99-12585. National Emission Standards for Hazardous Air Pollutants for Source Categories; National Emission Standards for Hazardous Air Pollutants for Mineral Wool Production  

  • [Federal Register Volume 64, Number 104 (Tuesday, June 1, 1999)]
    [Rules and Regulations]
    [Pages 29490-29510]
    From the Federal Register Online via the Government Publishing Office [www.gpo.gov]
    [FR Doc No: 99-12585]
    
    
    
    [[Page 29489]]
    
    _______________________________________________________________________
    
    Part III
    
    
    
    
    
    Environmental Protection Agency
    
    
    
    
    
    _______________________________________________________________________
    
    
    
    40 CFR Parts 9 and 63
    
    
    
    National Emission Standards for Hazardous Air Pollutants for Source 
    Categories and for Mineral Wool Production; Final Rule
    
    Federal Register / Vol. 64, No. 104 / Tuesday, June 1, 1999 / Rules 
    and Regulations
    
    [[Page 29490]]
    
    
    
    ENVIRONMENTAL PROTECTION AGENCY
    
    40 CFR Parts 9 and 63
    
    [FRL-6345-4]
    RIN 2060-AE08
    
    
    National Emission Standards for Hazardous Air Pollutants for 
    Source Categories; National Emission Standards for Hazardous Air 
    Pollutants for Mineral Wool Production
    
    AGENCY: Environmental Protection Agency (EPA).
    
    ACTION: Final rule.
    
    -----------------------------------------------------------------------
    
    SUMMARY: This action promulgates national emission standards for 
    hazardous air pollutants (NESHAP) for new and existing sources in 
    mineral wool production facilities. Hazardous air pollutants (HAPs) 
    emitted by the facilities covered by this rule include carbonyl sulfide 
    (COS), nine hazardous metals, formaldehyde, and phenol. Exposure to 
    these HAPs may be associated with adverse carcinogenic, respiratory, 
    nervous system, dermal, developmental, and/or reproductive health 
    effects. The EPA estimates that the final rule will reduce nationwide 
    emissions of HAPs from these facilities by 46 megagrams per year (Mg/
    yr) (51 tons per year (tpy)). In addition, emissions of particulate 
    matter (PM) will be reduced by approximately 186 Mg/yr (205 tpy). This 
    action also amends 40 CFR part 9 by updating the table of currently 
    approved information collection control numbers to include the 
    information requirements contained in this final rule.
        These standards implement section 112(d) of the Clean Air Act (Act) 
    by requiring all mineral wool production facilities that are major 
    sources to meet hazardous air pollutant (HAP) emission standards 
    reflecting the application of the maximum achievable control technology 
    (MACT). The emissions reductions achieved by these standards, when 
    combined with the emissions reductions achieved by other similar 
    standards, will provide protection to the public and achieve a primary 
    goal of the Act.
        A supplement to the proposed rule was proposed in the Federal 
    Register on February 12, 1999 (64 FR 7149). The EPA will give careful 
    consideration to all comments on the supplemental proposal and will 
    amend this final rule in a future action as appropriate.
    
    EFFECTIVE DATE: June 1, 1999. See the SUPPLEMENTARY INFORMATION section 
    concerning judicial review.
    
    ADDRESSES: Docket. The docket for this rulemaking containing the 
    information considered by the EPA in development of the final rule is 
    Docket A-95-33. This docket is available for public inspection between 
    8 a.m. and 5:30 p.m., Monday through Friday, excluding Federal 
    holidays, at the following address: U.S. Environmental Protection 
    Agency, Air and Radiation Docket and Information Center (6102), 401 M 
    Street, SW, Washington, DC 20460; telephone number (202) 260-7548. The 
    docket is located at the above address in Room M-1500, Waterside Mall 
    (ground floor). A reasonable fee may be charged for copying docket 
    materials.
    
    FOR FURTHER INFORMATION CONTACT: Ms. Mary Johnson, Minerals and 
    Inorganic Chemicals Group, Emission Standards Division (MD-13), U.S. 
    Environmental Protection Agency, Research Triangle Park, North Carolina 
    27711; telephone number (919) 541-5025; facsimile number (919) 541-
    5600; electronic mail address johnson.mary@epamail.epa.gov''.
    
    SUPPLEMENTARY INFORMATION:
    
    Regulated Entities
    
        Categories and entities potentially regulated by this action 
    include:
    
    ------------------------------------------------------------------------
                                                    Examples of regulated
                     Category                             entities
    ------------------------------------------------------------------------
    Industry..................................  Mineral wool production
                                                 facilities (SIC 3296).
    Federal government........................  None.
    State/local/tribal government.............  None.
    ------------------------------------------------------------------------
    
        This table is not intended to be exhaustive, but rather provides a 
    guide for readers regarding entities likely to be regulated by this 
    action. To determine whether your facility is regulated by this action, 
    you should examine the applicability criteria in Sec. 63.1177 of the 
    final rule. If you have any questions regarding the applicability of 
    this action to a particular entity, consult the appropriate regional 
    representative:
    
    Region I:
        Janet Bowen, Office of Ecosystem Protection, U.S. EPA, Region I, 
    CAP, JFK Federal Building, Boston, MA 02203, (617) 565-3595
    Region II:
        Kenneth Eng, Air Compliance Branch Chief, U.S. EPA, Region II, 290 
    Broadway, New York, NY 10007-1866, (212) 637-4000
    Region III:
        Bernard Turlinski, Air Enforcement Branch Chief, U.S. EPA, Region 
    III, 3AT10, 841 Chestnut Building, Philadelphia, PA 19107, (215) 566-
    2110
    Region IV:
        Lee Page, Air Enforcement Branch, U.S. EPA, Region IV, Atlanta 
    Federal Center, 61 Forsyth Street, Atlanta, GA 30303-3104, (404) 562-
    9131
    Region V:
        George T. Czerniak, Jr., Air Enforcement Branch Chief, U.S. EPA, 
    Region V, 5AE-26, 77 West Jackson Street, Chicago, IL 60604, (312) 353-
    2088
    Region VI:
        John R. Hepola, Air Enforcement Branch Chief, U.S. EPA, Region VI, 
    1445 Ross Avenue, Suite 1200, Dallas, TX 75202-2733, (214) 665-7220
    Region VII:
        Donald Toensing, Air Permitting and Compliance, Branch Chief, U.S. 
    EPA, Region VII, 726 Minnesota Avenue, Kansas City, KS 66101, (913) 
    551-7446
    Region VIII:
        Douglas M. Skie, Air and Technical Operations, Branch Chief, U.S. 
    EPA, Region VIII, 999 18th Street, Suite 500, Denver, CO 80202-2466, 
    (303) 312-6432
    Region IX:
        Barbara Gross, Air Compliance Branch Chief, U.S. EPA, Region IX, 75 
    Hawthorne Street, San Francisco, CA 94105, (415) 744-1138
    Region X:
        Anita Frankel, Air and Radiation Branch Chief, U.S. EPA, Region X, 
    AT-092, 1200 Sixth Avenue, Seattle, WA 98101, (206) 553-1757
    
    Plain Language
    
        The final rule is written in plain language. Plain language 
    regulatory writing involves structuring the rule around questions the 
    user may have. It takes the form of questions and answers and uses the 
    words ``I'' and ``you'' to represent the owner or operator.
    
    Judicial Review
    
        The NESHAP for mineral wool production plants was proposed on May 
    8, 1997 (62 FR 25370). This action announces the EPA's final decisions 
    on the rule. Under section 307(b)(1) of the Act, judicial review of the 
    NESHAP is available only by filing a petition for review in the U.S. 
    Court of Appeals for the District of Columbia Circuit within 60 days of 
    today's publication of this final rule. Under section 307(b)(2) of the 
    Act, the requirements that are the subject of today's rule may not be 
    challenged later in civil or criminal proceedings brought by the EPA to 
    enforce these requirements.
    
    [[Page 29491]]
    
    Technology Transfer Network
    
        In addition to being available in the docket, an electronic copy of 
    today's notice is also available through the Technology Transfer 
    Network (TTN). Following promulgation, a copy of the rule will be 
    posted on the TTN's policy and guidance page for newly proposed or 
    promulgated rules (http://www.epa.gov/ttn/oarpg/t3pfpr.html). The TTN 
    provides information and technology exchange in various areas of air 
    pollution control. If more information regarding the TTN is needed, 
    call the TTN HELP line at (919) 541-5384.
    
    Outline
    
        The information presented in this preamble is organized as follows:
    
    I. Statutory Authority
    II. Background and Public Participation
    III. Summary of Final Rule
        A. Applicability
        B. Standards
        C. Compliance and Performance Test Provisions
        D. Monitoring Requirements
        E. Notification, Recordkeeping, and Reporting Requirements
    IV. Summary of Changes Since Proposal
        A. Definitions
        B. Standards
        C. Performance Test Provisions
        D. Monitoring Requirements
        E. Notification, Recordkeeping, and Reporting Requirements
    V. Summary of Impacts
    VI. Summary of Responses to Major Comments
        A. General
        B. Definitions
        C. Selection of Emission Standards
        D. Monitoring
        E. Recordkeeping and Reporting
    VII. Administrative Requirements
        A. Docket
        B. Executive Order 12866--Regulatory Planning and Review
        C. Executive Order 12875--Enhancing the Intergovernmental 
    Partnership
        D. Executive Order 13084--Consultation and Coordination with 
    Indian Tribal Governments
        E. Unfunded Mandates Reform Act
        F. Regulatory Flexibility
        G. Submission to Congress and the Comptroller General
        H. Paperwork Reduction Act
        I. Pollution Prevention Act
        J. National Technology Transfer and Advancement Act
        K. Executive Order 13045--Protection of Children From 
    Environmental Health Risks and Safety Risks
    
    I. Statutory Authority
    
        The statutory authority for this rule is provided by sections 101, 
    112, 113, 114, 116, and 301 of the Act, as amended (42 U.S.C. 7401, 
    7412, 7413, 7414, 7416, and 7601). This rule is also subject to section 
    307(d) of the Act (42 U.S.C. 7407(d)).
    
    II. Background and Public Participation
    
        Section 112(d) of the Act directs the EPA to establish standards to 
    control all major sources emitting HAPs. On July 16, 1992, the EPA 
    published a list of major source categories, including ``Mineral Wool 
    Production,'' for which NESHAP are to be promulgated (57 FR 3156). The 
    NESHAP for mineral wool production (40 CFR part 63, subpart DDD) was 
    proposed in the Federal Register on May 8, 1997 (62 FR 25370). The 
    public comment period ended on July 7, 1997. Industry representatives, 
    regulatory authorities, environmental groups, and the general public 
    had the opportunity to comment on the proposed standards and to provide 
    additional information during the public comment period. Three comment 
    letters were received. Comments were received from the association 
    representing industry and from two representatives of air pollution 
    control equipment manufacturers. Today's final rule reflects the EPA's 
    full consideration of the comments. A summary of the major public 
    comments along with the EPA's responses are summarized in this 
    preamble. A more detailed discussion of public comments and the EPA's 
    responses are contained in the docket (Docket No. A-95-33; Item V-C-2).
    
