96-21628. Hazardous Waste Combustors; Revised Standards; Proposed Rule Notice of Data Availability and Request for Comments  

  • [Federal Register Volume 61, Number 165 (Friday, August 23, 1996)]
    [Proposed Rules]
    [Pages 43501-43515]
    From the Federal Register Online via the Government Publishing Office [www.gpo.gov]
    [FR Doc No: 96-21628]
    
    
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    ENVIRONMENTAL PROTECTION AGENCY
    40 CFR Parts 60, 63, 260, 261, 264, 265, 266, 270 and 271
    
    [FRL-5558-5]
    RIN 2050-AF01
    
    
    Hazardous Waste Combustors; Revised Standards; Proposed Rule--
    Notice of Data Availability and Request for Comments
    
    AGENCY: Environmental Protection Agency (EPA).
    
    ACTION: Notice of data availability and request for comments.
    
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    SUMMARY: This document is a notice of availability and invitation for 
    comment on the following information pertaining to the proposed revised 
    standards for hazardous waste combustors (61 FR 17358 (April 19, 
    1996)): Reports from an independent peer review of technical aspects of 
    the rule; additional analyses of various fuel oils to be used to 
    establish a specification to exclude comparable fuels; and information 
    on a synthesis gas process and product gas specifications that was 
    inadvertently not included in the docket.
        Readers should note that only comments about new information 
    discussed in this document will be considered during the comment 
    period. Issues related to the April 19, 1996 proposed rule that are not 
    directly affected by the documents or data referenced in this Notice of 
    Data Availability are not open for further comment.
    
    DATES: Written comments on the peer review reports, the new comparable 
    fuels analyses, and the synthesis gas process and product information 
    must be submitted by September 23, 1996.
    
    ADDRESSES: Commenters must send an original and two copies of their 
    comments referencing Docket Number F-96-RCSP-FFFFF to: RCRA Docket 
    Information Center, Office of Solid Waste (5305G), U.S. Environmental 
    Protection Agency Headquarters (EPA, HQ), 401 M Street, S.W., 
    Washington, D.C. 20460. Comments may also be submitted electronically 
    through the Internet to: rcra-docket@epamail.epa.gov. Comments in 
    electronic format should also be identified by the docket number F-96-
    RCSP-FFFFF. All electronic comments must be submitted as an ASCII file 
    avoiding the use of special characters and any form of encryption. 
    Commenters should not submit electronically any confidential business 
    information (CBI). An original and two copies of the CBI must be 
    submitted under separate cover to: RCRA CBI Document Control Officer, 
    OSW (5305W), 401 M Street, SW, Washington D.C. 20460. For other 
    information regarding submitting comments electronically, viewing the 
    comments received, and supporting information, please refer to the 
    proposed rule (61 FR 17358 (April 19, 1996)). The RCRA Information 
    Center is located at Crystal Gateway One, 1235 Jefferson Davis Highway, 
    First Floor, Arlington, Virginia and is open for public inspection and 
    copying of supporting information for RCRA rules from 9:00
    
    [[Page 43502]]
    
    am to 4:00 pm Monday through Friday, except for Federal holidays. The 
    public must make an appointment to view docket materials by calling 
    (703) 603-9230. The public may copy a maximum of 100 pages from any 
    regulatory document at no cost. Additional copies cost $0.15 per page.
    
    FOR FURTHER INFORMATION CONTACT: For general information, call the RCRA 
    Hotline at 1-800-424-9346 or TDD 1-800-553-7672 (hearing impaired) 
    including directions on how to access electronically some of the 
    documents and data referred to in this notice via EPA's Cleanup 
    Information Bulletin Board System (CLU-IN). The CLU-IN modem access 
    phone number is 301-589-8366 or Telnet to clu-in.epa.gov for Internet 
    access. Callers within the Washington Metropolitan Area must dial 703-
    412-9810 or TDD 703-412-3323 (hearing impaired). The RCRA Hotline is 
    open Monday-Friday, 9:00 a.m. to 6:00 p.m., Eastern Standard Time. For 
    other information on this notice, contact Shiva Garg (5302W), Office of 
    Solid Waste, 401 M Street, S.W., Washington, DC 20460, phone (703) 308-
    8459, e-mail: garg.shiva@epamail.epa.gov.
    
    SUPPLEMENTARY INFORMATION: On April 19, 1996, EPA proposed revised 
    standards for hazardous waste combustors (i.e., incinerators and cement 
    and lightweight aggregate kilns that burn hazardous waste). See 61 FR 
    17358. The Agency originally established a 60-day comment period, but 
    later extended it to 120 days (61 FR 27038 (May 30, 1996)). The last 
    date for receipt of comments on the Federal Register notice of April 
    19, 1996 continues to remain August 19, 1996.
        The Agency is today providing notice and opportunity to comment on 
    the following additional information pertaining to the proposed rule: 
    (1) Reports from an independent peer review of technical aspects of the 
    rule; (2) additional analyses of various fuel oils to be used to 
    establish a specification to exclude comparable fuels; and (3) 
    information on a synthesis gas process and product gas specifications 
    that was inadvertently not included in the docket.
    
    Peer Review Reports
    
        As part of the rule development process, the Agency initiated a 
    peer review of the proposed rule, preamble and relevant supporting 
    background documents in three subject areas of the rule: engineering, 
    risk assessment and economic analysis. The review panel members were 
    tasked with conducting a comprehensive and critical review of the 
    proposed rule in their designated subject areas, addressing a set of 
    questions pertaining to the technical basis of the approaches adopted 
    by the Agency, and providing comments and/or recommendations where 
    warranted. Each subject area panel prepared a summary report 
    highlighting the key points of discussion, including the consensus 
    reports or the dissenting opinions. Copies of the peer review panel 
    report of each subject area and individual review comments of each 
    panel member are available in the docket.
    
    Comparable Fuel Specification
    
        As part of the proposed comparable fuel specification, EPA used a 
    benchmark approach to develop a series of technical specifications that 
    would allow hazardous waste similar in composition to a commercially 
    available fossil fuel to be excluded under RCRA when burned. One of 
    these specifications included the Agency's proposal to limit the 
    Appendix VIII, Part 261, constituents in comparable fuels 1 to 
    those found in the benchmark fossil fuel. As discussed in the preamble 
    of the proposal (61 FR 17461), EPA was unable to analyze for some 
    compounds on the Appendix VIII list because either an analytical method 
    was not available or could not be identified in time for initial 
    analysis. Those compounds were not listed in the proposed 
    specifications published on April 19, 1996.
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        \1\ The specification would also include two metals that are 
    identified in Clean Air Act section 112(b) as hazardous air 
    pollutants: cobalt and manganese. See 61 FR 17460.
    ---------------------------------------------------------------------------
    
        EPA has subsequently been able to identify methods for analyzing 
    some additional Appendix VIII compounds and is presenting a proposed 
    specification level or detection limit for these compounds. These 
    compounds are listed in today's notice and also can be found, along 
    with the analytical methods, in the Draft Technical Support Document 
    for HWC MACT Standards, Addendum to Volume VI: Development of 
    Comparable Fuels Specifications, August 1996. EPA invites comment on 
    today's new individual specifications, as well as the composite 
    specifications, and the analytical methods used in EPA's new analysis.
        In addition, we want to clarify the rationale for proposing 
    comparable fuel specification limits for total halogens and total 
    nitrogen. Although neither total halogens nor total nitrogen are listed 
    on Appendix VIII, Part 261 (or proposed for Appendix X), we believe 
    that they should be limited to ensure that halogenated and nitrated 
    products of incomplete combustion (PICs) from burning excluded waste 
    would not be emitted at higher levels than from burning benchmark 
    fossil fuel. Halogenated and nitrated organic compounds can pose a 
    particular hazard to human health and the environment.
    
    Synthesis Gas Comparable Fuel Exclusion
    
        In discussing the exclusion of synthesis gas (syngas) fuel in the 
    proposed rule, EPA referenced a Molten Metals Technology (MMT) letter 
    that presented data on the MMT syngas process, including relevant 
    specifications. See preamble discussion at 61 FR 17465. In placing the 
    MMT information in the docket, an attachment to the letter containing 
    the data was inadvertently not placed in the docket until late in the 
    comment period. EPA has since received a request to extend the comment 
    period pertaining only to the syngas exclusion to allow adequate time 
    to review this attachment and provide comment on the syngas exclusion. 
    In response to this request, EPA is granting 30 days from the 
    publication date of this notice to comment on the proposed syngas fuel 
    exclusion.
    
