fuel. 
    Amoco, API, CMA, Nalco, Texaco, and Ashland stated that EPA should 
    allow the use of refinery blend stocks that meet ASTM D4814 
    specifications to formulate certification fuels. It was also suggested 
    that the finished certification test fuels should meet ASTM D4814 
    specifications. One commenter stated that, to help alleviate concerns 
    regarding fuel blending, the identity of each blending component should 
    be documented regarding its source and properties.
        AAMA stated that there might be characteristics that effect a 
    gasoline's deposit forming tendency which are not represented by 
    consideration of the five parameters proposed to define certification 
    test fuels. AAMA acknowledged that there are no data available to 
    determine which additional parameters would be appropriate to include 
    in the test fuel specifications. However, AAMA stated that 
    certification test fuels could be made more representative by requiring 
    that the major refinery streams be represented in the blending stocks 
    used to formulate these fuels. Such a practice would tend to help 
    ensure that yet-to-be-identified fuel severity factors are represented 
    in the certification test fuels. AAMA stated that requiring more than 
    one certification test fuel would allow for the inclusion of more 
    refinery streams in the formulation of certification test fuels, 
    thereby enhancing the representativeness of the testing.
        Comments from API and CMA requested that EPA allow certification 
    testing on a single fuel, formulated from refinery blend stocks, that 
    contains each nonoxygenate fuel severity factor at its highest level in 
    the proposed test fuel matrix, plus 10 percent ethanol. These 
    commenters stated that the increase in gasoline deposit forming 
    tendency resulting from the addition of 10 percent ethanol is more than 
    enough to address concerns about the potential deposit forming tendency 
    of MTBE. Hence, testing on a second MTBE-containing fuel should not be 
    required. On the other hand, commenters from the automobile industry 
    stated that testing on both ethanol- and MTBE-containing fuels should 
    still be required to account for differences in their tendency to form 
    deposits.
        c. Alternative Approaches that EPA Might Adopt. EPA is considering 
    several approaches, in addition to those proposed in the NPRM, to help 
    ensure the representativeness of the certification test fuels. Under 
    the first option, specifications on fuel parameters in addition to the 
    five that were proposed to be used to define certification test fuels 
    (olefins, sulfur, aromatics, T-90 distillation point, and oxygenate 
    content) would be added to better define the test fuels deposit forming 
    tendency. The NPRM discussed other fuel parameters that might have an 
    impact on a gasoline's tendency to form deposits. Several of these are 
    refinements on the nonoxygenate fuel parameters already considered.
        The limited data available indicates that diolefins may affect a 
    gasoline's tendency to form deposits more significantly than do mono-
    olefinic species. Certain species of sulfur, such as ditertiary butyl 
    disulfide, may also have more of an impact on a gasoline's deposit 
    forming severity than do other species of sulfur. In addition, limited 
    data suggests that heavier, polycyclic aromatic species may have a 
    greater impact on fuel severity than do other aromatic species. These 
    additional fuel parameters might be used in place of, or in addition 
    to, the less specific fuel parameters proposed in the NPRM (total 
    olefins, total sulfur, and total aromatics). Data were also discussed 
    in the NPRM suggesting that fuel nitrogen content might be useful in 
    helping to define the deposit forming tendency of certification test 
    fuels.
        Nevertheless, the data available appears to be insufficient to 
    positively identify these fuel parameters as additional severity 
    factors. Also, since levels of such fuel parameters as diolefins, 
    ditertiary butyl disulfide, polycyclic aromatics, and fuel nitrogen are 
    not commonly measured or reported, it would be difficult to determine 
    what levels of these additional fuel parameters would be appropriate to 
    require in certification test fuels. As noted earlier, the proposed 
    test fuel specifications on the levels of sulfur, olefins, aromatics, 
    and T90 were based on national gasoline survey data. EPA requests 
    comments on what additional fuel parameters could be used to help 
    better define the severity of certification test fuels, and on the 
    levels of such fuel parameters that would be appropriate to require in 
    the test fuels to ensure adequate deposit control.
        Given that it may not be feasible to use specifications on 
    additional fuel parameters to better define the severity certification 
    test fuels, EPA is considering several other alternatives to improve 
    their representativeness. One such approach would be to specify the 
    refinery blendstocks which must be used in the formulation of 
    certification test fuels. Due to their potential impact on the deposit 
    forming tendency of finished gasoline, EPA believes that specifications 
    on the minimum proportions of the following gasoline blendstocks to be 
    used in the formulation of certification test fuels may be useful in 
    helping to better define test fuel severity: full range fluid 
    catalytic-cracked (FCC) naphtha, full range reformate, full range 
    straight run naphtha, and light coker naphtha.
        The relative proportions of these blendstocks required to be used 
    in the formulation of certification test fuels could be based on the 
    fraction at which they are used in blending finished gasoline in the 
    U.S. In keeping with the proposed certification test fuel 
    specifications, which require that each of the four nonoxygenate fuel 
    severity factors must be represented at levels greater than their 
    respective national average levels, it may be appropriate to require 
    that the subject blendstocks be represented in the certification test 
    fuels at proportions that exceed their average representation in 
    finished U.S. gasoline. Based on this approach, appropriate 
    specifications on the minimum percentage of the subject refinery 
    blendstocks which must be used in formulating the certification test 
    fuels are likely to fall within the following ranges: 25 to 40 percent 
    full range FCC naphtha, 25 to 40 percent full range reformate, 1 to 3 
    percent full range straight run naphtha, and 1 to 3 percent light coker 
    naphtha.\10\ These specifications would account for approximately 50 to 
    85 percent of the gasoline blendstocks used in formulating 
    certification test fuels. The remaining blending components used in 
    formulating the test fuels could be drawn from any type of refinery 
    blendstock.
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        \10\For a review of the quantities of manufactured gasoline 
    blendstocks blended into U.S. gasoline during the period of April 1 
    through September 30, 1989, see the National Petroleum Refiners 
    Association Survey of U.S. Refining Industry Capacity to Produce 
    Reformulated Gasolines, part A, January 1991.
    ---------------------------------------------------------------------------
    