    III. Summary of Final Rule
    
    A. Applicability
    
        The final NESHAP applies to each existing, new, and reconstructed 
    cupola and curing oven at a mineral wool production facility that is 
    located at a plant site that is a major source of HAP emissions. 
    Facilities that manufacture wool fiberglass are not subject to this 
    rule but are subject to a separate NESHAP rulemaking for wool 
    fiberglass manufacturing.
    
    B. Standards
    
        Emissions of PM are regulated for existing cupolas. For new and 
    reconstructed cupolas, emissions of carbon monoxide (CO) are also 
    regulated. Emissions of formaldehyde are regulated for existing, new, 
    and reconstructed curing ovens. Particulate matter serves as a 
    surrogate for metal HAPs and CO is a surrogate for COS. In addition to 
    being a HAP itself, formaldehyde serves as a surrogate for phenol. A 
    numerical emission limit for PM expressed in kilograms per megagram 
    (kg/Mg) or pound per ton (lb/ton) of melt is promulgated in the final 
    rule. For CO or formaldehyde, the owner or operator may comply with 
    percent removal or numerical emission limits. The emission limits for 
    existing sources and new sources are presented below.
    
                 Summary of Emission Limits For Existing Sources
    ------------------------------------------------------------------------
               Source                     Pollutant           Emission limit
    ------------------------------------------------------------------------
    Cupola.....................  PM........................  0.05 kg/Mg
                                                              (0.10 lb/ton)
                                                              of melt.
    Curing oven................  Formaldehyde..............  0.03 kg/Mg
                                                              (0.06 lb/ton)
                                                              of melt or 80
                                                              percent
                                                              formaldehyde
                                                              removal.
    ------------------------------------------------------------------------
    
    
          Summary of Emission Limits For New and Reconstructed Sources
    ------------------------------------------------------------------------
               Source                     Pollutant           Emission limit
    ------------------------------------------------------------------------
    Cupola.....................  PM........................  0.05 kg/Mg
                                                              (0.10 lb/ton)
                                                              of melt.
                                 CO........................  0.05 kg/Mg
                                                              (0.10 lb/ton)
                                                              of melt or 99
                                                              percent CO
                                                              removal.
    Curing oven................  Formaldehyde..............  0.03 kg/Mg
                                                              (0.06 lb/ton)
                                                              of melt or 80
                                                              percent
                                                              formaldehyde
                                                              removal.
    ------------------------------------------------------------------------
    
        The owner or operator must also comply with operating limits. 
    Operating limits for cupolas are as follows:
        (1) Within one hour after the alarm on a bag leak detection system 
    sounds, the owner or operator must begin, and complete in a timely 
    manner, corrective actions as specified in their operations, 
    maintenance, and monitoring plan.
        (2) When the alarm on a bag leak detection system sounds for more 
    than
    
    [[Page 29492]]
    
    five percent of the total operating time in a six-month reporting 
    period, the owner or operator must develop and implement a written 
    quality improvement plan (QIP) consistent with the compliance assurance 
    monitoring requirements in Sec. 64.8(b)-(d) of 40 CFR part 64 (62 FR 
    54900, October 22, 1997).
        (3) For each new or reconstructed cupola, the owner or operator 
    must maintain the operating temperature of the thermal incinerator such 
    that the average operating temperature for each three-hour block period 
    never falls below the average temperature established during the 
    performance test.
        The owner or operator must meet the following operating limits for 
    curing ovens:
        (1) The owner or operator must maintain the free-formaldehyde 
    content of each resin lot and formaldehyde content of each binder 
    formulation at or below the specification ranges of the resin and 
    binder used during the performance test.
        (2) The owner or operator must maintain the operating temperature 
    of each thermal incinerator such that the average operating temperature 
    for each three-hour block period never falls below the average 
    temperature established during the performance test.
    
    C. Compliance and Performance Test Provisions
    
        For existing sources, compliance with the standards must be 
    demonstrated no later than three years from the effective date of the 
    final rule. An extension for a fourth year may be granted by the 
    Administrator under section 112(i)(3)(B) of the Act if necessary for 
    the installation of controls. For new and reconstructed sources, any 
    control devices or monitoring equipment necessary to meet the standards 
    must be installed. Performance testing must be completed and compliance 
    with all requirements of the final rule must be demonstrated by the 
    dates in Sec. 63.7 of the general provisions in subpart A of 40 CFR 
    part 63. On and after these dates, the owner or operator must comply 
    with the standards. The standards will apply at all times except during 
    periods of startup, shutdown, or malfunction.
        A performance test is required to demonstrate initial compliance 
    with the percent removal or numerical emissions limits for cupolas and 
    curing ovens. The performance test must be conducted while operating at 
    the maximum production rate and must consist of three test runs. All 
    monitoring systems and equipment must be installed, operational, and 
    properly calibrated prior to the performance tests. To comply with the 
    CO or formaldehyde emission limit for a cupola or curing oven 
    controlled by a thermal incinerator, or the PM limit for a fabric 
    filter-controlled cupola, measurements are made at the outlet of the 
    control device. If the owner or operator elects to comply with the 
    percent removal emission limit for CO or formaldehyde, measurements are 
    required at the inlet and outlet of the control device.
        The owner or operator is required to measure and record the amount 
    of raw materials, excluding coke, charged into and melted in each 
    cupola during each performance test run, determine the average hourly 
    melt rate for each performance test run, and determine the arithmetic 
    average of the average hourly melt rates associated with the three 
    performance test runs. The average hourly melt rate of the three 
    performance test runs is used to determine compliance.
        The owner or operator must conduct the performance test for each 
    curing oven while manufacturing the product that requires a binder 
    formulation made with the resin containing the highest free-
    formaldehyde content specification range. During the performance test, 
    the owner or operator must record the free-formaldehyde content 
    specification range of the resin used and the formulation of the binder 
    used, including formaldehyde content and binder specification.
        During the performance test for each cupola that uses a thermal 
    incinerator to comply with the emission limit for CO and each curing 
    oven that uses a thermal incinerator to comply with the formaldehyde 
    emission limit, the owner or operator is required to establish the 
    average operating temperature of the incinerator. The owner or operator 
    must continuously measure the operating temperature, determine the 
    average temperatures in consecutive 15-minute blocks, determine the 
    arithmetic average of the 15-minute block temperatures for each 
    performance test run, and determine the arithmetic average of the 
    average operating temperatures associated with the three performance 
    test runs.
        With prior approval from the Administrator, operating limits 
    established for control devices or processes during the initial 
    performance tests and used to monitor compliance may be expanded by 
    conducting additional performance tests to demonstrate compliance at 
    the new levels. Also, owners or operators of curing ovens may conduct 
    short-term experimental production runs without conducting additional 
    performance tests with prior approval from the Administrator.
    
    D. Monitoring Requirements
    
        Each fabric filter used on a cupola must be equipped with a bag 
    leak detection system having an audible alarm that automatically sounds 
    when an increase in particulate emissions above a predetermined level 
    is detected. The alarm must be located in an area where appropriate 
    plant personnel will be able to hear it. Such a device serves as an 
    indicator of the performance of the fabric filter and provides an 
    indication of when maintenance of the fabric filter is needed. The rule 
    requires that in response to an alarm, corrective actions be initiated 
    within one hour, and completed in a timely manner, according to the 
    operations, maintenance, and monitoring plan. The owner or operator is 
    in violation of this operating limit upon a failure to begin corrective 
    actions within one hour of the alarm.
        When the alarm is activated for more than five percent of the total 
    operating time during a six-month reporting period, the owner or 
    operator must develop and implement a written QIP consistent with the 
    compliance assurance monitoring requirements in Sec. 64.8(b)-(d) of 40 
    CFR part 64 (62 FR 54900, October 22, 1997). Failure to develop and 
    implement a written QIP that is consistent with the compliance 
    assurance monitoring requirements is a violation of this operating 
    limit.
        Each owner or operator of an affected curing oven must monitor and 
    record the free-formaldehyde content of each resin lot and the 
    formulation of each batch of binder used, including formaldehyde 
    content. Following the performance test, the owner or operator must 
    maintain the free-formaldehyde content of each resin lot and the 
    formaldehyde content of each binder formulation at or below the 
    specification ranges of the resin and binder used during the 
    performance test. If the free-formaldehyde content of a resin lot or 
    the formaldehyde content of a binder formulation exceeds the 
    performance test specification ranges, the owner or operator is in 
    violation of this operating limit.
        For each thermal incinerator used to control emissions from 
    affected cupolas or curing ovens, the owner or operator must 
    continuously measure the operating temperature of the incinerator. The 
    owner or operator must determine the average temperatures in 
    consecutive 15-minute blocks and then determine the arithmetic average 
    of the 15-minute averages for each one-hour period. The average 
    operating temperature of the
    
    [[Page 29493]]
    
    incinerator is based on the arithmetic average of the one-hour average 
    temperatures for each consecutive three-hour period. Following the 
    performance test, the owner or operator is required to maintain the 
    operating temperature so that the average operating temperature for 
    each three-hour block period never falls below the average temperature 
    established during the performance test. If the average temperature in 
    any three-hour block period falls below the average established during 
    the performance test, the owner or operator is in violation of this 
    operating limit. The owner or operator must operate and maintain each 
    incinerator as specified in their operations, maintenance, and 
    monitoring plan. Procedures for properly operating and maintaining an 
    incinerator must include an annual inspection.
        Under today's rule, the owner or operator may change control device 
    and process operating parameter levels established during performance 
    tests and used to monitor compliance. The owner or operator must notify 
    the Administrator and upon approval, conduct additional performance 
    tests at the proposed new control device or process operating parameter 
    levels to verify compliance with the applicable emission limits.
    