    Appendix--Comparable Fuel Constituent and Physical Specifications
    
        Note 1: All numbers in the tables of this appendix are expressed 
    to two significant figures.
    
     Table 1.--Detection and Detection Limit Values for a Possible Gasoline 
                                  Specification                             
    ------------------------------------------------------------------------
                                                                   Maximum  
                                          Concentration limit     detection 
               Chemical name             (mg/kg at 10,000 Btu/   limit (mg/ 
                                                  lb)                kg)    
    ------------------------------------------------------------------------
    1,1,1-Trichloroethane..............  Non-detect...........         34   
    
    [[Page 43503]]
    
                                                                            
    1,1,2-Trichloro-1,2,2-               Non-detect...........         30   
     trifluoroethane.                                                       
    1,1-Dichloro-1-propene.............  Non-detect...........         30   
    1,1-Dichloroethane.................  Non-detect...........         34   
    1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........          8.8 
     dioxin.                                                                
    1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........          8.8 
     furan.                                                                 
    1,2,3,4-Tetrachlorobenzene.........  Non-detect...........         14   
    1,2,3,5-Tetrachlorobenzene.........  Non-detect...........         14   
    1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........          8.8 
     dioxin.                                                                
    1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........          8.8 
     furan.                                                                 
    1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........          8.8 
     dioxin.                                                                
    1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........          8.8 
     furan.                                                                 
    1,2,3-Trichlorobenzene.............  Non-detect...........         14   
    1,2-Dichloroethane.................  Non-detect...........         34   
    1,2-Dichloropropane................  Non-detect...........         34   
    1,3-Dichloro-2-propanol............  Non-detect...........         30   
    1,3-Dichloropropane................  Non-detect...........         30   
    1,3-Propane sultone................  Non-detect...........         14   
    1-Chloronaphthalene................  Non-detect...........         14   
    2,2-Dichloropropane................  Non-detect...........         30   
    2,3,4,5-Tetrachlorophenol..........  Non-detect...........         14   
    2,3,4-Trichlorophenol..............  Non-detect...........         14   
    2,3,5-Trichlorophenol..............  Non-detect...........         14   
    2,3,6-Trichlorophenol..............  Non-detect...........         14   
    2,3,7,8-Tetrachlorodibenzo-p-dioxin  Non-detect...........          3.5 
    2,3,7,8-Tetrachlorodibenzo-p-furan.  Non-detect...........          3.5 
    2,3-Dichloro-1-propene.............  Non-detect...........         30   
    2,3-Dichlorophenol.................  Non-detect...........         14   
    2,4-D..............................  Non-detect...........          7.0 
    2,5-Dichlorophenol.................  Non-detect...........         14   
    2-Fluoroacetamide..................  Non-detect...........         14   
    2-Methylnaphthalene................  1200.................  ............
    2-Nitropropane.....................  Non-detect...........         30   
    3,3'-Dimethoxybenzidine............  Non-detect...........         14   
    3,4-Dichlorophenol.................  Non-detect...........         14   
    3,5-Dichlorophenol.................  Non-detect...........         14   
    3-/4-Chlorophenol..................  Non-detect...........         14   
    3-Nitroaniline.....................  Non-detect...........        670   
    4,4'-methylene-bis(2-chloroaniline)  Non-detect...........         14   
    4-Aminopyrridine...................  Non-detect...........         14   
    4-Chlorophenyl phenyl ether........  Non-detect...........        670   
    6-Propyl-2-thiouracil..............  Non-detect...........         14   
    Acenaphthene.......................  Non-detect...........        670   
    Acetone cyanohydrin................  Non-detect...........         14   
    Allyl alcohol......................  Non-detect...........         30   
    Ammonium vanadate..................  Non-detect...........         32   
    Anthracene.........................  Non-detect...........        670   
    Arochlor-1016......................  Non-detect...........          1.4 
    Arochlor-1221......................  Non-detect...........          1.4 
    Arochlor-1232......................  Non-detect...........          1.4 
    Arochlor-1242......................  Non-detect...........          1.4 
    Arochlor-1248......................  Non-detect...........          1.4 
    Arochlor-1254......................  Non-detect...........          1.4 
    Arochlor-1260......................  Non-detect...........          1.4 
    Arsenic acid.......................  Non-detect...........          0.27
    Arsenic pentoxide..................  Non-detect...........          0.22
    Arsenic trioxide...................  Non-detect...........          0.19
    Barium Cyanide.....................  Non-detect...........          3.7 
    Benzal chloride....................  Non-detect...........         14   
    Benzenethiol.......................  Non-detect...........         30   
    Benzyl chloride....................  Non-detect...........         14   
    Bis(2-chloroethoxy)methane.........  Non-detect...........        670   
    Bis(2-chloroethyl)ether............  Non-detect...........        670   
    Bis(2-ethylhexyl)phthalate.........  Non-detect...........        670   
    Bromide............................  Non-detect...........          5.0 
    Bromodichloromethane...............  Non-detect...........         34   
    Calcium Cyanide....................  Non-detect...........          1.8 
    Calcium chromate...................  Non-detect...........          4.2 
    Chlordane..........................  Non-detect...........         14   
    Chloride...........................  6.2..................  ............
    
    [[Page 43504]]
    
                                                                            
    Chloroethane.......................  Non-detect...........         34   
    Copper Cyanide.....................  Non-detect...........          1.7 
    Cyanide............................  Non-detect...........          1.0 
    Cyanogen Bromide...................  Non-detect...........          6.6 
    Cyanogen Chloride..................  Non-detect...........        100   
    Di-selenium-tetra-sulfide..........  Non-detect...........        830   
    Dibenzofuran.......................  Non-detect...........        670   
    Dibromochloromethane...............  Non-detect...........         34   
    Endosulfan I.......................  Non-detect...........          1.4 
    Endosulfan II......................  Non-detect...........          1.4 
    Endothal...........................  Non-detect...........         14   
    Endrin.............................  Non-detect...........          1.4 
    Endrin aldehyde....................  Non-detect...........          1.4 
    Endrin ketone......................  Non-detect...........          1.4 
    Epichlorohydrin....................  Non-detect...........         30   
    Ethyl carbamate....................  Non-detect...........         14   
    Ethylene glycol monoethyl ether....  Non-detect...........         14   
    Ethylenethiourea (2-                 Non-detect...........         14   
     Imidazolidinethione).                                                  
    Fluoride...........................  Non-detect...........          3.0 
    Heptachlor.........................  Non-detect...........          1.4 
    Heptachlor epoxide.................  Non-detect...........          2.8 
    Lead acetate.......................  Non-detect...........         13   
    Lead phosphate.....................  Non-detect...........          9.2 
    MNNG (N-Methyl-N-nitroso-N'-         Non-detect...........         14   
     nitroguanidine).                                                       
    Methomyl...........................  Non-detect...........          7.0 
    N-Nitrosodiphenylamine.............  Non-detect...........        670   
    Nickel Cyanide.....................  Non-detect...........          3.5 
    Nickel carbonyl....................  Non-detect...........          8.2 
    Nicotine...........................  Non-detect...........         14   
    Octachlorodibenzodioxin............  Non-detect...........         18   
    Octachlorodibenzofuran.............  Non-detect...........         18   
    Osmium tetraoxide..................  Non-detect...........         41   
    Phenanthrene.......................  Non-detect...........        670   
    Phenylthiourea.....................  Non-detect...........          7.0 
    Potassium Cyanide..................  Non-detect...........          2.5 
    Potassium Silver Cyanide...........  Non-detect...........          2.9 
    Propargyl alcohol..................  Non-detect...........         30   
    Pyrene.............................  Non-detect...........        670   
    Selenium dioxide...................  Non-detect...........          0.20
    Selenium sulfide...................  Non-detect...........          0.31
    Silver Cyanide.....................  Non-detect...........          2.6 
    Silvex.............................  Non-detect...........          7.0 
    Strychnine.........................  Non-detect...........         14   
    Tetra-selenium-tetra-sulfide.......  Non-detect...........       1600   
    Tetraethyl lead....................  Non-detect...........         11   
    Thallium acetate...................  Non-detect...........         18   
    Thallium carbonate.................  Non-detect...........         16   
    Thallium chloride..................  Non-detect...........         17   
    Thallium nitrate...................  Non-detect...........         18   
    Thallium oxide.....................  Non-detect...........         15   
    Thallium sulfate...................  Non-detect...........         17   
    Thioacetamide......................  Non-detect...........          7.0 
    Thiofanox..........................  Non-detect...........         14   
    Thiourea...........................  Non-detect...........          7.0 
    Toluene-2,4-diamine................  Non-detect...........          7.0 
    Toluene-2,6-diamine................  Non-detect...........          7.0 
    Vanadium pentoxide.................  Non-detect...........         18   
    Zinc Cyanide.......................  Non-detect...........          2.3 
    Zinc phosphide.....................  Non-detect...........          0.37
    alpha-BHC..........................  Non-detect...........          1.4 
    beta-BHC...........................  Non-detect...........          1.4 
    delta-BHC..........................  Non-detect...........          1.4 
    gamma-BHC (Lindane)................  Non-detect...........          1.4 
    m-Dinitrobenzene...................  Non-detect...........        670   
    p-Toluidine........................  Non-detect...........         14   
    trans-1,3-Dichloropropene..........  Non-detect...........         34   
    ------------------------------------------------------------------------
    