        EPA requests comment on the usefulness of this approach in 
    accounting for yet-to-be-identified fuel severity factors and in 
    preventing the use of certification test fuels with inappropriately 
    mild deposit forming severity. EPA specifically requests comment on 
    which refinery blend stocks should be included and on the proportions 
    at which they should be represented in the test fuels. EPA also 
    requests comment on the number of test fuels which would be needed to 
    adequately represent all the relevant refinery blend stocks given the 
    need to meet EPA's proposed fuel compositional specifications 
    (regarding minimum required levels of olefins, sulfur, aromatics, T-90, 
    and oxygenates). EPA believes that a single test fuel may not be 
    adequate for this purpose. In addition, the Agency requests comment on 
    the extent to which previous commenters concerns regarding potential 
    logistical problems associated with EPA's proposal to require testing 
    of finished commercial fuels also apply to the approach of formulating 
    test fuels from specified proportions of particular refinery blend 
    stocks.
        Another approach EPA is considering would involve raising the 
    levels of the four nonoxygenate fuel parameters required in the 
    certification test fuels. This approach may be useful in helping to 
    limit the variability in fuel severity for a given fuel specification, 
    because the extent of this variability may tend to decrease as levels 
    of these fuel parameters increase. EPA is considering requiring that 
    the 65th percentile levels of these four nonoxygenate fuel parameters 
    must be present in the certification test fuels after the addition of 
    oxygenates, rather than before their addition as was proposed. This 
    approach is being considered due to public comment on the NPRM which 
    indicated that allowing the levels of these fuel parameters to be 
    diluted by the addition of oxygenate may inappropriately reduce test 
    fuel severity. If EPA were to take such an approach, the resulting 
    increase in fuel severity may tend to reduce concerns over the 
    variability in fuel severity due to the effect of yet-to-be identified 
    fuel parameters. EPA requests comment on the extent to which 
    variability in test fuel severity would continue to be a concern if 
    such an approach were adopted.
        EPA also requests comment on whether it would be appropriate to 
    increase the required levels of the nonoxygenate fuel parameters still 
    further to limit the variability. To this end, EPA is considering 
    requiring that each of the nonoxygenate fuel parameters must be 
    represented in the certification test fuels at their respective 70th 
    percentile levels after the addition of oxygenate. Such comment should 
    also address the potential that such an upward adjustment in test fuel 
    severity may cause higher concentrations of detergent additive to be 
    used, with an associated heightening of concerns regarding the additive 
    contribution to the formation of CCD.
        Another approach EPA is considering would require that the deposit 
    forming tendency of test fuels be demonstrated through testing of the 
    non-additized fuels prior to their use for certification testing 
    purposes. Under this approach, each test fuel would be evaluated for 
    its tendency to form intake valve deposits using the BMW 318i test 
    procedure (as adopted by EPA for certification testing). The cost of 
    implementing such a requirement would naturally increase with the 
    number of test fuels required, and its adoption would be most 
    economical if only a single test fuel formulation were required. For a 
    fuel to be acceptable for use in certification testing, a specified 
    deposit weight would need to be accumulated during pre-certification 
    testing of the fuel in an unadditized state. EPA is considering several 
    alternative test fuel evaluation criteria. Under the first alternative, 
    at least 150-250 mg of intake valve deposits (on average) would be 
    required to be accumulated over the course of 10,000 test miles for a 
    test fuel to be acceptable. Under the second alternative, at least 80-
    120 mg of IVD would be required to be accumulated over the course of 
    5,000 test miles. Specific comment is also sought on point values 
    within the two mg ranges presented above.
        EPA requests comment on whether this approach is a necessary and 
    useful measure to ensure the representativeness of certification test 
    fuels. Comment is requested on whether it would be useful to require 
    that fuels meet compositional specifications if EPA were to require 
    that they be tested to demonstrate adequate deposit forming severity 
    prior to use for certification purposes. Specific comment is requested 
    on the level of IVD that should be required to be generated for a test 
    fuel to be acceptable as having an adequately severe deposit forming 
    tendency. EPA also requests comment on whether it is necessary to 
    require demonstration of a test fuel's tendency to form fuel injector 
    deposits (PFID) and the appropriate test/standard which might be used 
    to accomplish this purpose. One option under consideration is use of 
    the Chrysler 2.2L vehicle in the ASTM test with the fuel required to 
    generate a flow restriction in the range of 10-20 percent. Specific 
    comment is requested on this option including a point in the range and 
    also on whether a bench rig test may be sufficient to screen a test 
    fuel for its tendency to form PFID. Comment is also requested on other 
    measures which may be implemented to ensure the representativeness of 
    certification test fuels.
    2. Accounting for Potential Variability in the Deposit Forming Severity 
    of Ethanol
        EPA proposed that the ethanol used in formulating certification 
    test fuels must be of fuel-grade quality. Specially processed ethanol 
    would not be acceptable for use in formulating certification test 
    fuels. This requirement was proposed to account for the deposit forming 
    tendency of other substances commonly found in fuel-grade ethanol. EPA 
    now believes that depending on the processing method used to produce 
    fuel-grade ethanol, various levels and types of impurities may be 
    present. These varying levels of these impurities, such as fatty acids, 
    might potentially effect the deposit forming severity of fuel-grade 
    ethanol to different degrees. If this were the case, certification 
    testing could be conducted using fuels blended with fuel-grade ethanol 
    that has an inappropriately low tendency to increase gasoline forming 
    tendency.
        EPA requests comment on the extent to which this is a concern and 
    on potential approaches that EPA might take to ensure that the ethanol 
    used during certification testing is representative of in-use ethanol 
    blending stock in its tendency to from deposits. One approach would be 
    to require that ethanol used for certification testing purposes must 
    contain a minimum level of impurities. Specifications might also be 
    necessary on the type of impurities which must be present. The maximum 
    allowed levels of impurities specified in commercial standards for 
    fuel-grade ethanol might be useful in determining the levels of 
    impurities that must be present in ethanol used for certification 
    testing. Potable and chemical grade ethanol as well as fuel grade 
    ethanol which receives additional processing not common to all fuel 
    grade ethanol could not be used in testing. EPA also requests comment 
    on the extent to which the concerns discussed above may also apply to 
    MTBE used in certification testing. EPA also asks for comment on 
    whether the restrictions discussed above for ethanol should also be 
    applied to MTBE.
    