    E. Notification, Recordkeeping, and Reporting Requirements
    
        Notification, recordkeeping, and reporting requirements for NESHAP 
    are included in the general provisions (40 CFR part 63, subpart A). The 
    general provisions include requirements for: (1) Initial 
    notification(s) of applicability, notification of performance test, and 
    notification of compliance status; (2) a report of performance test 
    results; (3) a startup, shutdown, and malfunction plan, including a 
    semiannual report when a reportable event occurs and the steps in the 
    plan were not followed; and (4) semiannual reports of deviations from 
    established parameters. If deviations from established parameters are 
    reported, the owner or operator must report quarterly until a request 
    to return the reporting frequency to semiannual is approved.
        Owners or operators of affected cupolas and curing ovens must 
    submit an operations, maintenance, and monitoring plan as part of their 
    application for a title V permit. The plan must include procedures for 
    the proper operation and maintenance of processes and control devices 
    used to comply with the emission limits, including an annual inspection 
    of each thermal incinerator. The plan also must identify the process or 
    control device parameters to be monitored for compliance; the 
    established operating levels or ranges for each process or control 
    device; a monitoring schedule; the corrective actions to be taken when 
    process or control device parameters deviate from the levels 
    established during performance testing; and procedures for keeping 
    records to document compliance.
        In addition to requirements of the general provisions, the final 
    rule specifies additional records to be kept by the owner or operator. 
    The owner or operator is required to maintain records of the following, 
    as applicable:
        (1) Cupola production (melt) rate;
        (2) bag leak detection system alarms, the date and time of the 
    alarm, when corrective actions were initiated, the cause of the alarm, 
    an explanation of the corrective actions taken, and when the cause of 
    the alarm was corrected;
        (3) free-formaldehyde content of each resin lot and the binder 
    formulation, including formaldehyde content, of each binder batch used 
    in the manufacture of bonded products; and
        (4) incinerator operating temperature and results of incinerator 
    inspections, including periods when the average temperature in any 
    three-hour block period fell below the average temperature established 
    during the performance test and periods when the inspection identified 
    incinerator components in need of repair or maintenance, the date and 
    time of the problem, when corrective actions were intiated, the cause 
    of the problem, an explanation of the corrective actions taken, and 
    when the cause of the problem was corrected.
        The NESHAP general provisions require that records be maintained 
    for at least five years from the date of each record. The owner or 
    operator must retain the records on site for at least two years but may 
    retain the records off site the remaining three years. The records may 
    be retained on microfilm, on microfiche, on a computer, on computer 
    disks, or on magnetic tape disks. Reports may be made on paper or on 
    labeled computer disks using commonly available and compatible computer 
    software.
    
    IV. Summary of Changes Since Proposal
    
        Changes have been incorporated into the final NESHAP for mineral 
    wool production facilities in response to comments on the proposed 
    rule, with the exception of the format change to plain language. A 
    number of clarifications to the proposal language are reflected in the 
    final rule as a result of this question and answer format. The 
    principal changes made since proposal are summarized below. Additional 
    discussion of the changes and the rationale for these changes is 
    presented in section VI of this preamble.
    
    A. Definitions
    
        In response to public comments, minor clarifying changes were made 
    to the definition of mineral wool. Also, a definition for new source, 
    that incorporates the May 8, 1997 date that the NESHAP was proposed, 
    was added to the list of terms used in the final rule.
    
    B. Standards
    
        The final rule incorporates some changes to the proposed rule 
    regarding emission standards. Depending on available control and 
    monitoring technologies for particular source categories, emission 
    limits, as well as operating limits, are set forth as enforceable 
    regulatory requirements. In addition to emission limits, operating 
    limits are also included as part of the final rule regulating mineral 
    wool production facilities. These operating limits were included in the 
    proposed rule as monitoring requirements and have been moved into the 
    sections containing the emission limits in the final rule. These 
    operating limits specify the established requirements which are 
    enforceable and will be used to determine compliance.
        As a result of additional PM emissions data from fabric filter-
    controlled cupolas, the proposed PM emission limit of 0.03 kg/Mg (0.06 
    lb/ton) has been revised to 0.05 kg/Mg (0.10 lb/ton) in the final rule. 
    The additional data considered in making this determination are for 
    three cupolas controlled by fabric filters with identical parameters as 
    those previously determined to be representative of the MACT floor for 
    existing and new cupolas. An emissions limit of 0.05 kg/Mg (0.10 lb/
    ton) represents a level that can be achieved by the fabric filter-
    controlled cupola upon which the proposed PM emission limit was based, 
    as well as by these three fabric filter-controlled cupolas which are 
    also representative of the MACT floor.
    
    C. Performance Test Provisions
    
        A few changes were made to the performance test requirements in the 
    proposed rule. Revisions were made to clarify the proposed requirements 
    for performance testing by specifying in the final rule how to 
    establish the average operating temperature of an incinerator. The 
    proposed provision that would allow the owner or operator of curing 
    ovens subject to the NESHAP to conduct short-term experimental 
    production
    
    [[Page 29494]]
    
    runs without conducting additional performance tests was revised. The 
    final rule clarifies that the process modifications referred to in the 
    proposed rule mean pollution prevention process modifications.
        The proposed rule required the use of method 5 for determining the 
    concentration of PM with a minimum performance test run time of two 
    hours and a minimum sample volume of 2.5 dry standard cubic meters 
    (dscm) (90 dry standard cubic feet (dscf)). The final rule specifies a 
    minimum performance test run time of three hours and a minimum sample 
    volume of 3.75 dscm (135 dscf). These revisions are the result of re-
    evaluation of the test method procedures in response to public comments 
    regarding the level of the proposed emission limit for PM, and are to 
    ensure that an adequate amount of PM is captured on the filter for 
    analysis and subsequent compliance determination.
    
    D. Monitoring Requirements
    
        Several changes were made to the monitoring requirements in the 
    proposed rule. The final rule does not include the proposed 
    requirements to maintain the average hourly melt rate so that it does 
    not exceed the average melt rate established during the performance 
    test by more than 20 percent for more than five percent of the total 
    operating time in each six-month reporting period, and to do a repeat 
    performance test at the higher melt rate if the average hourly melt 
    rate exceeds the average melt rate established during the performance 
    test by more than 20 percent for more than five percent of the total 
    operating time in a six-month reporting period. The EPA determined that 
    these monitoring requirements are not necessary because compliance with 
    the PM standards will be assessed through use of a bag leak detection 
    system; compliance with the CO standards will be assessed through 
    monitoring incinerator operating temperature; and compliance with the 
    formaldehyde standards will be assessed through monitoring incinerator 
    operating temperature, monitoring free-formaldehyde content of resin, 
    and monitoring binder formulation. The average melt rate must still be 
    determined during each performance test in order to assess compliance 
    with the emissions standards. As a recordkeeping requirement, the final 
    rule continues to require that records of cupola melt rate be 
    maintained.
        As proposed, each fabric filter used on a cupola must be equipped 
    with a bag leak detection system having an audible alarm that 
    automatically sounds when an increase in particulate emissions above a 
    predetermined level is detected. The final rule clarifies that each 
    triboelectric bag leak detection system must be installed, operated, 
    adjusted, and maintained according to the EPA's ``Fabric Filter Bag 
    Leak Detection Guidance'' (EPA-454/R-98-015, September 1997) which is 
    available on the TTN under Emission Measurement Center (EMC), 
    Continuous Emission Monitoring. Other bag leak detection systems must 
    be installed, operated, adjusted, and maintained according to the 
    manufacturer's written specifications and recommendations. In response 
    to public comments and to maintain consistency with sensitivity (range) 
    specifications in other regulations, the final rule requires that the 
    bag leak detection system be capable of detecting PM emissions at 
    concentrations of 10 milligrams per actual cubic meter (0.0044 grains 
    per actual cubic foot). To maintain consistency with bag leak detection 
    system requirements in other regulations and to allow owners and 
    operators flexibility to make necessary bag leak detection system 
    adjustments, the final rule specifies that following initial 
    adjustment, the owner or operator may adjust the range, averaging 
    period, alarm set points, or alarm delay time as specified in the 
    approved operations, maintenance, and monitoring plan. The final rule 
    further specifies that in no event may the range be increased by more 
    than 100 percent or decreased by more than 50 percent over a 365 day 
    period unless a responsible official, as defined in Sec. 63.2 of the 
    general provisions in subpart A of 40 CFR part 63, certifies in writing 
    to the Administrator that the fabric filter has been inspected and 
    found to be in good operating condition. The final rule clarifies that 
    the alarm must be located in an area where appropriate plant personnel 
    will be able to hear it and that in response to the sounding of an 
    alarm, the owner or operator must complete corrective actions in a 
    timely manner.
        Under the proposed rule, the owner or operator would monitor and 
    record the free-formaldehyde content of each resin lot and the binder 
    formulation, including the formaldehyde content of each binder batch, 
    and would maintain the formaldehyde content of each binder formulation 
    at or below the level established during the performance test. The 
    final rule clarifies that the owner or operator must maintain the free-
    formaldehyde content of each resin lot and the formaldehyde content of 
    each binder formulation at or below the specification ranges of the 
    resin and binder used during the performance test. The use of ranges in 
    the final rule accommodates the fact that resins and binders are 
    produced in accordance with specification ranges rather than levels as 
    proposed.
        As proposed, the owner or operator would obtain, at a minimum, 
    valid three-hour block average incinerator operating temperatures for 
    75 percent of the operating hours per day for 90 percent of the 
    operating days per six-month reporting period. This requirement is not 
    included in the final rule in order to maintain consistency with the 
    compliance assurance monitoring final rule (62 FR 54899, October 22, 
    1997), which was revised based on comments received on its proposal and 
    now requires monitoring devices to be operational at all times that the 
    process is operational. Revisions were also made to clarify the 
    proposed requirements for monitoring incinerator operating temperature 
    by specifying in the final rule how to determine the average operating 
    temperature.
        Under the proposed rule, the owner or operator could change a 
    control device or process operating parameter level established during 
    the performance test by conducting additional performance tests at the 
    new parameter level. The final rule clarifies that the owner or 
    operator must notify the Administrator of the desire to expand the 
    range of a control device or process operating parameter level, and 
    upon approval, conduct additional performance tests at the proposed new 
    parameter levels before operating at these levels to verify compliance 
    with the emission limits.
    
    E. Notification, Recordkeeping, and Reporting Requirements
    
        A few changes were made since proposal to the notification, 
    recordkeeping, and reporting requirements. The final rule clarifies 
    that notifications of performance tests must be submitted to the 
    Administrator at least 60 days prior to the performance test. The final 
    rule also clarifies what elements are required to be included in 
    performance test reports. The proposed rule required an operations, 
    maintenance, and monitoring plan for each affected source that would 
    contain information on the proper operation and maintenance of control 
    devices, the parameters to be monitored for compliance and their 
    established operating levels, a monitoring schedule, corrective actions 
    to be taken when parameters deviate from the levels established during 
    performance testing, and procedures for keeping records to document 
    compliance. The final rule
    
    [[Page 29495]]
    
    specifies some example corrective actions for bag leak detection system 
    alarms that may be included in the operations, maintenance, and 
    monitoring plan. Consistent with the general provisions requirements to 
    operate and maintain air pollution control equipment in a manner 
    consistent with good air pollution control practices, the final rule 
    clarifies that the operations, maintenance, and monitoring plan 
    procedures for properly operating and maintaining control devices must 
    include, where applicable, an inspection of each incinerator at least 
    once per year. The final rule also clarifies that records of when 
    corrective actions were initiated and when the cause of the problem was 
    corrected must be maintained.
    