    
    
    [[Page 43505]]
    
    
    
     Table 2.--Detection and Detection Limit Values for a Possible Number 2 
                             Fuel Oil Specification                         
    ------------------------------------------------------------------------
                                                                   Maximum  
                                          Concentration limit     detection 
               Chemical name             (mg/kg at 10,000 Btu/   limit (mg/ 
                                                  lb)                kg)    
    ------------------------------------------------------------------------
    1,1,1-Trichloroethane..............  Non-detect...........         34   
    1,1,2-Trichloro-1,2,2-               Non-detect...........         30   
     trifluoroethane.                                                       
    1,1-Dichloro-1-propene.............  Non-detect...........         30   
    1,1-Dichloroethane.................  Non-detect...........         34   
    1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........         75   
     dioxin.                                                                
    1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........         75   
     furan.                                                                 
    1,2,3,4-Tetrachlorobenzene.........  Non-detect...........        100   
    1,2,3,5-Tetrachlorobenzene.........  Non-detect...........        100   
    1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........         75   
     dioxin.                                                                
    1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........         75   
     furan.                                                                 
    1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........         75   
     dioxin.                                                                
    1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........         75   
     furan.                                                                 
    1,2,3-Trichlorobenzene.............  Non-detect...........        100   
    1,2-Dichloroethane.................  Non-detect...........         34   
    1,2-Dichloropropane................  Non-detect...........         34   
    1,3-Dichloro-2-propanol............  Non-detect...........         30   
    1,3-Dichloropropane................  Non-detect...........         30   
    1,3-Propane sultone................  Non-detect...........        100   
    1-Chloronaphthalene................  Non-detect...........        100   
    2,2-Dichloropropane................  Non-detect...........         30   
    2,3,4,5-Tetrachlorophenol..........  Non-detect...........        100   
    2,3,4-Trichlorophenol..............  Non-detect...........        100   
    2,3,5-Trichlorophenol..............  Non-detect...........        100   
    2,3,6-Trichlorophenol..............  Non-detect...........        100   
    2,3,7,8-Tetrachlorodibenzo-p-dioxin  Non-detect...........         30   
    2,3,7,8-Tetrachlorodibenzo-p-furan.  Non-detect...........         30   
    2,3-Dichloro-1-propene.............  Non-detect...........         30   
    2,3-Dichlorophenol.................  Non-detect...........        100   
    2,4-D..............................  Non-detect...........          6.0 
    2,5-Dichlorophenol.................  Non-detect...........        100   
    2-Fluoroacetamide..................  Non-detect...........        100   
    2-Methylnaphthalene................  3400.................  ............
    2-Nitropropane.....................  Non-detect...........         30   
    3,3'-Dimethoxybenzidine............  Non-detect...........        100   
    3,4-Dichlorophenol.................  Non-detect...........        100   
    3,5-Dichlorophenol.................  Non-detect...........        100   
    3-/4-Chlorophenol..................  Non-detect...........        100   
    3-Nitroaniline.....................  Non-detect...........       1200   
    4,4'-methylene-bis(2-chloroaniline)  Non-detect...........        100   
    4-Aminopyrridine...................  Non-detect...........        100   
    4-Chlorophenyl phenyl ether........  Non-detect...........       1200   
    6-Propyl-2-thiouracil..............  Non-detect...........        100   
    Acenaphthene.......................  Non-detect...........       1200   
    Acetone cyanohydrin................  Non-detect...........        100   
    Allyl alcohol......................  Non-detect...........         30   
    Ammonium vanadate..................  Non-detect...........         28   
    Anthracene.........................  Non-detect...........       1200   
    Arochlor-1016......................  Non-detect...........          1.2 
    Arochlor-1221......................  Non-detect...........          1.2 
    Arochlor-1232......................  Non-detect...........          1.2 
    Arochlor-1242......................  Non-detect...........          1.2 
    Arochlor-1248......................  Non-detect...........          1.2 
    Arochlor-1254......................  Non-detect...........          1.2 
    Arochlor-1260......................  Non-detect...........          1.2 
    Arsenic acid.......................  Non-detect...........          0.23
    Arsenic pentoxide..................  Non-detect...........          0.18
    Arsenic trioxide...................  Non-detect...........          0.16
    Barium Cyanide.....................  Non-detect...........          3.7 
    Benzal chloride....................  Non-detect...........        100   
    Benzenethiol.......................  Non-detect...........         30   
    Benzyl chloride....................  Non-detect...........        100   
    Bis(2-chloroethoxy)methane.........  Non-detect...........       1200   
    Bis(2-chloroethyl)ether............  Non-detect...........       1200   
    Bis(2-ethylhexyl)phthalate.........  Non-detect...........       1200   
    Bromide............................  Non-detect...........          5.0 
    Bromodichloromethane...............  Non-detect...........         34   
    Calcium Cyanide....................  Non-detect...........          1.8 
    Calcium chromate...................  Non-detect...........          3.6 
    Chlordane..........................  Non-detect...........         12   
    
    [[Page 43506]]
    