    B. ASTM IVD and PFID Control Test Procedures
    
        In the NPRM, EPA proposed test procedures to evaluate IVD and PFID 
    control that were largely based on draft procedures under evaluation by 
    the American Society for Testing and Materials (ASTM) at the time of 
    the proposal. EPA also proposed that the ASTM test procedures might be 
    adopted in the detergent certification final rule if they were 
    finalized by ASTM in time, and there were no changes that would require 
    further public notice and comment.\11\ These test procedures have 
    recently been finalized by ASTM and EPA anticipates their adoption 
    under the detergent certification final rule.\12\ EPA requests comment 
    this approach. EPA proposed an alternate IVD control standard at a 
    5,000 mile test length, in addition to the traditional 10,000 mile 
    standard. Comment is requested on what addition to the ASTM IVD control 
    procedure would be necessary to allow the use of a 5,000 mile test 
    length as well as the 10,000 mile test length specified by ASTM.
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        \11\Drafts of the ASTM IVD and PFID test procedures were placed 
    in the public docket for review.
        \12\The ASTM procedures are designated as follows: ASTM test 
    method D 5500, ``Standard Test Method for Evaluation of Unleaded 
    Automotive Spark-Ignition Engine Fuel for Intake Valve Deposit 
    Formation'', and ASTM test method D 5598, ``Standard Test Method for 
    Evaluating Unleaded Automotive Spark-Ignition Engine Fuel for 
    Electronic Port Fuel Injector Fouling''.
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    C. Applicability of Gasoline Detergency Requirements
    
        The gasoline detergency requirements implemented by the interim 
    detergent registration rule apply to all gasoline, leaded and unleaded, 
    highway and off-road, including both reformulated and conventional 
    gasolines, oxygenated gasoline, and the gasoline component of M85 and 
    E85, as well as marine fuel and gasoline for military purposes. (M85 is 
    a mixture of 85% methanol and 15% gasoline. E85 is a mixture of 85% 
    ethanol and 15% gasoline.) Gasoline service accumulation fuel is also 
    required to comply with gasoline detergency requirements, as is the 
    gasoline component of alcohol blend service accumulation fuel. As noted 
    in the detergent registration final rule, the following types of 
    gasoline are exempted from compliance: aviation fuel, racing fuel, 
    emissions certification fuel, and gasoline used for research and 
    developmental purposes. Gasoline detergency requirements apply to all 
    gasoline other than those types for which an exemption was specifically 
    prescribed.
        As an example, although not specifically mentioned in the 
    regulation, since it is to be used in highway motor vehicles factory 
    fill fuel must comply with gasoline detergency requirements.\13\ 
    Factory fill fuels must comply with these requirements despite the 
    exemption from general fuel registration requirements noted for these 
    fuels in 40 CFR 79.4(a)(3).
    ---------------------------------------------------------------------------
    
        \13\Factory fill fuels must comply with these requirements 
    despite the exemption from general fuel registration requirements 
    noted for these fuels in 40 CFR 79.4(a)(3).
    ---------------------------------------------------------------------------
    
        An automobile manufacturer recently suggested to EPA that certain 
    detergent additives used in the gasoline portion of E85 may contribute 
    to the formation of deposits in vehicle fuel pumps in E85 vehicles.\14\ 
    EPA requests comment on the potential incompatibility of certain 
    detergent additives for use in the gasoline portion of E85, and on the 
    regulatory measures which EPA could take to address such a problem if 
    it exists. Comment is also requested on the extent to which such 
    concerns might also apply to M85 fuel.
    ---------------------------------------------------------------------------
    
        \14\Memorandum entitled: ``Phone Call with Gerald Barnes of 
    General Motors Regarding the Potential Incompatibility of Certain 
    Detergent Additives for use in the Gasoline Portion of E85 fuel.'', 
    Docket Item IV-E-34
    ---------------------------------------------------------------------------
    
    D. Aftermarket Detergent Additives
    
        The proposed detergent certification program did not cover the use 
    of aftermarket detergent additives.\15\ EPA requests comment on whether 
    any requirements regarding the deposit control efficiency of 
    aftermarket additives should be implemented, and the authority under 
    which EPA could act to implement such requirements. Specifically, EPA 
    requests comment on what requirements might be necessary on aftermarket 
    additives to limit their potential contribution to the formation of 
    CCD. This is of particular concern since EPA believes that the 
    manufacturers of such aftermarket additives advise their use at very 
    high concentrations to remedy PFID/IVD related problems. As discussed 
    earlier, potential interim CCD control options involve limiting the 
    concentrations used of detergents which have a tendency to form CCD.
    ---------------------------------------------------------------------------
    
        \15\Aftermarket detergent additives are marketed directly to 
    gasoline consumers for addition directly into the vehicle fuel tank.
    ---------------------------------------------------------------------------
    