    V. Summary of Impacts
    
        The impacts estimated to be attributable to the final rule are the 
    same as those estimated to be attributable to the proposed rule. 
    Nationwide emissions of metal HAPs from mineral wool production cupolas 
    are estimated to be 1.0 Mg/yr (1.1 tpy) at the current level of 
    control. Existing PM emissions are estimated to be 239 Mg/yr (263 tpy). 
    Implementation of the final rule will reduce nationwide metal HAP and 
    PM emissions from existing cupolas by 0.91 Mg/yr (1.0 tpy) and 186 Mg/
    yr (205 tpy), respectively. Formaldehyde and phenol emissions from 
    existing curing ovens are estimated to be 54 Mg/yr (59 tpy) and 14 Mg/
    yr (16 tpy), respectively. Nationwide emissions of formaldehyde and 
    phenol will be reduced by about 30 Mg/yr (34 tpy) and 14 Mg/yr (16 
    tpy), respectively, as a result of this final rule. Although the EPA 
    does not anticipate any new cupolas or curing ovens within the next 
    five years, installation of a new cupola with a 7.3 megagram per hour 
    (8 ton per hour) capacity would result in estimated reductions of COS 
    and CO emissions by 104 Mg/yr (114 tpy) and 1,256 Mg/yr (1,384 tpy), 
    respectively, in addition to metal HAP and PM reductions.
        Because this rule is based on the use of fabric filters and thermal 
    incinerators, there are no water pollution impacts. Solid waste 
    generated by fabric filters in the form of ash is disposed of by 
    landfilling. With the addition of fabric filters to five cupolas, the 
    amount of solid waste is expected to increase by about 350 Mg/yr (390 
    tpy) from the current level of 24,800 Mg/yr (27,300 tpy) nationwide. 
    The rule is estimated to have no significant effect on energy 
    consumption.
        The total nationwide capital and annualized costs for existing 
    cupolas under the final rule are estimated to be $1.5 million and 
    $608,900/yr, respectively. These costs represent the addition of fabric 
    filters to five cupolas but do not include the monitoring costs of bag 
    leak detection systems required on all affected cupolas. Capital and 
    annualized costs for a bag leak detection system are estimated at 
    $9,100 and $1,800/yr for each affected cupola, respectively.
        The total nationwide capital cost of complying with the 
    requirements for existing curing ovens is estimated to be $795,800 with 
    a nationwide annual cost of $641,600. These costs result from the 
    addition of thermal incinerators to two curing ovens.
        Total nationwide capital costs for the standard are estimated at 
    $2.6 million and nationwide annual costs are estimated at $1.4 million, 
    including installation, operation, and maintenance of emission control 
    and monitoring systems.
        Under the final rule, market-level price increases are estimated to 
    range from 0.5 percent to 2.1 percent, resulting in quantity 
    adjustments of -0.59 percent and -1.71 percent, respectively. The 
    decreases in quantity demanded may lead to the loss of approximately 
    nine jobs. There is no indication that the costs associated with 
    achieving the reductions required by the final rule will cause facility 
    closure.
    
    VI. Summary of Responses to Major Comments
    
        The EPA proposed the NESHAP for the mineral wool production source 
    category on May 8, 1997 (62 FR 25370). A 60-day comment period from May 
    8, 1997 to July 7, 1997, was provided to accept written comments from 
    the public on the proposed rule.
        The EPA received a total of three comment letters regarding the 
    proposed NESHAP for mineral wool production. A copy of each comment 
    letter is available for public inspection in the docket for the 
    rulemaking (Docket No. A-95-33; see the ADDRESSES section of this 
    document for information on inspecting the docket). The EPA has had 
    follow-up discussions with commenters regarding specific issues 
    initially raised in their written comments that were submitted to the 
    EPA during the comment period. Copies of correspondence and other 
    information exchanged between the EPA and the commenters during the 
    post-comment period are available for public inspection in the docket 
    for the rulemaking.
        All of the comments received by the EPA were reviewed and carefully 
    considered by the EPA. Changes to the rule were made where the EPA 
    determined it to be appropriate. A summary of responses to major 
    comments received on the proposed rule is presented below. Additional 
    discussion of the EPA's responses to public comments is presented in 
    the document ``Summary of Public Comments and Responses on Mineral Wool 
    Production NESHAP'' (docket item V-C-2).
    
    A. General
    
        Comment: One commenter stated that there have been some shutdowns 
    in the industry that affect the information presented in the preamble 
    to the proposed rule. Currently, there are 15 mineral wool production 
    facilities located in eight states. Five of the 15 plants manufacture 
    bonded products and contain a total of ten cupolas and five curing 
    ovens. Ten active plants manufacture only nonbonded products, with a 
    total of 21 cupolas. Thus, the total industry currently operates 31 
    cupolas and five curing ovens, rather than the 36 cupolas and six 
    curing ovens reported by the EPA in the Federal Register document. The 
    commenter further stated that six of the ten companies in the mineral 
    wool production industry are small businesses, rather than seven of the 
    ten companies being small businesses as stated in the EPA's Federal 
    Register document.
        Response: The EPA acknowledges the information regarding shutdowns 
    and changes in the industry profile as noted by the commenter. The EPA 
    believes, however, that temporary shutdown of production lines is not 
    unusual in this industry because the manufacture of mineral wool 
    products is order-driven, and that these lines could be restarted in 
    the future. The EPA, therefore, has not made any changes to the 
    estimated impacts resulting from the rule. When considering these 
    changes in the industry profile, the technology representative of the 
    best controlled cupolas and curing ovens remains fabric filters and 
    thermal incinerators, respectively. Therefore, these changes do not 
    affect the proposed MACT floors for cupolas and curing ovens. Regarding 
    the number of small businesses within the source category, two separate 
    sources of information obtained by the EPA indicate that the company in 
    question has less than 750 employees. Thus, the EPA continues to 
    believe that seven of the ten mineral wool manufacturing companies are 
    small businesses. No revisions to the final rule are necessary as a 
    result of these comments.
    
    [[Page 29496]]
    
    B. Definitions
    
        Comment: One commenter suggested that the definition of ``bonded 
    product'' be amended to read ``Bonded product means mineral wool to 
    which a hazardous air pollutant-based binder (e.g., phenol, 
    formaldehyde) has been applied and cured.''
        Response: After consideration of this comment, the EPA has decided 
    to leave the definition of ``bonded product'' as it is in the proposed 
    rule to allow the broadest coverage of this term. Once binder has been 
    applied to mineral wool, whether cured or not, hazardous air 
    pollutants, which are the focus of the definition, have been introduced 
    into the production process.
        Comment: One commenter suggested that the definition of ``mineral 
    wool'' be amended to read ``Mineral wool means a fibrous glassy 
    substance made from natural rock (such as basalt), recycled blast 
    furnace slag, or a mixture of rock and slag; it may be used as a 
    thermal or acoustical insulation material or in the manufacturing of 
    other products to provide structural strength, sound absorbency, fire 
    resistance, or other uses.''
        Response: After consideration of this comment, the EPA has decided 
    to modify the definition of ``mineral wool'' by adding ``or other 
    required properties'' rather than ``or other uses'' as suggested by the 
    commenter. The EPA believes that this modification adequately expands 
    the definition of ``mineral wool'' as the commenter requested, as well 
    as provides more clarification than the commenter's suggested revision. 
    The EPA does not believe it is necessary or technically correct to add 
    ``recycled'' to the definition.
        Comment: One commenter suggested that the definition of ``cupola'' 
    be amended to read ``Cupola means a melting system consisting of raw 
    material bins, weighing and charging equipment, electrical power 
    system, controls, a large water cooled metal vessel with water cooling 
    system, combustion air fans, duct work, tuyeres and oxygen enrichment 
    system with combustion air preheater, molten slag handling and spinning 
    equipment, off gas duct work, fan and a structure to support and house 
    the melting system. The cupola is charged with a mixture of fuel, rock 
    and/or blast furnace slag and additives; as the fuel is burned, the 
    charged mixture is heated to a molten state, flows from the metal 
    vessel and is spun into mineral wool.''
        Response: After consideration of this comment, the EPA has decided 
    to leave the definition of ``cupola'' as it is in the proposed rule to 
    allow the broadest coverage of this term. The EPA does not agree that 
    all of the items in the commenter's suggested definition are part of a 
    cupola. It is the EPA's intention to define ``cupola'' in general terms 
    in order to cover all possible configurations. Some configurations may 
    not include all of the items included in the commenter's suggested 
    definition.
    