                                                                            
    Chloride...........................  Non-detect...........          5.0 
    Chloroethane.......................  Non-detect...........         34   
    Copper Cyanide.....................  Non-detect...........          1.7 
    Cyanide............................  Non-detect...........          1.0 
    Cyanogen Bromide...................  Non-detect...........          6.6 
    Cyanogen Chloride..................  Non-detect...........          8.6 
    Di-selenium-tetra-sulfide..........  Non-detect...........        370   
    Dibenzofuran.......................  Non-detect...........       1200   
    Dibromochloromethane...............  Non-detect...........         34   
    Endosulfan I.......................  Non-detect...........          1.2 
    Endosulfan II......................  Non-detect...........          1.2 
    Endothal...........................  Non-detect...........        100   
    Endrin.............................  Non-detect...........          1.2 
    Endrin aldehyde....................  Non-detect...........          1.2 
    Endrin ketone......................  Non-detect...........          1.2 
    Epichlorohydrin....................  Non-detect...........         30   
    Ethyl carbamate....................  Non-detect...........        100   
    Ethylene glycol monoethyl ether....  Non-detect...........        100   
    Ethylenethiourea (2-                 Non-detect...........         12   
     Imidazolidinethione).                                                  
    Fluoride...........................  Non-detect...........          3.0 
    Heptachlor.........................  Non-detect...........          1.2 
    Heptachlor epoxide.................  Non-detect...........          2.4 
    Lead acetate.......................  Non-detect...........         22   
    Lead phosphate.....................  Non-detect...........         15   
    MNNG (N-Metyl-N-nitroso-N'-          Non-detect...........         12   
     nitroguanidine).                                                       
    Methomyl...........................  Non-detect...........          6.0 
    N-Nitrosodiphenylamine.............  Non-detect...........       1200   
    Nickel Cyanide.....................  Non-detect...........          3.5 
    Nickel carbonyl....................  Non-detect...........          7.0 
    Nicotine...........................  Non-detect...........        100   
    Octachlorodibenzodioxin............  Non-detect...........        150   
    Octachlorodibenzofuran.............  Non-detect...........        150   
    Osmium tetraoxide..................  Non-detect...........         40   
    Phenanthrene.......................  860..................  ............
    Phenylthiourea.....................  Non-detect...........          6.0 
    Potassium Cyanide..................  Non-detect...........          2.5 
    Potassium Silver Cyanide...........  Non-detect...........          2.9 
    Propargyl alcohol..................  Non-detect...........         30   
    Pyrene.............................  Non-detect...........       1200   
    Selenium dioxide...................  Non-detect...........          0.21
    Selenium sulfide...................  Non-detect...........          0.34
    Silver Cyanide.....................  Non-detect...........          2.6 
    Silvex.............................  Non-detect...........          6.0 
    Strychnine.........................  Non-detect...........        100   
    Tetra-selenium-tetra-sulfide.......  Non-detect...........        710   
    Tetraethyl lead....................  Non-detect...........         18   
    Thallium acetate...................  Non-detect...........         15   
    Thallium carbonate.................  Non-detect...........         14   
    Thallium chloride..................  Non-detect...........         14   
    Thallium nitrate...................  Non-detect...........         16   
    Thallium oxide.....................  Non-detect...........         12   
    Thallium sulfate...................  Non-detect...........         15   
    Thioacetamide......................  Non-detect...........          6.0 
    Thiofanox..........................  Non-detect...........        100   
    Thiourea...........................  Non-detect...........          6.0 
    Toluene-2,4-diamine................  Non-detect...........          6.0 
    Toluene-2,6-diamine................  Non-detect...........          6.0 
    Vanadium pentoxide.................  Non-detect...........         18   
    Zinc Cyanide.......................  Non-detect...........          2.3 
    Zinc phosphide.....................  Non-detect...........          0.32
    alpha-BHC..........................  Non-detect...........          1.2 
    beta-BHC...........................  Non-detect...........          1.2 
    delta-BHC..........................  Non-detect...........          1.2 
    gamma-BHC (Lindane)................  Non-detect...........          1.2 
    m-Dinitrobenzene...................  Non-detect...........       1200   
    p-Toluidine........................  Non-detect...........        100   
    trans-1,3-Dichloropropene..........  Non-detect...........         34   
    ------------------------------------------------------------------------
    
    
    
    [[Page 43507]]
    
    
    
      Table 3.--Detection and Detection Limit Values for a Possile Number 4 
                             Fuel Oil Specification                         
    ------------------------------------------------------------------------
                                                                   Maximum  
                                          Concentration limit     detection 
               Chemical name             (mg/kg at 10,000 Btu/   limit (mg/ 
                                                  lb)                kg)    
    ------------------------------------------------------------------------
    1,1,1-Trichloroethane..............  Non-detect...........         17   
    1,1,2-Trichloro-1,2,2-               Non-detect...........         29   
     trifluoroethane.                                                       
    1,1-Dichloro-1-propene.............  Non-detect...........         29   
    1,1-Dichloroethane.................  Non-detect...........         17   
    1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........         72   
     dioxin.                                                                
    1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........         72   
     furan.                                                                 
    1,2,3,4-Tetrachlorobenzene.........  Non-detect...........        100   
    1,2,3,5-Tetrachlorobenzene.........  Non-detect...........        100   
    1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........         72   
     dioxin.                                                                
    1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........         72   
     furan.                                                                 
    1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........         72   
     dioxin.                                                                
    1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........         72   
     furan.                                                                 
    1,2,3-Trichlorobenzene.............  Non-detect...........        100   
    1,2-Dichloroethane.................  Non-detect...........         17   
    1,2-Dichloropropane................  Non-detect...........         17   
    1,3-Dichloro-2-propanol............  Non-detect...........         29   
    1,3-Dichloropropane................  Non-detect...........         29   
    1,3-Propane sultone................  Non-detect...........        100   
    1-Chloronaphthalene................  Non-detect...........        100   
    2,2-Dichloropropane................  Non-detect...........         29   
    2,3,4,5-Tetrachlorophenol..........  Non-detect...........        100   
    2,3,4-Trichlorophenol..............  Non-detect...........        100   
    2,3,5-Trichlorophenol..............  Non-detect...........        100   
    2,3,6-Trichlorophenol..............  Non-detect...........        100   
    2,3,7,8-Tetrachlorodibenzo-p-dioxin  Non-detect...........         29   
    2,3,7,8-Tetrachlorodibenzo-p-furan.  Non-detect...........         29   
    2,3-Dichloro-1-propene.............  Non-detect...........         29   
    2,3-Dichlorophenol.................  Non-detect...........        100   
    2,4-D..............................  Non-detect...........          5.7 
    2,5-Dichlorophenol.................  Non-detect...........        100   
    2-Fluoroacetamide..................  Non-detect...........        100   
    2-Methylnaphthalene................  1000.................          -   
    2-Nitropropane.....................  Non-detect...........         29   
    3,3'-Dimethoxybenzidine............  Non-detect...........        100   
    3,4-Dichlorophenol.................  Non-detect...........        100   
    3,5-Dichlorophenol.................  Non-detect...........        100   
    3-/4-Chlorophenol..................  Non-detect...........        100   
    3-Nitroaniline.....................  Non-detect...........        200   
    4,4'-methylene-bis(2-chloroaniline)  Non-detect...........        100   
    4-Aminopyrridine...................  Non-detect...........        100   
    4-Chlorophenyl phenyl ether........  Non-detect...........        200   
    6-Propyl-2-thiouracil..............  Non-detect...........        100   
    Acenaphthene.......................  Non-detect...........        200   
    Acetone cyanohydrin................  Non-detect...........        100   
    Allyl alcohol......................  Non-detect...........         29   
    Ammonium vanadate..................  Non-detect...........         68   
    Anthracene.........................  Non-detect...........        200   
    Arochlor-1016......................  Non-detect...........          1.1 
    Arochlor-1221......................  Non-detect...........          1.1 
    Arochlor-1232......................  Non-detect...........          1.1 
    Arochlor-1242......................  Non-detect...........          1.1 
    Arochlor-1248......................  Non-detect...........          1.1 
    Arochlor-1254......................  Non-detect...........          1.1 
    Arochlor-1260......................  Non-detect...........          1.1 
    Arsenic acid.......................  Non-detect...........          0.43
    Arsenic pentoxide..................  Non-detect...........          0.35
    Arsenic trioxide...................  Non-detect...........          0.30
    Barium Cyanide.....................  Non-detect...........          3.7 
    Benzal chloride....................  Non-detect...........        100   
    Benzenethiol.......................  Non-detect...........         29   
    Benzyl chloride....................  Non-detect...........        100   
    Bis(2-chloroethoxy)methane.........  Non-detect...........        200   
    Bis(2-chloroethyl)ether............  Non-detect...........        200   
    Bis(2-ethylhexyl)phthalate.........  Non-detect...........        200   
    Bromide............................  Non-detect...........          5.0 
    Bromodichloromethane...............  Non-detect...........         17   
    Calcium Cyanide....................  Non-detect...........          1.8 
    Calcium chromate...................  Non-detect...........          6.9 
    Chlordane..........................  Non-detect...........         11   
    
    [[Page 43508]]
    