    E. Detergent Additives Certified for Use in California Phase-2 
    Reformulated Gasoline
    
        The interim detergent registration rule specified that data used to 
    support the certification of detergent additives under California's 
    detergent additive program, specifically for use in California Phase-2 
    Reformulated Gasoline, will be acceptable for use in demonstrating the 
    performance of detergents used to comply with Federal detergent 
    gasoline requirements only for gasoline sold within the state of 
    California. During a workshop on the interim requirements for deposit 
    control additives, held by the American Petroleum Institute (API) on 
    October 26, 1994, commenters from the audience suggested that EPA 
    should allow California Phase-2 reformulated gasoline that is additized 
    with detergents certified under California's detergent additive program 
    to be sold outside of California. EPA agrees that this approach is in 
    keeping with the goals of this program. The addition of such a 
    provision would also allow improved flexibility in the gasoline 
    distribution system.
        Therefore, EPA proposes to amend the provisions of the interim 
    detergent rule to provide that gasoline additized within the state of 
    California in accordance with the requirements of the California Air 
    Resource Board's (CARB's) detergent rule may also be sold outside of 
    the state of California. Specifically, EPA proposes to amend section 
    80.141(e)(1) of the regulatory text to state that, under the interim 
    program, CARB detergent certification data specific to California 
    phase-2 reformulated gasoline will be accepted as adequate support of 
    detergent effectiveness for detergent gasoline that is blended within 
    the state of California in accordance with CARB's detergent program.
    
    F. Allowed Variation in the Concentration of Detergent-Active 
    Components Within a Single Registration for a Detergent Additive 
    Package
    
        During the workshop on the interim requirements for deposit control 
    additives held by API, commenters from the audience requested 
    clarification of the allowed variation in the concentration of 
    detergent-active components in a detergent additive package under a 
    single additive registration. They stated that it is not possible to 
    comply with the requirements of section 80.141(c)(2), which state that 
    no variation is allowed in the concentration of any of the detergent-
    active components under a single variation, given variability in 
    manufacturing process. They further stated that upward variation in the 
    concentration of these components should be allowed, since such 
    variation would not compromise the additive's deposit control 
    efficiency. Indeed, as suggested by these commenters, EPA intended the 
    language of section 80.141(c)(2) to prevent downward variation in the 
    concentrations of the detergent-active components from the minimum 
    concentrations reported in the subject additive registration. It was 
    not intended to prevent an upward variation in the concentration of 
    these components. Therefore, to clarify this provision, EPA proposes to 
    amend section 80.141(c)(2) to state that upward variation in the 
    concentration of detergent active components would be permitted, 
    provided that such variation is specified in the registration, and that 
    such variability does not change the minimum recommended concentration 
    reported to be necessary to control deposits.
    
    G. Enforcement Issues
    
        EPA has several enforcement issues for which comments are requested 
    prior to the issuance of the certification final rule. EPA believes 
    these issues are integral to successful enforcement of the detergent 
    program, and will be addressing these issues in the certification final 
    rule.
    1. Meters
        a. Required Use of Meters on Automated Additization Systems.
        In the NPRM, the proposed mass balance (now volumetric additive 
    reconciliation, or ``VAR'') formulas provided for three different 
    additization systems: hand blending, meters on every injector, and a 
    metering system that did not have meters on every injector. EPA 
    requested comments on whether the certification rule should require, 
    for the purpose of measurement accuracy, that automated additization 
    equipment be equipped with meters on every injector.
        EPA received no comments specifically addressing this issue. 
    However, API commented that the final automated VAR formulas should be 
    flexible enough to permit the use of presently existing automated 
    additization equipment, which includes meters on every injector, 
    metered systems without meters on every injector, and automated systems 
    without any meters that measure detergent use through tank inventory 
    gauging.
        The VAR formula in the interim program final rule does not require 
    automated detergent blenders to have metered measurement systems, in 
    deference to lead time concerns. However, as was proposed in the NPRM, 
    EPA does intend to require some form of metered measurements for 
    automated detergent blenders in the certification program final rule. 
    EPA is still interested in receiving comments about the value of 
    requiring systems with meters on every injector, as opposed to 
    permitting the use of metered systems that measure the flow from many 
    injectors on one meter.
        A metered measurement system will be required in the certification 
    program final rule because meters are unquestionably a more accurate 
    measurement system than tank inventory gauging. Meters measure the 
    actual flow of product going through them, while inventory gauges 
    merely determine drop in tank volume. As API commented in its analysis 
    of automated additization system errors, inventory measurement systems 
    are subject to error both in measuring inventory as well as in 
    measuring additions to inventory. API's own member survey, submitted to 
    EPA as comment, suggested that metered systems would need a smaller 
    accuracy tolerance range than inventory systems, i.e., an 8 to 10 
    percent tolerance based on metered system errors, as opposed to the 
    greater 10 to 15 percent tolerance range based on inventory system 
    errors. (Parenthetically, an enforcement tolerance was not provided in 
    the interim program final rule and is not anticipated in the 
    certification program final rule. This issue was addressed at length in 
    the preamble to the interim program final rule.)
        The final detergent certification program rule, expected to be 
    effective in mid-1996, will not have the lead time issues associated 
    with implementation of the interim program. EPA therefore reconfirms 
    its proposal that, under the final certification program, all automated 
    detergent blenders using the automated formula be required to have 
    metered measurements. Furthermore, to assure accuracy of the VAR 
    measurements, EPA proposes that all metered systems must include meters 
    on every injector. This more stringent proposal recognizes that not all 
    metered systems can accurately establish whether gasoline is being 
    appropriately additized. If the system merely has a master meter which 
    measures, in the aggregate, the flow of detergent from the tank into a 
    multitude of injectors, it is not possible to determine whether any 
    particular injector is operating properly and dispensing the proper 
    amount of detergent. To ensure that each injector is dispensing the 
    appropriate detergent concentration, a meter would have to be installed 
    on each injector.
        Obviously, EPA wants to fulfill its statutory mandate of ensuring 
    the proper additization of gasoline to prevent deposits, and believes 
    it is necessary to require all automated systems to be equipped with 
    meters on every injector. However, the Agency is also concerned about 
    the costs of such a requirement, and is therefore very interested in 
    receiving comments about the number of automated blenders that would 
    need to upgrade under such a requirement, the cost that would accrue to 
    such blenders, as well as the aggregate cost. The Agency would then be 
    interested in comparing these costs with the value received in 
    additional additization accuracy expected to result from this 
    requirement.
        b. Precision of Metered Measurements. The NPRM proposed that VAR 
    detergent measurements for automated blenders be determined and 
    recorded to one tenth of a gallon. API commented that detergent volume 
    measurement should only be required to be recorded at the gallon level, 
    since scaling back the determination to precision of a gallon would be 
    necessary to accommodate all present additization systems. In deference 
    to the concern that some parties would be unable to upgrade to systems 
    with precision to at least one tenth of a gallon in time for the 
    January 1, l995 implementation date of the interim program rule, the 
    interim program requires VAR detergent measurements to be recorded only 
    to the nearest gallon.
        EPA is now proposing that, under the certification program final 
    rule, the VAR detergent measurements for automated blenders must be 
    recorded to a precision of at least one tenth of a gallon. This 
    provision is consistent with the proposal that all automated blenders 
    using the automated VAR formula must be equipped with metered detergent 
    measurement equipment. It is EPA's understanding that metered equipment 
    is easily able to measure to the one tenth of a gallon precision 
    standard, and it should not be difficult for regulated parties to meet 
    this higher level of precision once the provisions of the certification 
    program go into effect. Comments are requested about the measurement 
    capabilities of metered measurement equipment and about the 
    reasonableness of requiring recording accuracy to one tenth of a 
    gallon.
    2. The Use of a Per-Gallon Minimum Detergent Requirement within VAR 
    Compliance Periods for Automated Detergent Blenders
        In the NPRM, EPA proposed that all detergent blenders conduct 
    regular product reconciliations to determine the accuracy of their 
    additizations. Hand blenders were proposed to perform this 
    reconciliation on a per-batch basis, whereas automated blenders, not 
    having the uniform capability to easily determine per-batch usage, were 
    proposed to perform the reconciliations on a weekly basis.\16\ The 
    detergent reconciliation proposed for automated blenders was, in 
    effect, an averaging procedure, permitting automated blenders to 
    calculate the accuracy of their additization throughout the compliance 
    period on an averaged basis.
    ---------------------------------------------------------------------------
    