    C. Selection of Emission Standards
    
        Comment: One commenter strongly supported the subcategorization in 
    the proposed rule of plants with and without bonded lines. The 
    commenter further stated that it is within the EPA's authority under 
    the Act to define appropriate subcategories and that the differences 
    between plants with and without bonded lines are substantial and 
    consistent with the types of differences that the EPA has used to 
    subcategorize other source categories.
        Response: No changes in the final rule are necessary as a result of 
    this comment.
        Comment: One commenter supported the EPA's proposed MACT floor for 
    new and existing sources.
        Response: No changes in the final rule are necessary as a result of 
    this comment.
        Comment: One commenter strongly supported the EPA's proposed 
    decision not to require an incinerator as above the MACT floor control 
    for existing cupolas. Reasons cited by the commenter are that a cupola 
    incinerator requirement would be unduly costly and economically 
    devastating to an industry that produces an environmentally beneficial 
    product using a waste product that would otherwise be landfilled, that 
    a cupola incinerator requirement would not provide any significant 
    health benefits, and that a cupola incinerator may even have negative 
    net health impacts due to secondary emissions of nitrogen oxides 
    (NOX) and sulfur dioxide (SO2).
        Response: No changes in the final rule are necessary as a result of 
    this comment.
        Comment: One commenter stated that the EPA should require control 
    of CO and COS emissions from existing cupolas. The commenter further 
    stated that thermal oxidizers provide excellent control of cupola CO/
    COS emissions and that the EPA incorrectly concluded that the costs and 
    ancillary emissions from thermal oxidizers are too high for the EPA to 
    require their use on existing cupolas. The commenter stated that in 
    fact, thermal oxidizer costs have been declining in real terms, and 
    NOX emissions from thermal oxidizers currently are 
    guaranteed at very low levels. Further, the commenter believes that the 
    EPA's subcategorization of mineral wool production facilities based on 
    the production of bonded products, and leading to MACT floors for 
    cupola CO/COS emissions of no control, is inappropriate. Where 
    subcategorization does not result in distinct emission limits or 
    floors, the commenter believes that regulatory simplicity dictates that 
    it should be avoided. The commenter also believes that the MACT floor 
    for existing cupolas does call for thermal oxidizer-based limits given 
    that the MACT floor level of control would be the use of thermal 
    incineration or its equivalent in the absence of subcategorization.
        Response: The EPA disagrees that subcategorization is either 
    prohibited by the statute or unwise as a policy matter. While 
    regulatory simplicity may be a consideration in how the EPA exercises 
    its discretion, the statute does not dictate that this consideration 
    supersede other legitimate considerations in establishing 
    subcategories. As the EPA has noted in several rulemakings, the Act 
    provides the EPA with substantial discretion to consider various 
    factors when determining whether subcategorization is appropriate (see, 
    e.g., 59 FR 29196-29200, June 6, 1994, Federal Register notice on 
    determination of MACT floor for medium storage vessels at facilities 
    subject to the hazardous organic NESHAP which indicates that the EPA 
    may consider whether production processes used at different sources are 
    sufficiently distinct to justify the creation of a subcategory).
        In considering whether it is appropriate to subcategorize in this 
    rule, the EPA continues to believe the basis for subcategorizing stated 
    in the preamble to the proposed rule is valid (see 62 FR 25376-25377, 
    May 8, 1997). Another commenter supported the EPA's view that it has 
    substantial discretion to subcategorize and agreed with the EPA's 
    decision to subcategorize in the proposed rule. Further, the EPA has 
    taken several steps to accomplish the goal of regulatory simplicity in 
    this rulemaking. For example, the EPA has emphasized readability in the 
    plain language format of the final rule. In addition, the EPA has 
    promulgated the cupola standards in one section, rather than in 
    separate sections for each subcategory. Therefore, the EPA believes it 
    has accomplished the goal of making the regulations as simple as 
    possible while at the same time recognizing appropriate distinctions 
    between the different types of facilities in the industry through 
    subcategorization.
    
    [[Page 29497]]
    
        Regarding the commenter's statement about thermal oxidizer costs 
    and ancillary emissions, the commenter did not provide any cost or 
    NOX emissions data to substantiate the assertion that a 
    requirement to install thermal oxidizers on existing cupolas would be 
    cost effective. The EPA continues to believe that the data in the 
    record does not indicate that CO/COS controls are cost effective or 
    otherwise appropriate for either subcategory. The EPA has not made any 
    changes to the rule as a result of these comments.
        Comment: One commenter supported the EPA's proposing thermal 
    incineration as the MACT floor for both new and existing curing ovens 
    and new cupolas. The commenter further stated that significantly higher 
    control efficiencies can be achieved beyond the 80 percent discussed in 
    the proposed rule with the use of catalytic incineration or oxidation 
    and, in fact, volatile organic compound (VOC) reductions in excess of 
    98 percent can be achieved. According to the commenter, catalytic 
    oxidation is a cost-effective control option which has been used for 
    many years in diverse applications and the commenter believes that 
    significant further VOC reductions can be cost-effectively achieved by 
    using the technology to also control the emissions from existing 
    cupolas. The commenter stated that catalytic incineration minimizes the 
    temperature required for the destruction of VOCs and consequently, 
    minimizes the production of NOX and sulfur oxide 
    (SOX) emissions from the combustion of sulfur bearing fuels. 
    Another commenter stated that thermal oxidizers or equivalent controls 
    can easily provide the proposed 80 percent reduction in curing oven 
    formaldehyde emissions and suggested that the EPA mention the 
    capabilities of regenerative thermal oxidizers to reduce fuel costs in 
    the preamble to the final rule.
        Response: Neither commenter provided costs or data indicating 
    destruction efficiency of catalytic oxidizers or regenerative thermal 
    oxidizers on a mineral wool cupola or curing oven. In addition, 
    catalytic oxidizers and regenerative thermal oxidizers are not 
    demonstrated in the mineral wool production industry. The proposed 80 
    percent reduction in curing oven formaldehyde emissions is based upon 
    test data from a recuperative thermal incinerator representative of 
    MACT for curing ovens in the mineral wool production industry. The EPA 
    has not made any changes to the rule as a result of these comments.
        Comment: One commenter recommended that the proposed PM emission 
    standard for existing cupolas be increased significantly from the 
    proposed limit of 0.06 lb/ton of melt to 0.9 lb/ton to ensure that 
    cupolas equipped with a fabric filter (also known as a baghouse) can 
    comply with the standard. The commenter believes that emissions tests 
    upon which the EPA based the proposed PM standard involved invalid 
    tests that resulted in unrepresentative PM emission levels. According 
    to the commenter, the baghouse had defects that resulted in the 
    improper influx of air into the outlet stream, thereby diluting the 
    observed PM emission level. The commenter stated that approximately 70-
    90 percent more air was emitted at the outlet than entered the intake 
    and that this defect prevents the test results from being used to 
    establish emission levels representative of a properly functioning 
    baghouse. The commenter also noted that the baghouse differential 
    pressures varied widely during the emissions tests, which could 
    indicate a number of problems with the baghouse including air leaks or 
    problems with bag cleaning.
        Response: The commenter's request to increase the proposed PM 
    emission standard to ensure that cupolas equipped with fabric filters 
    can comply with the standard indicates a misunderstanding of the nature 
    of section 112 of the Act, as well as the MACT determination process, 
    which requires that emission standards for existing sources be set not 
    less stringent than the level achieved by the average of the best 
    performing five sources for categories or subcategories with fewer than 
    30 sources. This determination is made assuming that some sources will 
    need to install new emission controls or improve performance of their 
    existing controls to meet a standard that is not less stringent than 
    the MACT floor.
        Regarding the commenter's statement that baghouse defects resulted 
    in improper influx of air into the outlet stream and dilution of the PM 
    emission level, dilution air is of no significance given that the 
    proposed PM emission standard is in pounds of PM per ton of melt. 
    Emissions data from the baghouse-controlled cupola indicates a PM 
    removal efficiency of about 99.8 percent, and therefore, casts doubt 
    upon the commenter's assertion that the data are not representative of 
    a properly functioning baghouse. In addition, EPA believes that if the 
    commenter's statement about baghouse operational problems during the 
    emissions testing upon which the proposed PM standard is based 
    accurately assessed the situation, then the emission test results would 
    be biased high and the emission standard would, therefore, be biased 
    high. This certainly does not support raising the limit to an even 
    higher level. When provided the opportunity to review the emissions 
    test report, the facility did not have any comments regarding baghouse 
    defects resulting in the improper influx of air into the outlet stream 
    and diluted PM emission levels. Furthermore, when the EPA discussed the 
    proposed PM emission standard of 0.06 lb/ton with industry 
    representatives and State and local environmental agency 
    representatives prior to proposal, no concerns were expressed. In 
    addition, the commenter provided no basis for a PM emission standard of 
    0.9 lb/ton of melt. Based on the above discussion, the EPA has not made 
    any changes to the proposed PM emission standard as a result of these 
    comments.
        During a follow-up meeting with the commenter (see Docket Item IV-
    E-1), held at the commenter's request to provide an opportunity to 
    present to the EPA clarification of the comments and issues of concern 
    regarding the proposed emission standards, the commenter provided the 
    EPA with additional PM emissions data from fabric filter-controlled 
    cupolas. These data are from the Emission Factor Documentation for AP-
    42 Section 8.16, Mineral Wool Manufacturing. These PM data are from 
    three fabric filter-controlled cupolas at the same facility as the 
    fabric filter-controlled cupola upon which the EPA based its proposed 
    PM emission standard. Because the parameters for these three fabric 
    filters are the same as those parameters previously determined to be 
    representative of the MACT floor for existing and new sources and 
    because these cupolas are at the same facility as the cupola tested by 
    the EPA and would therefore experience similar operating and 
    maintenance practices, the EPA has decided that the PM data from these 
    three fabric filter-controlled cupolas should be considered in 
    development of the final rule. When data from these three additional 
    fabric filter-controlled cupolas are included in the data base, PM data 
    representative of the MACT floor for cupolas now consists of the 
    following: 0.04 lb/ton, 0.05 lb/ton, 0.065 lb/ton, and 0.099 lb/ton. 
    Based on these data, the EPA has determined that a PM emission limit of 
    0.10 lb/ton represents a level that can be achieved by all four cupolas 
    controlled with well designed, operated, and maintained fabric filters, 
    and is representative of the MACT floor in the final rule.
        Comment: One commenter stated that emissions data from the second 
    facility in the EPA test program indicate that PM emissions from a 
    cupola also
    
    [[Page 29498]]
    