                                                                            
    Chloride...........................  Non-detect...........          5.0 
    Chloroethane.......................  Non-detect...........         17   
    Copper Cyanide.....................  Non-detect...........          1.7 
    Cyanide............................  Non-detect...........          1.0 
    Cyanogen Bromide...................  Non-detect...........          6.6 
    Cyanogen Chloride..................  Non-detect...........          8.6 
    Di-selenium-tetra-sulfide..........  Non-detect...........       1300   
    Dibenzofuran.......................  Non-detect...........        200   
    Dibromochloromethane...............  Non-detect...........         17   
    Endosulfan I.......................  Non-detect...........          1.1 
    Endosulfan II......................  Non-detect...........          1.1 
    Endothal...........................  Non-detect...........        100   
    Endrin.............................  Non-detect...........          1.1 
    Endrin aldehyde....................  Non-detect...........          1.1 
    Endrin ketone......................  Non-detect...........          1.1 
    Epichlorohydrin....................  Non-detect...........         29   
    Ethyl carbamate....................  Non-detect...........        100   
    Ethylene glycol monoethyl ether....  Non-detect...........        100   
    Ethylenethiourea (2-                 Non-detect...........        110   
     Imidazolidinethione).                                                  
    Fluoride...........................  Non-detect...........          3.0 
    Heptachlor.........................  Non-detect...........          1.1 
    Heptachlor epoxide.................  Non-detect...........          2.3 
    Lead acetate.......................  Non-detect...........         34   
    Lead phosphate.....................  Non-detect...........         24   
    MNNG (N-Metyl-N-nitroso-N'-          Non-detect...........        110   
     nitroguanidine).                                                       
    Methomyl...........................  Non-detect...........         57   
    N-Nitrosodiphenylamine.............  Non-detect...........        200   
    Nickel Cyanide.....................  Non-detect...........          3.5 
    Nickel carbonyl....................  Non-detect...........         13   
    Nicotine...........................  Non-detect...........        100   
    Octachlorodibenzodioxin............  Non-detect...........        140   
    Octachlorodibenzofuran.............  Non-detect...........        140   
    Osmium tetraoxide..................  Non-detect...........         40   
    Phenanthrene.......................  250..................          -   
    Phenylthiourea.....................  Non-detect...........         57   
    Potassium Cyanide..................  Non-detect...........          2.5 
    Potassium Silver Cyanide...........  Non-detect...........          2.9 
    Propargyl alcohol..................  Non-detect...........         29   
    Pyrene.............................  Non-detect...........        200   
    Selenium dioxide...................  Non-detect...........          0.35
    Selenium sulfide...................  Non-detect...........          0.56
    Silver Cyanide.....................  Non-detect...........          2.6 
    Silvex.............................  Non-detect...........          5.7 
    Strychnine.........................  Non-detect...........        100   
    Tetra-selenium-tetra-sulfide.......  Non-detect...........       2400   
    Tetraethyl lead....................  Non-detect...........         29   
    Thallium acetate...................  Non-detect...........         30   
    Thallium carbonate.................  Non-detect...........         26   
    Thallium chloride..................  Non-detect...........         27   
    Thallium nitrate...................  Non-detect...........         30   
    Thallium oxide.....................  Non-detect...........         24   
    Thallium sulfate...................  Non-detect...........         28   
    Thioacetamide......................  Non-detect...........         57   
    Thiofanox..........................  Non-detect...........        100   
    Thiourea...........................  Non-detect...........         57   
    Toluene-2,4-diamine................  Non-detect...........         57   
    Toluene-2,6-diamine................  Non-detect...........         57   
    Vanadium pentoxide.................  Non-detect...........         18   
    Zinc Cyanide.......................  Non-detect...........          2.3 
    Zinc phosphide.....................  Non-detect...........          0.75
    alpha-BHC..........................  Non-detect...........          1.1 
    beta-BHC...........................  Non-detect...........          1.1 
    delta-BHC..........................  Non-detect...........          1.1 
    gamma-BHC (Lindane)................  Non-detect...........          1.1 
    m-Dinitrobenzene...................  Non-detect...........        200   
    p-Toluidine........................  Non-detect...........        100   
    trans-1,3-Dichloropropene..........  Non-detect...........         17   
    ------------------------------------------------------------------------
    
    
    
    [[Page 43509]]
    
    
    
     Table 4.--Detection and Detection Limit Values for a Possible Number 6 
                             Fuel Oil Specification                         
    ------------------------------------------------------------------------
                                                                   Maximum  
                                          Concentration limit     detection 
               Chemical name             (mg/kg at 10,000 Btu/   limit (mg/ 
                                                  lb)                kg)    
    ------------------------------------------------------------------------
    1,1,1-Trichloroethane..............  Non-detect...........         21   
    1,1,2-Trichloro-1,2,2-               Non-detect...........         26   
     trifluoroethane.                                                       
    1,1-Dichloro-1-propene.............  Non-detect...........         26   
    1,1-Dichloroethane.................  Non-detect...........         21   
    1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........         64   
     dioxin.                                                                
    1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........         64   
     furan.                                                                 
    1,2,3,4-Tetrachlorobenzene.........  Non-detect...........        100   
    1,2,3,5-Tetrachlorobenzene.........  Non-detect...........        100   
    1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........         64   
     dioxin.                                                                
    1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........         64   
     furan.                                                                 
    1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........         64   
     dioxin.                                                                
    1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........         64   
     furan.                                                                 
    1,2,3-Trichlorobenzene.............  Non-detect...........        100   
    1,2-Dichloroethane.................  Non-detect...........         21   
    1,2-Dichloropropane................  Non-detect...........         21   
    1,3-Dichloro-2-propanol............  Non-detect...........         26   
    1,3-Dichloropropane................  Non-detect...........         26   
    1,3-Propane sultone................  Non-detect...........        100   
    1-Chloronaphthalene................  Non-detect...........        100   
    2,2-Dichloropropane................  Non-detect...........         26   
    2,3,4,5-Tetrachlorophenol..........  Non-detect...........        100   
    2,3,4-Trichlorophenol..............  Non-detect...........        100   
    2,3,5-Trichlorophenol..............  Non-detect...........        100   
    2,3,6-Trichlorophenol..............  Non-detect...........        100   
    2,3,7,8-Tetrachlorodibenzo-p-dioxin  Non-detect...........         26   
    2,3,7,8-Tetrachlorodibenzo-p-furan.  Non-detect...........         26   
    2,3-Dichloro-1-propene.............  Non-detect...........         26   
    2,3-Dichlorophenol.................  Non-detect...........        100   
    2,4-D..............................  Non-detect...........          5.1 
    2,5-Dichlorophenol.................  Non-detect...........        100   
    2-Fluoroacetamide..................  Non-detect...........        100   
    2-Methylnaphthalene................  4200.................  ............
    2-Nitropropane.....................  Non-detect...........         26   
    3,3'-Dimethoxybenzidine............  Non-detect...........        100   
    3,4-Dichlorophenol.................  Non-detect...........        100   
    3,5-Dichlorophenol.................  Non-detect...........        100   
    3-/4-Chlorophenol..................  Non-detect...........        100   
    3-Nitroaniline.....................  Non-detect...........        980   
    4,4'-methylene-bis(2-chloroaniline)  Non-detect...........        100   
    4-Aminopyrridine...................  Non-detect...........        100   
    4-Chlorophenyl phenyl ether........  Non-detect...........        980   
    6-Propyl-2-thiouracil..............  Non-detect...........        100   
    Acenaphthene.......................  Non-detect...........        980   
    Acetone cyanohydrin................  Non-detect...........        100   
    Allyl alcohol......................  Non-detect...........         26   
    Ammonium vanadate..................  Non-detect...........        590   
    Anthracene.........................  Non-detect...........        980   
    Arochlor-1016......................  Non-detect...........          1.0 
    Arochlor-1221......................  Non-detect...........          1.0 
    Arochlor-1232......................  Non-detect...........          1.0 
    Arochlor-1242......................  Non-detect...........          1.0 
    Arochlor-1248......................  Non-detect...........          1.0 
    Arochlor-1254......................  Non-detect...........          1.0 
    Arochlor-1260......................  Non-detect...........          1.0 
    Arsenic acid.......................  Non-detect...........          0.39
    Arsenic pentoxide..................  Non-detect...........          0.31
    Arsenic trioxide...................  Non-detect...........          0.27
    Barium Cyanide.....................  Non-detect...........          3.7 
    Benzal chloride....................  Non-detect...........        100   
    Benzenethiol.......................  Non-detect...........         26   
    Benzyl chloride....................  Non-detect...........        100   
    Bis(2-chloroethoxy)methane.........  Non-detect...........        980   
    Bis(2-chloroethyl)ether............  Non-detect...........        980   
    Bis(2-ethylhexyl)phthalate.........  Non-detect...........        980   
    Bromide............................  Non-detect...........          5.0 
    Bromodichloromethane...............  Non-detect...........         21   
    Calcium Cyanide....................  Non-detect...........          1.8 
    Calcium chromate...................  Non-detect...........          6.1 
    Chlordane..........................  Non-detect...........         10   
    
    [[Page 43510]]
    