        \16\In fact, pursuant to comments, the interim program requires 
    only a monthly reconciliation period for automated blenders.
    ---------------------------------------------------------------------------
    
        To limit the ability to average detergent usage, EPA also proposed 
    in the NPRM that any intentional alteration of the detergent 
    concentration within the compliance period would terminate the period 
    and necessitate the start of a new period. Under this proposal, 
    intentional compensation for under-additization discovered in the 
    period would not be permitted. However, in its comments, API expressed 
    concern that, without a significant enforcement tolerance to determine 
    compliance with the VAR standard over the entire period, automated 
    detergent blenders in some circumstances would be required to make 
    concentration adjustments in order to stay in compliance. As explained 
    in detail in the interim program final rule, EPA did not believe it was 
    appropriate to create a VAR standard enforcement tolerance, but did 
    decide to permit limited intentional compensation within the compliance 
    period for discovered under-additizations. The permissible adjustment 
    was limited to 10 percent above the concentration initially used in the 
    period. The purpose of this limitation was to prevent blenders from 
    attempting to compensate for substantial under-additizations (and thus 
    avoid liability for such under-additizations) by means of intentionally 
    over-additizing, to a significant degree, for the rest of the period.
        However, the Agency still has concerns that permitting averaging 
    over the automated blender VAR compliance period will tolerate 
    unacceptable amounts of per-gallon under-additization of gasoline. 
    Depending on the amount of additized gasoline measured in the 
    compliance period, it is clear that even the 10 percent adjustment 
    limitation could permit some quantity of gasoline being non-additized 
    or significantly under-additized. Even if serious under-additization 
    occurred early in the period, the averaged compliance standard might 
    still be attained by the blender through the permissible upward 
    adjustment of the detergent concentration rate for the rest of the 
    period.
        Naturally, EPA would like to ensure that all gasoline is additized 
    at an effective detergent concentration rate, as established during 
    certification testing. The VAR compliance procedures included in the 
    interim program go a considerable way toward accomplishing this goal, 
    but only on an average for the compliance period. Individual loads of 
    gasoline may still be severely out of specification. Consequently, for 
    the final certification program rule, EPA is proposing that, within the 
    monthly compliance period for automated blenders, each load of the 
    product must be additized at a rate that is at least 90 percent of the 
    certified detergent treat rate. This 90 percent figure would allow for 
    some lapse in equipment efficiency while providing assurance that each 
    load in the averaging period will approximate the certification 
    standard. The reasonableness of the proposed 90 percent minimum 
    requirement is supported by on an API member survey which was submitted 
    as a comment to EPA. This survey indicated that many blenders (73 per 
    cent of proprietary systems, and 37 percent of non-proprietary systems) 
    can apparently attain a monthly blending accuracy to within 10 per cent 
    of the goal.
        The minimum per-gallon requirement within the averaged VAR 
    compliance standard would not only provide greater assurance of across-
    the-period accurate additization, but would also provide EPA with a 
    useful enforcement tool. With this per-gallon minimum, EPA would be 
    able to sample and test additized gasoline for detergent program 
    compliance at the facilities of any regulated party. Under the interim 
    program, on the contrary, the testing of additized product may reveal 
    complete non-additization without necessarily establishing a violation, 
    since there is no minimum per-gallon requirement under the interim 
    period's VAR procedures. Although extensive sampling and testing of 
    additized product is not presently contemplated, the ability to conduct 
    such testing on a case-specific basis and to establish violations based 
    on such testing would be very useful.
        EPA is requesting comments on the proposed per-gallon minimum 
    requirement within the VAR compliance procedures. The Agency is 
    particularly interested in learning whether the 90 percent minimum 
    requirement is considered attainable, what problems would be associated 
    with this minimum requirement, what records would be useful in 
    monitoring compliance with the requirement, and what the costs would be 
    in attaining compliance with a minimum standard. Comment is also 
    requested on an alternate per-gallon minimum requirement, with 
    rationale to support its adoption instead of a 90 percent minimum 
    requirement. If commenters believe the per-gallon minimum concept is 
    not appropriate, EPA requests suggestions for alternative means to 
    assure greater additization accuracy throughout the VAR compliance 
    period. One such alternative option being contemplated by the Agency is 
    the previously proposed weekly compliance period, which would obviously 
    permit less extensive averaging than the longer, monthly period.
    3. Presumptive Liability for VAR Violations
        Under the interim program final rule, only detergent blenders will 
    be held liable for VAR violations. However, EPA stated in the preamble 
    to interim program rule that this issue may be revisited in the 
    detergent certification final rule. Although some commenters asserted 
    that detergent blenders should be the only parties liable for VAR 
    violations, EPA believes that parties other than, or in addition to 
    detergent blenders, could cause VAR violations. Therefore, limiting 
    liability for VAR violations to detergent blenders may allow culpable 
    parties to evade liability for VAR violations that they have caused.
        For example, a party may cause VAR violations by providing 
    inaccurate or incomplete blending instructions to detergent blenders, 
    or by conspiring with detergent blenders to sell under-additized 
    gasoline that violates VAR requirements. The latter scenario could come 
    about if a retailer attempted to save money by intentionally purchasing 
    cheaper, unadditized or under-additized gasoline from a terminal which 
    was intentionally violating VAR requirements to produce such gasoline. 