    controlled with a baghouse averaged 0.6 lb/ton of melt, an order of 
    magnitude higher than the proposed PM standard of 0.06 lb/ton. Thus, 
    emissions from this facility would not meet the EPA's proposed PM 
    emission standard, even though the facility is equipped with the 
    control technology that represents the MACT floor. The commenter 
    acknowledged that the PM emissions data from this facility includes 
    emissions from both the cupola and fiber collection process but stated 
    that the facility is nevertheless required to meet the emission limit 
    set by the EPA. The commenter further stated that at least one other 
    mineral wool company vents the fiber collection process as well as the 
    cupola through a baghouse and it would be infeasible for this facility 
    to meet the proposed PM standard. Further, it would be very expensive 
    and counter-productive with respect to emission levels to force the 
    facility to rearrange its baghouse operation to exclude the fiber 
    collection process air. Because it is possible that the collection 
    chamber may require additional PM controls in the future as a result, 
    for example, of the EPA's recently proposed PM2.5 ambient 
    standard, an additional reason to set the cupola PM emission standard 
    at a higher level is therefore to permit the facility to meet the 
    proposed PM emission standard with its current configuration, and to 
    provide other companies additional flexibility to reduce PM emissions 
    in the future.
        Response: The EPA cannot foresee or accommodate all configurations 
    of processes ducted to a common control device. Section 63.7 of the 
    general provisions in subpart A of 40 CFR part 63 allows the use of 
    alternative test methods and procedures based on review and approval by 
    the EPA of relevant supporting information. The supporting data and 
    information are submitted as part of the site specific test plan and 
    are evaluated for approval by the EPA on a case-by-case basis. Because 
    all facilities have the opportunity to request alternative methods and 
    procedures for testing and demonstrating compliance with the cupola 
    emission standards, the EPA again believes the proposed PM emission 
    standard should not be raised to consider emissions not regulated by 
    the MACT standards, and has therefore, not made any changes to the rule 
    as a result of these comments.
        Comment: One commenter stated that other mineral wool manufacturing 
    companies indicated that a 0.06 lb/ton PM standard would not be 
    feasible with their existing installed baghouse controls. Earlier data 
    collected by the EPA as part of a screening study not associated with 
    the MACT standards development process found controlled particulate 
    emissions from industry tests of six mineral wool cupolas equipped with 
    baghouses ranged from 0.0044 to 0.70 lb/ton, while the average 
    controlled emission level was 0.42 lb/ton. The commenter further stated 
    that because most if not all mineral wool facilities will be unable to 
    meet the proposed 0.06 lb/ton of melt PM standard on a consistent 
    basis, the proposed standard is inconsistent with the intended 
    objective of basing the standard on the existing baghouse technology 
    installed by many facilities that represent the MACT floor.
        Response: The EPA reviewed the 1980 document ``Source Category 
    Survey: Mineral Wool Manufacturing Industry'' which contains the 
    earlier data referred to by the commenter. Upon review, it was noted 
    that only one facility with a cupola controlled by a baghouse as 
    referenced in the 1980 report is still operational and it is not 
    apparent from the study what the PM emissions associated with the 
    cupola at this facility were. It is apparent, however, from an 
    information collection request response submitted by this facility to 
    the EPA in 1993, that new baghouses were installed in 1986 and 1987 for 
    each of their two operating cupolas. Thus, the test data supplied by 
    this facility for the 1980 study is not relevant. The commenter did not 
    provide any data on baghouse design, maintenance, or operation 
    characteristics to show that the facilities tabulated in the 1980 study 
    were representative of MACT.
        The commenter's statement that the proposed standard is 
    inconsistent with the intended objective of basing the standard on the 
    existing baghouse technology installed by many facilities that 
    represent the MACT floor mischaracterizes the intent of the EPA and of 
    section 112 of the Act. As previously stated, the statute requires the 
    level of control to be not less stringent than the average level 
    achieved by the best performing five sources, rather than be based on 
    what all facilities can achieve with their current control and 
    maintenance practices. The Act, through requiring all sources to meet a 
    standard that is not less stringent than the MACT floor, assumes that 
    existing controls may need to be replaced or upgraded at some sources. 
    In many cases, bags within the fabric filter may need to be replaced 
    and a more rigorous operation and maintenance plan may be necessary to 
    meet the MACT. Accordingly, the EPA has decided that no changes in the 
    final rule are necessary as a result of these comments.
        Comment: One commenter recommended that the proposed formaldehyde 
    emission standard for existing curing ovens be increased significantly 
    from 0.06 pounds of formaldehyde per ton of melt (lb/ton) to 0.4 lb/ton 
    because the commenter has concerns that the proposed standard may not 
    be consistently achieved by an incinerator on the curing oven. The 
    commenter stated that for example, the EPA's data from one tested 
    facility (Facility B) showed that formaldehyde emissions from a curing 
    oven equipped with an incinerator were 0.4 lb/ton, which is almost an 
    order of magnitude above the proposed formaldehyde standard. The 
    commenter acknowledged that the EPA's background documentation explains 
    that only a portion of Facility B's curing oven exhaust passes through 
    the high temperature incinerator but nevertheless, the input 
    formaldehyde concentration into Facility B's curing oven incinerator 
    was still over six times higher (1.3 lb/ton) than the low measured 
    formaldehyde input at the facility upon which the proposed emission 
    standard is based (0.2 lb/ton) (Facility A). The commenter stated that 
    because the Facility A input level was abnormally low, the low output 
    after incineration may also not be representative of other curing 
    ovens. The commenter further stated that assuming Facility B's curing 
    oven incinerator is the least efficient of the three curing oven 
    incinerators existing in the industry, Facility B would be the median 
    of the 5 curing ovens remaining in the industry. Thus, the commenter 
    concluded that the MACT floor should be set at the emission limit 
    corresponding to Facility B's curing oven incinerator.
        Response: While the commenter characterizes the input formaldehyde 
    concentration into Facility A's curing oven incinerator as strikingly 
    low relative to the input formaldehyde concentration into Facility B's 
    curing oven incinerator, the commenter did not submit data to indicate 
    that the emissions measured for Facility A's curing oven incinerator 
    are in error. The EPA recognized the potential variability in input 
    formaldehyde, and for this reason proposed an alternative emission 
    standard, also based on Facility A, requiring reduction of uncontrolled 
    formaldehyde emissions by at least 80 percent. Regarding the 
    commenter's concern that the proposed standards may not be consistently 
    achieved by an incinerator, another commenter indicated that thermal 
    oxidizers or equivalent controls can easily provide
    
    [[Page 29499]]
    
    the proposed 80 percent reduction in curing oven formaldehyde 
    emissions. Furthermore, in the preamble to the proposed national 
    emission standards for hazardous air pollutants for wool fiberglass 
    manufacturing (62 FR 15228), the EPA stated that emission test 
    measurements demonstrate that a thermal incinerator installed at these 
    facilities is at least 99 percent effective in the removal of 
    formaldehyde and phenol from curing ovens. Additionally, under the 
    relevant emission standard for Facility B, 80 percent removal would 
    translate into a limit of 0.26 lb/ton of melt, not 0.4 lb/ton of melt 
    as proposed by the commenter.
        Originally, Facility A's curing oven incinerator was selected as 
    being representative of the MACT floor for existing sources and 
    Facility B's curing oven incinerator was selected as being 
    representative of MACT for new sources. These determinations were based 
    on incinerator operating temperatures and gas residence times. After 
    emissions testing was completed, the EPA decided to discount the data 
    from Facility B because the curing oven incinerator was not operating 
    properly as evidenced by a low formaldehyde removal efficiency of about 
    69 percent. Also, discussions with Facility B personnel revealed that 
    gas flows within the curing oven were not within design parameters 
    during the emissions test. Based on the above information, the EPA 
    determined that Facility A's curing oven incinerator represented MACT 
    for existing and new sources. Accordingly, other facilities with curing 
    ovens, including Facility B, will be required to install new 
    incinerators, or replace or modify their existing incinerators, as 
    necessary, to meet the curing oven formaldehyde emission standards. 
    After consideration of these comments, the EPA has decided to leave the 
    formaldehyde emissions standards at 0.06 lb/ton of melt and 80 percent 
    reduction of uncontrolled formaldehyde as in the proposed rule.
        Comment: One commenter recommended that the EPA include an emission 
    limit for COS of 0.05 pounds of COS per ton of melt (lb/ton) as an 
    alternative to proposed emission standards for new cupolas of 0.10 
    pounds of CO per ton of melt (lb/ton) or 99 percent CO removal. The 
    commenter stated that this alternative emission limit would give new 
    sources in the future the flexibility to explore alternative methods to 
    reduce COS through process modifications or other approaches. The 
    commenter further stated that while they are not aware of any feasible 
    process modifications that can significantly reduce COS at this time, 
    it is possible that alternative designs or processes that reduce COS 
    emissions may be developed in the future that could be feasible for a 
    new plant. The commenter believes that because the relationship between 
    CO and COS involves some fluctuation and uncertainty, a direct COS 
    alternative would be helpful to encourage exploration of such 
    alternative means of compliance in any future new mineral wool plants.
        Response: During development of the cupola emission standards, the 
    EPA considered including an emission standard for COS for plants that 
    choose to use process modifications, rather than thermal incineration, 
    as a means of reducing COS emissions from new cupolas. When the EPA 
    discussed this option with industry representatives, they considered 
    this approach and strongly indicated, as the commenter does, that there 
    are no feasible process modifications capable of reducing COS emissions 
    to the level contemplated for a standard. In addition, the commenter 
    provided no basis for a COS emission standard of 0.05 lb/ton of melt. 
    Accordingly, the EPA has not made any changes to the rule as a result 
    of this comment.
    
    D. Monitoring
    
        Comment: One commenter expressed concern that the monitoring 
    equipment for baghouses required to meet the proposed PM standard is 
    overly sensitive, would be unduly costly, and would trigger false 
    alarms. The commenter recommended revising the bag leak detection 
    system specifications from 1 milligram per cubic meter (mg/m\3\) to 10 
    mg/m\3\ in order to be consistent with other MACT standards, such as 
    the secondary lead standard where the minimum detection capability of 
    the bag leak detection system was revised from 1 to 10 mg/m\3\.
        Response: After consideration of this comment, the EPA has decided 
    to modify the required minimum detection capability for bag leak 
    detection systems to 10 mg/m\3\ (0.0044 gr/ft\3\). This change does not 
    alter the intended function of the bag leak detector, which is to 
    detect broken bags or other defects in baghouses, and is consistent 
    with the specification for sensitivity in other EPA standards.
        Comment: One commenter suggested that the EPA allow the use of 
    opacity monitors for bag leak detection because these monitors comply 
    with Performance Specification 1 of Appendix B of 40 CFR part 60, and 
    have been used for many years on electric arc furnace baghouses where 
    the opacity limit is set at 3 percent.
        Response: The commenter did not submit data to prove that opacity 
    monitors are as sensitive as bag leak detection systems or can meet 
    their minimum detection capability specification. The facts that 
    opacity monitors comply with Performance Specification 1 of Appendix B 
    of 40 CFR part 60 and that opacity monitors have been used on electric 
    arc furnace baghouses are no indication that opacity monitors are 
    suitable for use on cupola baghouses. The EPA continues to believe that 
    a bag leak detection system will provide the best indication of cupola 
    baghouse performance at the low PM levels characteristic of these 
    sources. The EPA has not made any changes to the rule as a result of 
    this comment.
    
    E. Recordkeeping and Reporting
    
        Comment: One commenter stated that although they agree with the 
    need for startup, shutdown, and malfunction plans, the proposed rule 
    does not clearly provide that emissions may temporarily exceed the 
    emission limits during startup, shutdown, or malfunctions. The 
    commenter recommended that the proposed rule should therefore specify 
    that emission limits may be temporarily exceeded during startup, 
    shutdown, or malfunctions without violating the standard provided the 
    company is taking appropriate actions consistent with its startup, 
    shutdown, and malfunction plan. The commenter further recommended that 
    the EPA should provide some flexibility in the rule for unexpected 
    developments and upsets that are difficult to predict and control in 
    the mineral wool industry. The commenter stated that there is no 
    practical or legal reason why a single perceived deviation from a 
    defined operating range should be deemed to be out of compliance, but 
    rather, some margin of error should be permitted in the form of one or 
    two allowable excursions per month.
        Response: Section 63.6(f) of the general provisions in subpart A of 
    40 CFR part 63 provides that nonopacity emission standards shall apply 
    at all times except during periods of startup, shutdown, and 
    malfunction. The situation the commenter describes regarding unexpected 
    developments and upsets are covered under the definition of a 
    malfunction in the general provisions provided the failures are not 
    caused in part by poor maintenance or careless operation. The EPA, 
    therefore, does not believe that an additional provision in the form of 
    one or two allowable excursions per month is warranted. The EPA has 
    specified in the
    
    [[Page 29500]]
    
    final rule, however, that the owner or operator must comply with the 
    standards at all times except during periods of startup, shutdown, or 
    malfunction.
    