                                                                            
    Chloride...........................  Non-detect...........          5.0 
    Chloroethane.......................  Non-detect...........         21   
    Copper Cyanide.....................  Non-detect...........          1.7 
    Cyanide............................  Non-detect...........          1.0 
    Cyanogen Bromide...................  Non-detect...........          6.6 
    Cyanogen Chloride..................  Non-detect...........          8.6 
    Di-selenium-tetra-sulfide..........  Non-detect...........       1400   
    Dibenzofuran.......................  Non-detect...........        980   
    Dibromochloromethane...............  Non-detect...........         21   
    Endosulfan I.......................  Non-detect...........          1.0 
    Endosulfan II......................  Non-detect...........          1.0 
    Endothal...........................  Non-detect...........        100   
    Endrin.............................  Non-detect...........          1.0 
    Endrin aldehyde....................  Non-detect...........          1.0 
    Endrin ketone......................  Non-detect...........          1.0 
    Epichlorohydrin....................  Non-detect...........         26   
    Ethyl carbamate....................  Non-detect...........        100   
    Ethylene glycol monoethyl ether....  Non-detect...........        100   
    Ethylenethiourea (2-                 Non-detect...........        100   
     Imidazolidinethione).                                                  
    Fluoride...........................  Non-detect...........          3.0 
    Heptachlor.........................  Non-detect...........          1.0 
    Heptachlor epoxide.................  Non-detect...........          2.0 
    Lead acetate.......................  Non-detect...........        110   
    Lead phosphate.....................  Non-detect...........         79   
    MNNG (N-Metyl-N-nitroso-N'-          Non-detect...........        100   
     nitroguanidine).                                                       
    Methomyl...........................  Non-detect...........         50   
    N-Nitrosodiphenylamine.............  Non-detect...........        980   
    Nickel Cyanide.....................  Non-detect...........          3.5 
    Nickel carbonyl....................  Non-detect...........        330   
    Nicotine...........................  Non-detect...........        100   
    Octachlorodibenzodioxin............  Non-detect...........        130   
    Octachlorodibenzofuran.............  Non-detect...........        130   
    Osmium tetraoxide..................  Non-detect...........         40   
    Phenanthrene.......................  860..................  ............
    Phenylthiourea.....................  Non-detect...........         50   
    Potassium Cyanide..................  Non-detect...........          2.5 
    Potassium Silver Cyanide...........  Non-detect...........          2.9 
    Propargyl alcohol..................  Non-detect...........         26   
    Pyrene.............................  610..................  ............
    Selenium dioxide...................  Non-detect...........          0.40
    Selenium sulfide...................  Non-detect...........          0.63
    Silver Cyanide.....................  Non-detect...........          2.6 
    Silvex.............................  Non-detect...........          5.1 
    Strychnine.........................  Non-detect...........        100   
    Tetra-selenium-tetra-sulfide.......  Non-detect...........       2600   
    Tetraethyl lead....................  Non-detect...........         94   
    Thallium acetate...................  Non-detect...........         26   
    Thallium carbonate.................  Non-detect...........         23   
    Thallium chloride..................  Non-detect...........         24   
    Thallium nitrate...................  Non-detect...........         27   
    Thallium oxide.....................  Non-detect...........         21   
    Thallium sulfate...................  Non-detect...........         25   
    Thioacetamide......................  Non-detect...........         50   
    Thiofanox..........................  Non-detect...........        100   
    Thiourea...........................  Non-detect...........         50   
    Toluene-2,4-diamine................  Non-detect...........         50   
    Toluene-2,6-diamine................  Non-detect...........         50   
    Vanadium pentoxide.................  Non-detect...........         18   
    Zinc Cyanide.......................  Non-detect...........          2.3 
    Zinc phosphide.....................  Non-detect...........         11   
    alpha-BHC..........................  Non-detect...........          5.0 
    beta-BHC...........................  Non-detect...........          5.0 
    delta-BHC..........................  Non-detect...........          1.0 
    gamma-BHC (Lindane)................  Non-detect...........          1.0 
    m-Dinitrobenzene...................  Non-detect...........        980   
    p-Toluidine........................  Non-detect...........        100   
    trans-1,3-Dichloropropene..........  Non-detect...........         21   
    ------------------------------------------------------------------------
    
    
    
    [[Page 43511]]
    
    
    
     Table 5.--Detection and Detection Limit Values for a Possible Composite
                  Fuel Specification--50th Percentile Analysis              
    ------------------------------------------------------------------------
                                                                   Maximum  
                                          Concentration limit     detection 
               Chemical name             (mg/kg at 10,000 Btu/   limit (mg/ 
                                                  lb)                kg)    
    ------------------------------------------------------------------------
    1,1,1-Trichloroethane..............  Non-detect...........         17   
    1,1,2-Trichloro-1,2,2-               Non-detect...........         29   
     trifluoroethane.                                                       
    1,1-Dichloro-1-propene.............  Non-detect...........         29   
    1,1-Dichloroethane.................  Non-detect...........         17   
    1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........         64   
     dioxin.                                                                
    1,2,3,4,6,7,8-Heptachlorodibenzo-p-  Non-detect...........         64   
     furan.                                                                 
    1,2,3,4-Tetrachlorobenzene.........  Non-detect...........        100   
    1,2,3,5-Tetrachlorobenzene.........  Non-detect...........        100   
    1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........         64   
     dioxin.                                                                
    1,2,3,6,7,8-Hexachlorodibenzo-p-     Non-detect...........         64   
     furan.                                                                 
    1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........         64   
     dioxin.                                                                
    1,2,3,7,8-Pentachlorodibenzo-p-      Non-detect...........         64   
     furan.                                                                 
    1,2,3-Trichlorobenzene.............  Non-detect...........        100   
    1,2-Dichloroethane.................  Non-detect...........         17   
    1,2-Dichloropropane................  Non-detect...........         17   
    1,3-Dichloro-2-propanol............  Non-detect...........         29   
    1,3-Dichloropropane................  Non-detect...........         29   
    1,3-Propane sultone................  Non-detect...........        100   
    1-Chloronaphthalene................  Non-detect...........        100   
    2,2-Dichloropropane................  Non-detect...........         29   
    2,3,4,5-Tetrachlorophenol..........  Non-detect...........        100   
    2,3,4-Trichlorophenol..............  Non-detect...........        100   
    2,3,5-Trichlorophenol..............  Non-detect...........        100   
    2,3,6-Trichlorophenol..............  Non-detect...........        100   
    2,3,7,8-Tetrachlorodibenzo-p-dioxin  Non-detect...........         26   
    2,3,7,8-Tetrachlorodibenzo-p-furan.  Non-detect...........         26   
    2,3-Dichloro-1-propene.............  Non-detect...........         29   
    2,3-Dichlorophenol.................  Non-detect...........        100   
    2,4-D..............................  Non-detect...........          5.7 
    2,5-Dichlorophenol.................  Non-detect...........        100   
    2-Fluoroacetamide..................  Non-detect...........        100   
    2-Methylnaphthalene................  1000.................  ............
    2-Nitropropane.....................  Non-detect...........         29   
    3,3'-Dimethoxybenzidine............  Non-detect...........        100   
    3,4-Dichlorophenol.................  Non-detect...........        100   
    3,5-Dichlorophenol.................  Non-detect...........        100   
    3-/4-Chlorophenol..................  Non-detect...........        100   
    3-Nitroaniline.....................  Non-detect...........        220   
    4,4'-methylene-bis(2-chloroaniline)  Non-detect...........        100   
    4-Aminopyrridine...................  Non-detect...........        100   
    4-Chlorophenyl phenyl ether........  Non-detect...........        220   
    6-Propyl-2-thiouracil..............  Non-detect...........        100   
    Acenaphthene.......................  Non-detect...........        220   
    Acetone cyanohydrin................  Non-detect...........        100   
    Allyl alcohol......................  Non-detect...........         29   
    Ammonium vanadate..................  Non-detect...........         31   
    Anthracene.........................  Non-detect...........        220   
    Arochlor-1016......................  Non-detect...........          1.1 
    Arochlor-1221......................  Non-detect...........          1.1 
    Arochlor-1232......................  Non-detect...........          1.1 
    Arochlor-1242......................  Non-detect...........          1.1 
    Arochlor-1248......................  Non-detect...........          1.1 
    Arochlor-1254......................  Non-detect...........          1.1 
    Arochlor-1260......................  Non-detect...........          1.1 
    Arsenic acid.......................  Non-detect...........          0.27
    Arsenic pentoxide..................  Non-detect...........          0.22
    Arsenic trioxide...................  Non-detect...........          0.19
    Barium Cyanide.....................  Non-detect...........          3.7 
    Benzal chloride....................  Non-detect...........        100   
    Benzenethiol.......................  Non-detect...........         29   
    Benzyl chloride....................  Non-detect...........        100   
    Bis(2-chloroethoxy)methane.........  Non-detect...........        220   
    Bis(2-chloroethyl)ether............  Non-detect...........        220   
    Bis(2-ethylhexyl)phthalate.........  Non-detect...........        220   
    Bromide............................  Non-detect...........          5.0 
    Bromodichloromethane...............  Non-detect...........         17   
    Calcium Cyanide....................  Non-detect...........          1.8 
    Calcium chromate...................  Non-detect...........          4.2 
    