    In this scenario, the collusion would occur because the retailer would 
    benefit from the lower cost of its purchased gasoline, and the terminal 
    would benefit from the sale of the misadditized product to the 
    retailer.
        Further, the newly proposed per-gallon minimum requirement within 
    the VAR procedures would make it possible for EPA to effectively 
    discover VAR per-gallon minimum violations downstream, at retail 
    outlets or at other regulated parties receiving product from the 
    detergent blenders. When such violations are found, EPA needs the 
    ability to hold these parties liable for such VAR violations. As shown 
    in the preceding paragraph, it clearly could be in the financial 
    interest of these parties to cause VAR violations by colluding with 
    detergent blenders to sell VAR violating, less expensive gasoline.
        EPA believes that parties who cause VAR violations should not 
    escape liability for those violations. Therefore, EPA is considering as 
    an option under the detergent certification final rule, that all 
    parties in the misadditized product's distribution system, including 
    detergent blenders but excepting upstream carriers, will be 
    presumptively liable for such VAR violations. As is typically the case, 
    carriers upstream to where a violation is found will be liable for such 
    violations if EPA can establish that they caused the violation.
        The rationale for imposing a presumptive liability scheme for VAR 
    violations would be the same as that which supports presumptive 
    liability for other violations in the detergent program, and for 
    violations of other EPA fuels programs such as reformulated gasoline, 
    gasoline volatility, and lead contamination. Typically, many parties 
    handle and control gasoline, detergent and detergent-additized post-
    refinery component, which are, often times, fungible products. Under 
    these circumstances, it will be difficult for EPA to determine who, in 
    addition to the detergent blender, might have caused the VAR 
    violations. When multiple parties potentially may have caused a 
    violation, the Agency needs a presumptive liability scheme to 
    effectively enforce its regulatory program.
        All presumptively liable parties would have the right to establish 
    an affirmative defence to such liability. EPA expects that the vast 
    majority of VAR violations will be caused by detergent blenders, and in 
    these cases, the blenders will be the only parties liable.
        EPA requests comments on the issue of presumptive liability for VAR 
    violations, including comments regarding EPA's legal authority to 
    impose such liability. Parties disagreeing with EPA's proposed approach 
    are urged to submit alternative options to address the problem of 
    multiple party causation of VAR violations. One alternative approach 
    that EPA is considering, and is requesting comment on, is the 
    imposition of an affirmative duty (with attendant penalties) on 
    upstream parties transferring title to detergent or custody to those 
    who will physically do the blending, to transfer accurate written 
    blending instructions for use of that detergent. In addition, a new 
    liability section would be created which would hold any regulated party 
    liable for a VAR violation if EPA could establish that the party caused 
    the violation.
    4. Right of Entry to Inspect the Premises of Regulated Parties in the 
    Detergent Distribution System
        Current regulations permit EPA to enter the premises of gasoline 
    refiners, retailers, wholesale purchaser-consumers, distributors, and 
    importers, and to make inspections, take samples, and conduct tests at 
    such facilities to determine compliance with EPA requirements. See 40 
    C.F.R. 80.4. EPA is today proposing to amend this provision to include 
    manufacturers, distributors, and carriers of detergent additives.
        To investigate possible violations of detergent specifications 
    promulgated under Sections 211(l) and 211(c), and to ensure compliance 
    with those specifications, it is necessary for EPA to have the ability 
    to collect samples of detergent additives at the facilities of the 
    detergent manufacturer, distributor, and carrier. Section 211(l) 
    directs EPA to establish, by regulation, specifications for detergent 
    additives that must be used to prevent the accumulation of engine or 
    fuel system deposits. EPA must be able to sample the detergent additive 
    before it is blended into gasoline to ensure that manufacturers produce 
    detergents that comply with EPA regulations, and to ensure that 
    distributors and carriers of detergents do not take actions that alter 
    detergents in such a way that the requirements are not met. Further, 
    this approach is consistent with the currently existing provision in 
    Part 80 under which EPA may enter the facilities of gasoline refiners 
    and other parties, and make inspections, take samples, and conduct 
    tests at such facilities to determine compliance with the requirements 
    of that part.
        Therefore, under EPA's broad authority under Section 301(a) to 
    promulgate such regulations as are necessary to carry out the Agency's 
    functions under the Act, and EPA's authority under Sections 114, 
    211(c), and 211(l), EPA is proposing to amend the currently existing 
    right of entry provision in 40 C.F.R. 80.4 to include detergent 
    manufacturers, distributors, and carriers. Also, see Dow Chemical Co. 
    v. United States, 476 U.S. 227 (1986), recognizing EPA's broad 
    authority to use reasonable means to carry out its investigatory 
    function under the Act, including but not limited to Section 114. EPA 
    invites comment on this proposed amendment.
    5. The Use of Multiple Detergent Concentrations by Automated Detergent 
    Blenders
        Under the proposed regulatory approach published in the NPRM, 
    automated detergent blenders were not permitted to include several 
    detergent concentrations in one VAR compliance record. Any change in 
    concentration under the NPRM would have necessitated the start of a new 
    VAR period. The purpose of this limitation was to prevent the attempt 
    by blenders to compensate for significant under-additization within a 
    compliance period by changing the rate of additization in the rest of 
    the period.
        The Agency received a comment protesting this prohibition against 
    the use of several detergent set rates in one VAR record. The commenter 
    argued that this restriction would penalize blenders with sophisticated 
    equipment that could automatically change set rates depending on the 
    product being additized. According to this commenter, such a blender 