    VII. Administrative Requirements
    
    A. Docket
    
        The docket is intended to be an organized file of the 
    administrative records compiled by the EPA. The docket is a dynamic 
    file because information is added throughout the rulemaking 
    development. The docketing system is intended to allow members of the 
    public and industries involved to readily identify and locate documents 
    so that they can effectively participate in the rulemaking process. 
    Along with the proposed and promulgated standards and their preambles, 
    the docket will contain the record in case of judicial review. (See 
    section 307(d)(7)(A) of the Act.) The location of the docket, which 
    includes all public comments received on the proposed rule, is in the 
    ADDRESSES section at the beginning of this preamble.
    
    B. Executive Order 12866--Regulatory Planning and Review
    
        Under Executive Order 12866 (58 FR 51735, October 4, 1993), the EPA 
    must determine whether the regulatory action is ``significant'' and 
    therefore subject to review by the Office of Management and Budget 
    (OMB) and the requirements of the Executive Order. The Executive Order 
    defines ``significant regulatory action'' as one that is likely to 
    result in a rule that may:
        (1) Have an annual effect on the economy of $100 million or more or 
    adversely affect in a material way the economy, a sector of the 
    economy, productivity, competition, jobs, the environment, public 
    health or safety, or State, local, or tribal governments or 
    communities;
        (2) create a serious inconsistency or otherwise interfere with an 
    action taken or planned by another agency;
        (3) materially alter the budgetary impact of entitlements, grants, 
    user fees, or loan programs, or the rights and obligations of 
    recipients thereof; or
        (4) raise novel legal or policy issues arising out of legal 
    mandates, the President's priorities, or the principles set forth in 
    the Executive Order.
        It has been determined that this action is not a ``significant 
    regulatory action'' under the terms of the Executive Order and is 
    therefore not subject to OMB review.
    
    C. Executive Order 12875--Enhancing the Intergovernmental Partnership
    
        Under Executive Order 12875, the EPA may not issue a regulation 
    that is not required by statute and that creates a mandate upon a 
    State, local or tribal government, unless the Federal government 
    provides the funds necessary to pay the direct compliance costs 
    incurred by those governments, or the EPA consults with those 
    governments. If the EPA complies by consulting, Executive Order 12875 
    requires the EPA to provide to the OMB a description of the extent of 
    the EPA's prior consultation with representatives of affected State, 
    local and tribal governments, the nature of their concerns, copies of 
    any written communications from the governments, and a statement 
    supporting the need to issue the regulation. In addition, Executive 
    Order 12875 requires the EPA to develop an effective process permitting 
    elected officials and other representatives of State, local and tribal 
    governments ``to provide meaningful and timely input in the development 
    of regulatory proposals containing significant unfunded mandates.''
        Today's rule does not create a mandate on State, local or tribal 
    governments. The rule does not impose any enforceable duties on State, 
    local or tribal governments, because they do not own or operate any 
    sources that would be subject to this rule. Accordingly, the 
    requirements of section 1(a) of Executive Order 12875 do not apply to 
    this rule.
    
    D. Executive Order 13084--Consultation and Coordination With Indian 
    Tribal Governments
    
        Under Executive Order 13084, the EPA may not issue a regulation 
    that is not required by statute, that significantly or uniquely affects 
    the communities of Indian tribal governments, and that imposes 
    substantial direct compliance costs on those communities, unless the 
    Federal government provides the funds necessary to pay the direct 
    compliance costs incurred by the tribal governments, or the EPA 
    consults with those governments. If the EPA complies by consulting, 
    Executive Order 13084 requires the EPA to provide to the OMB, in a 
    separately identified section of the preamble to the rule, a 
    description of the extent of the EPA's prior consultation with 
    representatives of affected tribal governments, a summary of the nature 
    of their concerns, and a statement supporting the need to issue the 
    regulation. In addition, Executive Order 13084 requires the EPA to 
    develop an effective process permitting elected officials and other 
    representatives of Indian tribal governments ``to provide meaningful 
    and timely input in the development of regulatory policies on matters 
    that significantly or uniquely affect their communities.''
        Today's rule does not significantly or uniquely affect the 
    communities of Indian tribal governments. No affected facilities are 
    owned or operated by Indian tribal governments. Accordingly, the 
    requirements of section 3(b) of Executive Order 13084 do not apply to 
    this rule.
    
    E. Unfunded Mandates Reform Act
    
        Title II of the Unfunded Mandates Reform Act of 1995 (UMRA), Pub. 
    L. 104-4, establishes requirements for Federal agencies to assess the 
    effects of their regulatory actions on State, local, and tribal 
    governments and the private sector. Under section 202 of the UMRA, the 
    EPA generally must prepare a written statement, including a cost-
    benefit analysis, for proposed and final rules with ``Federal 
    mandates'' that may result in expenditures by State, local, and tribal 
    governments, in the aggregate, or by the private sector, of $100 
    million or more in any one year. Before promulgating an EPA rule for 
    which a written statement is needed, section 205 of the UMRA generally 
    requires the EPA to identify and consider a reasonable number of 
    regulatory alternatives and adopt the least costly, most cost-effective 
    or least burdensome alternative that achieves the objectives of the 
    rule. The provisions of section 205 do not apply when they are 
    inconsistent with applicable law. Moreover, section 205 allows the EPA 
    to adopt an alternative other than the least costly, most cost-
    effective or least burdensome alternative if the Administrator 
    publishes with the final rule an explanation why that alternative was 
    not adopted. Before the EPA establishes any regulatory requirements 
    that may significantly or uniquely affect small governments, it must 
    have developed under section 203 of the UMRA a small government agency 
    plan. The plan must provide for notifying potentially affected small 
    governments, enabling officials of affected small governments to have 
    meaningful and timely input in the development of EPA regulatory 
    proposals with significant Federal intergovernmental mandates, and 
    informing, educating, and advising small governments on compliance with 
    the regulatory requirements.
        The EPA has determined that this rule does not contain a Federal 
    mandate that may result in expenditures of $100
    
    [[Page 29501]]
    
    million or more for State, local, and tribal governments, in the 
    aggregate, or the private sector in any one year. The EPA projects that 
    annual economic impacts would be far less than $100 million. Thus, 
    today's rule is not subject to the requirements of sections 202 and 205 
    of the UMRA. In addition, the EPA has determined that this rule 
    contains no regulatory requirements that might significantly or 
    uniquely affect small governments because it does not impose any 
    enforceable duties on small governments; such governments own or 
    operate no sources subject to the rule and therefore would not be 
    required to purchase control systems to meet the requirements of the 
    rule.
    
    F. Regulatory Flexibility
    
        The Regulatory Flexibility Act (RFA) generally requires an agency 
    to conduct a regulatory flexibility analysis of any rule subject to 
    notice and comment rulemaking requirements unless the agency certifies 
    that the rule will not have a significant economic impact on a 
    substantial number of small entities. Small entities include small 
    businesses, small not-for-profit enterprises, and small governmental 
    jurisdictions. The EPA has determined that seven of the ten firms that 
    potentially would be subject to the final rule are small firms. The EPA 
    has met with all of these small firms and their trade association. They 
    have been fully involved in this rulemaking and their concerns and 
    comments have been considered in the development of this rule. Also, a 
    representative of the EPA's Office of the Small Business Ombudsman 
    participated in the development of these standards as a work group 
    member to ensure that the requirements of the standards were examined 
    for potential adverse economic impacts and those impacts were mitigated 
    to the extent feasible while still achieving the rule's environmental 
    objectives.
        Five of the seven small firms would incur emission control costs 
    that are less than 0.1 percent of sales; one firm would incur control 
    costs estimated to be 2.4 percent of the firm's sales; and another firm 
    would incur control costs believed to be in excess of 3 percent. (See 
    Docket Item II-A-16 for a discussion of this analysis.) Thus, this rule 
    affects only a small number of small businesses. Further, most of the 
    small businesses impacted by this rule will experience minimal 
    increases in costs. Only two small businesses are projected to incur 
    costs exceeding 0.1 percent of sales.
    
    G. Submission to Congress and the Comptroller General
    
        The Congressional Review Act, 5 U.S.C. 801 et seq., as added by the 
    Small Business Regulatory Enforcement Fairness Act of 1996, generally 
    provides that before a rule may take effect, the agency promulgating 
    the rule must submit a rule report, which includes a copy of the rule, 
    to each House of the Congress and to the Comptroller General of the 
    United States. The EPA will submit a report containing this rule and 
    other required information to the U.S. Senate, the U.S. House of 
    Representatives, and the Comptroller General of the United States prior 
    to publication of the rule in the Federal Register. This action is not 
    a ``major rule'' as defined by 5 U.S.C. 804(2). This rule will be 
    effective June 1, 1999.
    