    [[Page 43512]]
    
                                                                            
    Chlordane..........................  Non-detect...........         11   
    Chloride...........................  2.6..................  ............
    Chloroethane.......................  Non-detect...........         17   
    Copper Cyanide.....................  Non-detect...........          1.7 
    Cyanide............................  Non-detect...........          1.0 
    Cyanogen Bromide...................  Non-detect...........          6.6 
    Cyanogen Chloride..................  Non-detect...........          8.6 
    Di-selenium-tetra-sulfide..........  Non-detect...........        420   
    Dibenzofuran.......................  Non-detect...........        220   
    Dibromochloromethane...............  Non-detect...........         17   
    Endosulfan I.......................  Non-detect...........          1.1 
    Endosulfan II......................  Non-detect...........          1.1 
    Endothal...........................  Non-detect...........        100   
    Endrin.............................  Non-detect...........          1.1 
    Endrin aldehyde....................  Non-detect...........          1.1 
    Endrin ketone......................  Non-detect...........          1.1 
    Epichlorohydrin....................  Non-detect...........         29   
    Ethyl carbamate....................  Non-detect...........        100   
    Ethylene glycol monoethyl ether....  Non-detect...........        100   
    Ethylenethiourea (2-                 Non-detect...........         14   
     Imidazolidinethione).                                                  
    Fluoride...........................  Non-detect...........          3.0 
    Heptachlor.........................  Non-detect...........          1.1 
    Heptachlor epoxide.................  Non-detect...........          2.3 
    Lead acetate.......................  Non-detect...........         26   
    Lead phosphate.....................  Non-detect...........         18   
    MNNG (N-Metyl-N-nitroso-N'-          Non-detect...........         14   
     nitroguanidine).                                                       
    Methomyl...........................  Non-detect...........          7.0 
    N-Nitrosodiphenylamine.............  Non-detect...........        220   
    Nickel Cyanide.....................  Non-detect...........          3.5 
    Nickel carbonyl....................  Non-detect...........          8.2 
    Nicotine...........................  Non-detect...........        100   
    Octachlorodibenzodioxin............  Non-detect...........        130   
    Octachlorodibenzofuran.............  Non-detect...........        130   
    Osmium tetraoxide..................  Non-detect...........         40   
    Phenanthrene.......................  250..................  ............
    Phenylthiourea.....................  Non-detect...........          7.0 
    Potassium Cyanide..................  Non-detect...........          2.5 
    Potassium Silver Cyanide...........  Non-detect...........          2.9 
    Propargyl alcohol..................  Non-detect...........         29   
    Pyrene.............................  140..................  ............
    Selenium dioxide...................  Non-detect...........          0.26
    Selenium sulfide...................  Non-detect...........          0.41
    Silver Cyanide.....................  Non-detect...........          2.6 
    Silvex.............................  Non-detect...........          5.7 
    Strychnine.........................  Non-detect...........        100   
    Tetra-selenium-tetra-sulfide.......  Non-detect...........        810   
    Tetraethyl lead....................  Non-detect...........         22   
    Thallium acetate...................  Non-detect...........         18   
    Thallium carbonate.................  Non-detect...........         16   
    Thallium chloride..................  Non-detect...........         17   
    Thallium nitrate...................  Non-detect...........         18   
    Thallium oxide.....................  Non-detect...........         15   
    Thallium sulfate...................  Non-detect...........         17   
    Thioacetamide......................  Non-detect...........          7.0 
    Thiofanox..........................  Non-detect...........        100   
    Thiourea...........................  Non-detect...........          7.0 
    Toluene-2,4-diamine................  Non-detect...........          7.0 
    Toluene-2,6-diamine................  Non-detect...........          7.0 
    Vanadium pentoxide.................  Non-detect...........         18   
    Zinc Cyanide.......................  Non-detect...........          2.3 
    Zinc phosphide.....................  Non-detect...........          0.37
    alpha-BHC..........................  Non-detect...........          1.2 
    beta-BHC...........................  Non-detect...........          1.2 
    delta-BHC..........................  Non-detect...........          1.1 
    gamma-BHC (Lindane)................  Non-detect...........          1.1 
    m-Dinitrobenzene...................  Non-detect...........        220   
    p-Toluidine........................  Non-detect...........        100   
    
    [[Page 43513]]
    
                                                                            
    trans-1,3-Dichloropropene..........  Non-detect...........         17   
    ------------------------------------------------------------------------
    
    
    
       Table 6.--Detection and Detection Limit Values for a Possible Composite Fuel Specification--90th Percentile  
                                                        Analysis                                                    
    ----------------------------------------------------------------------------------------------------------------
                                                                                                          Maximum   
                          Chemical name                         Concentration limit (mg/kg at 10,000     detection  
                                                                              Btu/lb)                  limit (mg/kg)
    ----------------------------------------------------------------------------------------------------------------
    1,1,1-Trichloroethane....................................  Non-detect...........................          34    
    1,1,2-Trichloro-1,2,2-trifluoroethane....................  Non-detect...........................          30    
    1,1-Dichloro-1-propene...................................  Non-detect...........................          30    
    1,1-Dichloroethane.......................................  Non-detect...........................          34    
    1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin................  Non-detect...........................          74    
    1,2,3,4,6,7,8-Heptachlorodibenzo-p-furan.................  Non-detect...........................          74    
    1,2,3,4-Tetrachlorobenzene...............................  Non-detect...........................         100    
    1,2,3,5-Tetrachlorobenzene...............................  Non-detect...........................         100    
    1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin...................  Non-detect...........................          74    
    1,2,3,6,7,8-Hexachlorodibenzo-p-furan....................  Non-detect...........................          74    
    1,2,3,7,8-Pentachlorodibenzo-p-dioxin....................  Non-detect...........................          74    
    1,2,3,7,8-Pentachlorodibenzo-p-furan.....................  Non-detect...........................          74    
    1,2,3-Trichlorobenzene...................................  Non-detect...........................         100    
    1,2-Dichloroethane.......................................  Non-detect...........................          34    
    1,2-Dichloropropane......................................  Non-detect...........................          34    
    1,3-Dichloro-2-propanol..................................  Non-detect...........................          30    
    1,3-Dichloropropane......................................  Non-detect...........................          30    
    1,3-Propane sultone......................................  Non-detect...........................         100    
    1-Chloronaphthalene......................................  Non-detect...........................         100    
    2,2-Dichloropropane......................................  Non-detect...........................          30    
    2,3,4,5-Tetrachlorophenol................................  Non-detect...........................         100    
    2,3,4-Trichlorophenol....................................  Non-detect...........................         100    
    2,3,5-Trichlorophenol....................................  Non-detect...........................         100    
    2,3,6-Trichlorophenol....................................  Non-detect...........................         100    
    2,3,7,8-Tetrachlorodibenzo-p-dioxin......................  Non-detect...........................          30    
    2,3,7,8-Tetrachlorodibenzo-p-furan.......................  Non-detect...........................          30    
    2,3-Dichloro-1-propene...................................  Non-detect...........................          30    
    2,3-Dichlorophenol.......................................  Non-detect...........................         100    
    2,4-D....................................................  Non-detect...........................           6.7  
    2,5-Dichlorophenol.......................................  Non-detect...........................         100    
    2-Fluoroacetamide........................................  Non-detect...........................         100    
    2-Methylnaphthalene......................................  2500.................................           -    
    2-Nitropropane...........................................  Non-detect...........................          30    
    3,3'-Dimethoxybenzidine..................................  Non-detect...........................         100    
    3,4-Dichlorophenol.......................................  Non-detect...........................         100    
    3,5-Dichlorophenol.......................................  Non-detect...........................         100    
    3-/4-Chlorophenol........................................  Non-detect...........................         100    
    3-Nitroaniline...........................................  Non-detect...........................         700    
    4,4'-methylene-bis(2-chloroaniline)......................  Non-detect...........................         100    
    4-Aminopyrridine.........................................  Non-detect...........................         100    
    4-Chlorophenyl phenyl ether..............................  Non-detect...........................         700    
    6-Propyl-2-thiouracil....................................  Non-detect...........................         100    
    Acenaphthene.............................................  Non-detect...........................         700    
    Acetone cyanohydrin......................................  Non-detect...........................         100    
    Allyl alcohol............................................  Non-detect...........................          30    
    Ammonium vanadate........................................  Non-detect...........................          86    
    Anthracene...............................................  Non-detect...........................         700    
    Arochlor-1016............................................  Non-detect...........................           1.3  
    Arochlor-1221............................................  Non-detect...........................           1.3  
    Arochlor-1232............................................  Non-detect...........................           1.3  
    Arochlor-1242............................................  Non-detect...........................           1.3  
    Arochlor-1248............................................  Non-detect...........................           1.3  
    Arochlor-1254............................................  Non-detect...........................           1.3  
    Arochlor-1260............................................  Non-detect...........................           1.3  
    Arsenic acid.............................................  Non-detect...........................           0.41 
    Arsenic pentoxide........................................  Non-detect...........................           0.34 
    Arsenic trioxide.........................................  Non-detect...........................           0.29 
    Barium Cyanide...........................................  Non-detect...........................           3.7  
    