    would be required to create a new VAR record every time his equipment 
    automatically switched concentration rates to accommodate different 
    grades of product being additized.
        EPA does not intend to discourage the use of sophisticated 
    additization equipment by detergent blenders. Therefore, under the 
    interim program EPA did not prohibit the use of several set rates on a 
    single VAR record. However, blenders are required to meet the following 
    conditions under the interim program to ensure additization accuracy: 
    no concentration set rate can be set below the detergent's lowest 
    additive concentration (LAC); each initial set rate used in the period 
    must be recorded on the VAR record, along with the product to be 
    additized with each rate; no adjustments to the initially set rates can 
    be made in the period above 10 percent of the initial rate; the blender 
    must maintain records of all adjustments to the set rates.
        These requirements protect additization accuracy, while at the same 
    time, provide industry with the flexibility to use sophisticated 
    additization equipment capable of automatically varying set rates. The 
    Agency continues to believe that these VAR requirements are useful. 
    However, further restrictions are necessary to ensure additization 
    accuracy under the detergent certification final rule.
        Under the interim program, automated blenders can measure on a 
    single VAR record product being additized by the same detergent under 
    different set rates, as long as they meet the conditions stated above. 
    Since VAR compliance under the interim program is an averaged 
    compliance, there is no way to determine under this procedure if the 
    product being additized at the lower rate is actually meeting its LAC 
    requirements, because the product being additized at the higher rates 
    would conceal any failure of the lower product to meet the averaged 
    standard. This procedure of multi-rate averaging is thus not conducive 
    to assuring the additization of all product.
        Consequently, EPA is proposing that, under the detergent 
    certification final rule, automated blenders may continue to blend 
    their detergent at multiple rates in one VAR period, but product being 
    blended at each set rate must have its own VAR record. This would 
    ensure that product additized at each rate meets the LAC standard. 
    Further, the Agency is also proposing that a blender choosing to use 
    different set rates within a single VAR period must have equipment that 
    can accurately measure detergent use at each set rate, (e.g. meters 
    which can switch to measuring different rates, meters on individual 
    injectors measuring different rates, or other effective systems). This 
    latter requirement will ensure that the accuracy of each set rate's 
    additization can be effectively measured, not merely estimated or 
    assumed.
        Comments are requested about these proposed changes to automated 
    blender VAR requirements. Specifically requested is information about 
    the cost associated with implementation of these changes, such as the 
    number of blenders they would impact, the number of blenders that would 
    be forced to upgrade their equipment to accommodate these changes, and 
    the cost of such upgrades. If commenters are opposed to the 
    implementation of these changes, they are urged to submit alternative 
    plans to address the problem of ensuring proper additization of product 
    additized at lower concentrations when multiple concentrations are 
    being measured.
    6. Regulation of Imported Additized Gasoline
        Under the NPRM, importers of gasoline are regulated parties, 
    subject to the requirements of the detergent rule. They are thus 
    subject to product transfer document requirements and the prohibitions 
    against the transfer and sale of nonconforming product. They are 
    permitted to import either additized or nonadditized product. If they 
    additize the gasoline they import, they are considered detergent 
    blenders, and are subject to VAR requirements for the gasoline. If they 
    import additized gasoline but are not detergent blenders, they are not 
    required to create and maintain VAR records establishing VAR 
    compliance. However, if the product they import is sampled and shown to 
    be under- additized, the importer would be presumptively liable for the 
    violation. As a practical matter, it would be extremely difficult for 
    the importer to effectively meet its affirmative defence requirements, 
    unless it would provide EPA with the VAR records documenting proper 
    additization of the product.
        The Agency believes the control over imported gasoline needs to be 
    strengthened in regard to gasoline which is additized prior to 
    importation. As was extensively discussed in the NPRM, enforcement of 
    the detergent regulation will primarily be based on record review, 
    since sampling and testing of additized gasoline for compliance will be 
    difficult. Agency review of VAR records to determine accurate 
    additization is thus critical to the success of the program. It is just 
    as important for EPA to be able to review VAR records for imported 
    gasoline which is additized, as it is to review those records for 
    domestic product, given the sampling and testing limitation. Under the 
    interim program, however, Agency review of VAR records for imported 
    additized gasoline will be limited to those situations in which 
    violations have already been discovered through testing or otherwise. 
    This means that, in regard to imported gasoline, the Agency is deprived 
    of its prime measures to determine detergent program violations.
        To correct this deficiency, EPA is proposing that the detergent 
    certification final rule will amend the definition of detergent blender 
    to include importers of additized gasoline within the definition. If 
    importers choose to import additized product, they must be held 
    accountable for its additization accuracy as detergent blenders. If 
    not, those selling domestically additized gasoline will be at a 
    disadvantage to importers, since VAR records establishing violations 
    will not be generally available for EPA review. Including importers of 
    additized product within the definition of detergent blender will make 
    the importers responsible for the creation and maintenance of the VAR 
    records verifying additization accuracy, as well as with compliance 
    with the other VAR requirements that apply to domestically additized 
    product. EPA requests comments about the proposed amendment of the 
    definition of detergent blender.
    