    [[Page 43514]]
    
                                                                                                                    
    Benzal chloride..........................................  Non-detect...........................         100    
    Benzenethiol.............................................  Non-detect...........................          30    
    Benzyl chloride..........................................  Non-detect...........................         100    
    Bis(2-chloroethoxy)methane...............................  Non-detect...........................         700    
    Bis(2-chloroethyl)ether..................................  Non-detect...........................         700    
    Bis(2-ethylhexyl)phthalate...............................  Non-detect...........................         700    
    Bromide..................................................  Non-detect...........................           5.0  
    Bromodichloromethane.....................................  Non-detect...........................          34    
    Calcium Cyanide..........................................  Non-detect...........................           1.8  
    Calcium chromate.........................................  Non-detect...........................           6.6  
    Chlordane................................................  Non-detect...........................          13    
    Chloride.................................................  2.7..................................           -    
    Chloroethane.............................................  Non-detect...........................          34    
    Copper Cyanide...........................................  Non-detect...........................           1.7  
    Cyanide..................................................  Non-detect...........................           1.0  
    Cyanogen Bromide.........................................  Non-detect...........................           6.6  
    Cyanogen Chloride........................................  Non-detect...........................           8.6  
    Di-selenium-tetra-sulfide................................  Non-detect...........................        1200    
    Dibenzofuran.............................................  Non-detect...........................         700    
    Dibromochloromethane.....................................  Non-detect...........................          34    
    Endosulfan I.............................................  Non-detect...........................           1.3  
    Endosulfan II............................................  Non-detect...........................           1.3  
    Endothal.................................................  Non-detect...........................         100    
    Endrin...................................................  Non-detect...........................           1.3  
    Endrin aldehyde..........................................  Non-detect...........................           1.3  
    Endrin ketone............................................  Non-detect...........................           1.3  
    Epichlorohydrin..........................................  Non-detect...........................          30    
    Ethyl carbamate..........................................  Non-detect...........................         100    
    Ethylene glycol monoethyl ether..........................  Non-detect...........................         100    
    Ethylenethiourea (2-Imidazolidinethione).................  Non-detect...........................         110    
    Fluoride.................................................  Non-detect...........................           3.0  
    Heptachlor...............................................  Non-detect...........................           1.3  
    Heptachlor epoxide.......................................  Non-detect...........................           2.7  
    Lead acetate.............................................  Non-detect...........................          74    
    Lead phosphate...........................................  Non-detect...........................          53    
    MNNG (N-Metyl-N-nitroso-N'-nitroguanidine)...............  Non-detect...........................         110    
    Methomyl.................................................  Non-detect...........................          54    
    N-Nitrosodiphenylamine...................................  Non-detect...........................         700    
    Nickel Cyanide...........................................  Non-detect...........................           3.5  
    Nickel carbonyl..........................................  Non-detect...........................          46    
    Nicotine.................................................  Non-detect...........................         100    
    Octachlorodibenzodioxin..................................  Non-detect...........................         150    
    Octachlorodibenzofuran...................................  Non-detect...........................         150    
    Osmium tetraoxide........................................  Non-detect...........................          40    
    Phenanthrene.............................................  730..................................           -    
    Phenylthiourea...........................................  Non-detect...........................          54    
    Potassium Cyanide........................................  Non-detect...........................           2.5  
    Potassium Silver Cyanide.................................  Non-detect...........................           2.9  
    Propargyl alcohol........................................  Non-detect...........................          30    
    Pyrene...................................................  600..................................           -    
    Selenium dioxide.........................................  Non-detect...........................           0.34 
    Selenium sulfide.........................................  Non-detect...........................           0.53 
    Silver Cyanide...........................................  Non-detect...........................           2.6  
    Silvex...................................................  Non-detect...........................           6.7  
    Strychnine...............................................  Non-detect...........................         100    
    Tetra-selenium-tetra-sulfide.............................  Non-detect...........................        2300    
    Tetraethyl lead..........................................  Non-detect...........................          63    
    Thallium acetate.........................................  Non-detect...........................          28    
    Thallium carbonate.......................................  Non-detect...........................          25    
    Thallium chloride........................................  Non-detect...........................          26    
    Thallium nitrate.........................................  Non-detect...........................          29    
    Thallium oxide...........................................  Non-detect...........................          23    
    Thallium sulfate.........................................  Non-detect...........................          27    
    Thioacetamide............................................  Non-detect...........................          54    
    Thiofanox................................................  Non-detect...........................         100    
    Thiourea.................................................  Non-detect...........................          54    
    Toluene-2,4-diamine......................................  Non-detect...........................          54    
    Toluene-2,6-diamine......................................  Non-detect...........................          54    
    Vanadium pentoxide.......................................  Non-detect...........................          18    
    
    [[Page 43515]]
    
                                                                                                                    
    Zinc Cyanide.............................................  Non-detect...........................           2.3  
    Zinc phosphide...........................................  Non-detect...........................           1.7  
    alpha-BHC................................................  Non-detect...........................           1.4  
    beta-BHC.................................................  Non-detect...........................           1.4  
    delta-BHC................................................  Non-detect...........................           1.3  
    gamma-BHC (Lindane)......................................  Non-detect...........................           1.3  
    m-Dinitrobenzene.........................................  Non-detect...........................         700    
    p-Toluidine..............................................  Non-detect...........................         100    
    trans-1,3-Dichloropropene................................  Non-detect...........................          34    
    ----------------------------------------------------------------------------------------------------------------
    
    
        Dated: August 15, 1996.
    Elizabeth A. Cotsworth,
    Acting Director, Office of Solid Waste.
    [FR Doc. 96-21628 Filed 8-22-96; 8:45 am]
    BILLING CODE 6560-50-P
    
    
    

Document Information

Published:
08/23/1996
Department:
Environmental Protection Agency
Entry Type:
Proposed Rule
Action:
Notice of data availability and request for comments.
Document Number:
96-21628
Dates:
Written comments on the peer review reports, the new comparable fuels analyses, and the synthesis gas process and product information must be submitted by September 23, 1996.
Pages:
43501-43515 (15 pages)
Docket Numbers:
FRL-5558-5
RINs:
2050-AF01: RCRA Smarter Waste Reporting
RIN Links:
https://www.federalregister.gov/regulations/2050-AF01/rcra-smarter-waste-reporting
PDF File:
96-21628.pdf
CFR: (9)
40 CFR 60
40 CFR 63
40 CFR 260
40 CFR 261
40 CFR 264
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