    IV. Public Participation
    
        EPA has encouraged full participation of the regulated industry and 
    other interested parties in the development of the rule to implement 
    the statutory requirements and continues to do so. A public workshop 
    was held on February 13, 1992 to initiate open discussion of the 
    relevant issues and EPA met with numerous industry representatives 
    separately to obtain their input.
        The Notice of Proposed Rulemaking (NPRM) was published on December 
    6, 1993 (58 FR 64213) and a public hearing was held in Ann Arbor, 
    Michigan on January 11, 1994. Comments on the NPRM were accepted until 
    March 11, 1994. EPA received 31 written comments on the NPRM before the 
    close of the initial comment period and has received additional 
    comments since that time particularly with respect to the issues 
    discussed in this notice. EPA encourages additional comment on the 
    issues discussed in this notice through the close of the current 
    comment period. (For the date on which the comment period closes see 
    the Dates section in this notice.) EPA does not intend to hold an 
    additional public hearing to discuss the issues raised in this notice.
    
    V. Electronic Copies of Rulemaking Documents
    
        Electronic copies of this notice, and other documents associated 
    with the detergent certification rule are available on the Office of 
    Air Quality Planning and Standards (OAQPS) Technology Transfer Network 
    Bulletin Board System (TTNBBS). Instructions for accessing TTNBBS and 
    downloading the relevant files are described below.
        TTNBBS can be accessed using a dial-in telephone line (919- 541-
    5742) and a 1200, 2400, or 9600 bps modem (equipment up to 14.4 Kbps 
    can be accommodated). The parity of the modem should be set to N or 
    none, the data bits to 8, and the stop bits to 1. When first signing on 
    to the bulletin board, the user will be required to answer some basic 
    informational questions to register into the system. After registering, 
    proceed through the following options from a series of menus:
    
    (T) GATEWAY TO TTN TECHNICAL AREAS (Bulletin Board)
    (M) OMS
    (K) Rulemaking and Reporting
    (3) Fuels
    (4) Detergent Additives
    
        At this point, the system will list all available files in the 
    chosen category in chronological order with brief descriptions. The 
    following five ``.ZIP'' files are currently available:
    
    ``DCA__PRE.ZIP'' (Preamble from the Notice of Proposed Rulemaking)
    ``DCA__IFP.ZIP'' (Preamble to the final rule on the Interim 
    Requirements for Deposit Control Additives)
    ``DCA__IFR.ZIP'' (Regulatory text for the final rule on the Interim 
    Requirements for Deposit Control Additives)
    ``DCA__RIA.ZIP'' (Regulatory Impact Analysis)
    ``DCA__RCN.ZIP'' (Notice to Reopen the Comment Period)
    
        File information can be obtained from the ``READ.ME'' file. Choose 
    from the following options when prompted:
    
    ownload, 

    rotocol, xamine, ew, ist, elp or to exit. To download a file, e.g., filename.ZIP, the user needs to choose a file transfer protocol appropriate for the user's computer from the options listed on the terminal. The user's computer is then ready to receive the file by invoking the user's resident file transfer software. Programs and instructions for de-archiving compressed files can be found under ystems Utilities from the top menu, under rchivers/de-archivers. Please note that due to differences between the software used to develop the document and the software into which the document may be downloaded, changes in format, page length, etc. may occur. TTNBBS is available 24 hours a day, 7 days a week except Monday morning from 8-12 EST, when the system is down for maintenance and backup. For help in accessing the system, call the systems operator at 919-541-5384 in Research Triangle Park, North Carolina, during normal business hours EST. V. Statutory Authority The statutory authority for the regulation of gasoline detergent additives is granted to EPA by sections 211 (c) and (l) of the Clean Air Act, as amended, 42 U.S.C. 7414, 7545 (c) and (k), and 7601. List of Subjects in 40 CFR Part 80 Environmental protection. Fuel additives, Gasoline detergent additives, Gasoline motor vehicle pollution, Penalties, Reporting and recordkeeping requirements. Dated: December 19, 1994. Richard D. Wilson, Acting Assistant Administrator for Air and Radiation. [FR Doc. 94-31815 Filed 12-27-94; 8:45 am] BILLING CODE 6560-50-P

Document Information

Published:
12/28/1994
Entry Type:
Uncategorized Document
Action:
Proposed rule; reopening of comment period.
Document Number:
94-31815
Dates:
Written comments on the specific issues discussed in this document will be accepted until January 27, 1995. EPA is not soliciting new comments on aspects of the original proposed rule that are not
Pages:
0-0 (None pages)
Docket Numbers:
Federal Register: December 28, 1994, AMS-FRL-5128-9
Supporting Documents:
» Legacy Index for Docket A-91-77
» Regulation of Fuels and Fuel Additives: Minor Revisions; Direct Final Rule
» Regulation of Fuels and Fuel Additives: Certification Standards for Deposit Control Gasoline Additives
» Regulation of Fuels and Fuel Additives: Standards for Deposit Control Gasoline Additives; Reopening of Comment Period
» Regulation of Fuels and Fuel Additives: Standards for Deposit Control Gasoline Additives; Reopening of Comment Period
» Regulation of Fuels and Fuel Additives: Interim Requirements for Deposit Control Gasoline Additives
» Regulation of Fuels and Fuel Additives: Standards for Deposit Control Gasoline Additives
» Gasoline Detergent Additives Regulations; Notice of Public Workshop
CFR: (1)
40 CFR 60