    H. Paperwork Reduction Act
    
        The OMB has approved the information collection requirements 
    contained in this rule under the provisions of PRA, 44 U.S.C. 3501 et 
    seq. and has assigned OMB control number 2060-0362.
        The information collection requirements include the notification, 
    recordkeeping, and reporting requirements of the NESHAP general 
    provisions, authorized under section 114 of the Act, which are 
    mandatory for all owners and operators subject to national emission 
    standards. All information submitted to the EPA for which a claim of 
    confidentiality is made is safeguarded according to EPA policies in 40 
    CFR part 2, subpart B. This rule does not require any notifications or 
    reports beyond those required by the general provisions. Subpart DDD 
    does require additional records of specific information needed to 
    determine compliance with the rule. These include records of: (1) 
    Cupola production (melt) rate; (2) all bag leak detection system 
    alarms, the date and time of the alarm, when corrective actions were 
    initiated, the cause of the alarm, an explanation of the corrective 
    actions taken, and when the cause of the alarm was corrected; (3) the 
    free-formaldehyde content of each resin lot and the binder formulation, 
    including formaldehyde content, of each binder batch used in the 
    manufacture of bonded products; and (4) incinerator operating 
    temperature, including all periods when the average temperature in any 
    three-hour block period fell below the average temperature established 
    during the performance test, and the results of the annual inspection, 
    including any problems discovered during the inspection, the date and 
    time of the problem, when corrective actions were initiated, the cause 
    of the problem, an explanation of the corrective actions taken, and 
    when the cause of the problem was corrected. Each of these information 
    requirements is needed to determine compliance with the standards.
        The annual public reporting and recordkeeping burden to industry 
    for this collection is estimated to be 6,107 labor hours per year at an 
    annual cost of $196,206. This estimate includes a one-time performance 
    test and report (with repeat tests where needed); one-time preparation 
    of a startup, shutdown, and malfunction plan with semiannual reports of 
    any event in which the procedures were not followed; preparation of an 
    operations, maintenance, and monitoring plan; semiannual excess 
    emissions reports; notifications; and recordkeeping. The total capital 
    cost associated with the monitoring requirements is estimated to be 
    $309,400. This estimate includes the capital and startup costs 
    associated with installation of a bag leak detection system for each 
    affected cupola. The annualized cost of that capital is $44,059 per 
    year, and the operation and maintenance of the monitoring equipment is 
    estimated to be $17,000 per year.
        Burden means the total time, effort, or financial resources 
    expended by persons to generate, maintain, retain, or disclose or 
    provide information to or for a Federal agency. This includes the time 
    needed to review instructions; develop, acquire, install, and utilize 
    technology and systems for the purposes of collecting, validating, and 
    verifying information, processing and maintaining information, and 
    disclosing and providing information; adjust the existing ways to 
    comply with any previously applicable instructions and requirements; 
    train personnel to be able to respond to a collection of information; 
    search data sources; complete and review the collection of information; 
    and transmit or otherwise disclose the information.
        An Agency may not conduct or sponsor, and a person is not required 
    to respond to, a collection of information unless it displays a 
    currently valid OMB control number. The OMB control numbers for EPA's 
    regulations are listed in 40 CFR part 9 and 48 CFR chapter 15. In 
    compliance with the Paperwork Reduction Act (PRA), the EPA is amending 
    the table in 40 CFR part 9 of currently approved information collection 
    request (ICR) control numbers issued by the OMB for various 
    regulations.
    
    [[Page 29502]]
    
        This amendment updates the table to accurately display those 
    information requirements contained in this final rule. The EPA will 
    continue to present OMB control numbers in a consolidated table format 
    to be codified in 40 CFR part 9 of the EPA's regulations, and in each 
    Code of Federal Regulations volume containing EPA regulations. The 
    table lists the section numbers with reporting and recordkeeping 
    requirements, and the current OMB control numbers. This display of the 
    OMB control number and its subsequent codification in the CFR satisfy 
    the requirements of the PRA (44 U.S.C. 3501 et seq.) and OMB's 
    implementing regulations at 5 CFR part 1320.
        The ICR was previously subject to public notice and comment prior 
    to OMB approval. As a result, the EPA finds there is ``good cause'' 
    under section 553(b)(3)(B) of the Administrative Procedures Act (5 
    U.S.C. 553(b)(3)(B)) to amend this table without prior notice and 
    comment. Due to the technical nature of the table, further notice and 
    comment would be unnecessary. For the same reasons, the EPA also finds 
    that there is good cause under 5 U.S.C. 553(d)(3).
    
    I. Pollution Prevention Act
    
        The Pollution Prevention Act of 1990 states that pollution should 
    be prevented or reduced at the source whenever feasible. During the 
    development of these standards, the EPA explored opportunities to 
    eliminate or reduce emissions through the application of new processes 
    or work practices. By reducing or eliminating the formaldehyde and 
    phenol in binder formulations, HAPs from the curing process would be 
    reduced or eliminated without the use of air pollution control 
    equipment. Alternative binders have been investigated by various 
    mineral wool producers. Acceptable alternatives have been difficult to 
    identify due to the higher costs of the potential alternative binders; 
    the problems associated with requalification of altered products to 
    meet required product specifications; the production process changes 
    necessitated by the use of modified binders; and the concerns regarding 
    potential toxicity of new binder ingredients. Thus, at this time an 
    acceptable alternative binder has not been commercially demonstrated.
    
    J. National Technology Transfer and Advancement Act
    
        Section 12(d) of the National Technology Transfer and Advancement 
    Act (NTTAA), Pub. L. 104-113 (March 7, 1996), directs the EPA to use 
    voluntary consensus standards in regulatory and procurement activities 
    unless to do so would be inconsistent with applicable law or otherwise 
    impractical. Voluntary consensus standards are technical standards 
    (such as materials specifications, test methods, sampling procedures, 
    and business practices) which are developed or adopted by voluntary 
    consensus standard bodies. Where available and potentially applicable 
    voluntary consensus standards are not used by EPA, the Act requires the 
    Agency to provide Congress, through the OMB, an explanation for not 
    using such standards. This section summarizes the EPA's response to the 
    requirements of the NTTAA for the analytical test methods promulgated 
    as part of this final rule.
        Consistent with the NTTAA, the EPA conducted searches to identify 
    voluntary consensus standards for the EPA's emissions sampling and 
    analysis reference methods and industry recommended materials analysis 
    procedures cited in this rule. Candidate voluntary consensus standards 
    for materials analysis were identified for free-formaldehyde content. 
    Consensus comments provided by industry experts were that the candidate 
    standards did not meet industry materials analysis requirements. 
    Therefore, EPA has determined these voluntary consensus standard are 
    impractical for the mineral wool production NESHAP. The EPA, in 
    consultation with the North American Insulation Manufacturers 
    Association (NAIMA), has formulated an industry-specific materials 
    analysis, consensus standard for free-formaldehyde content which is 
    promulgated in this rule.
        The EPA search to identify voluntary consensus standards for the 
    EPA's emissions sampling and analysis reference methods cited in this 
    rule identified 17 voluntary consensus standards that appeared to have 
    possible use in lieu of EPA standard reference methods. However, after 
    reviewing available standards, EPA determined that 12 of the candidate 
    consensus standards identified for measuring emissions of the HAPs or 
    surrogates subject to emission standards in the rule would not be 
    practical due to lack of equivalency, documentation, validation data 
    and other important technical and policy considerations. Five of the 
    remaining candidate consensus standards are new standards under 
    development that EPA plans to follow, review and consider adopting at a 
    later date. This rule requires standard EPA emission test methods known 
    to the industry and States. Approved alternative methods also may be 
    used with prior EPA approval.
    
    K. Executive Order 13045--Protection of Children From Environmental 
    Health Risks and Safety Risks
    
        Executive Order 13045 (62 FR 19885, April 23, 1997) applies to any 
    rule that (1) is determined to be ``economically significant'' as 
    defined under Executive Order 12866, and (2) concerns the environmental 
    health or safety risk that the EPA has reason to believe may have a 
    disproportionate effect on children. If the regulatory action meets 
    both criteria, the EPA must evaluate the environmental health or safety 
    effects of the planned rule on children, and explain why the planned 
    regulation is preferable to other potentially effective and reasonably 
    feasible alternatives considered by the EPA.
        The EPA interprets Executive Order 13045 as applying only to those 
    regulatory actions that are based on health or safety risks, such that 
    the analysis required under section 5-501 of the Order has the 
    potential to influence the regulation. This final rule is not subject 
    to Executive Order 13045 because it is not an economically significant 
    regulatory action as defined by Executive Order 12866, and it is based 
    on technology performance and not on health or safety risks.
    
    List of Subjects
    
    40 CFR Part 9
    
        Environmental protection, Recordkeeping and reporting requirements.
    
    40 CFR Part 63
    
        Environmental protection, Air pollution control, Hazardous 
    substances, Mineral wool production, Recordkeeping and reporting 
    requirements.
    
        Dated: May 13, 1999.
    Carol M. Browner,
    Administrator.
    
        For the reasons set out in the preamble, parts 9 and 63 of title 
    40, chapter I of the Code of Federal Regulations are amended as 
    follows:
    
    PART 9--OMB APPROVALS UNDER THE PAPERWORK REDUCTION ACT
    
        1. The authority citation for part 9 continues to read as follows:
    
        Authority: 7 U.S.C. 135 et seq., 136-136y; 15 U.S.C. 2001, 2003, 
    2005, 2006, 2601-2671; 21 U.S.C. 331j, 346a, 348; 31 U.S.C. 9701; 33 
    U.S.C. 1251 et seq., 1311, 1313d, 1314, 1318, 1321, 1326, 1330, 
    1342, 1344, 1345(d) and (e), 1361; E.O. 11735, 38 FR 21243, 3 CFR, 
    1971-1975 Comp. p. 973; 42 U.S.C. 241, 242b, 243, 246, 300f, 300g, 
    300g-1, 300g-2, 300g-3, 300g-4, 300g-5, 300g-6, 300j-1, 300j-2, 
    300j-3, 300j-4, 300j-9, 1857 et seq.,
    
    [[Page 29503]]
    
    6901-6992k, 7401-7671q, 7542, 9601-9657, 11023, 11048.
    
        2. Section 9.1 is amended by adding a new entry in numerical order 
    to the table under the indicated heading to read as follows:
    
    
    Sec. 9.1  OMB approvals under the Paperwork Reduction Act.
    
     * * * * *
    
    ------------------------------------------------------------------------
                    40 CFR citation                      OMB control No.
    ------------------------------------------------------------------------
     
                     *        *        *        *        *
       National Emission Standards for Hazardous Air Pollutants for Source
                                 Categories \3\
     
                      *        *        *        *        *
    63.1178--63.1194...............................                2060-0362
     
                      *        *        *        *        *
    ------------------------------------------------------------------------
    \3\ The ICRs referenced in this section of the table encompass the
      applicable general provisions contained in 40 CFR part 63, subpart A,
      which are not independent information collection requirements.
    
     * * * * *
    
    PART 63--NATIONAL EMISSION STANDARDS FOR HAZARDOUS AIR POLLUTANTS 
    FOR SOURCE CATEGORIES
    
        3. The authority citation for part 63 continues to read as follows:
    
        Authority: 42 U.S.C. 7401 et seq.
    
        4. Part 63 is amended by adding subpart DDD to read as follows:
    
    Subpart DDD--National Emission Standards for Hazardous Air Pollutants 
    for Mineral Wool Production
    
    Sec.
    63.1175  What is the purpose of this subpart?
    63.1176  Where can I find definitions of key words used in this 
    subpart?
    63.1177  Am I subject to this subpart?
    
    Standards
    
    63.1178  For cupolas, what standards must I meet?
    63.1179  For curing ovens, what standards must I meet?
    63.1180  When must I meet these standards?
    
    Compliance With Standards
    
    63.1181  How do I comply with the particulate matter standards for 
    existing, new, and reconstructed cupolas?
    63.1182  How do I comply with the carbon monoxide standards for new 
    and reconstructed cupolas?
    63.1183  How do I comply with the formaldehyde standards for 
    existing, new, and reconstructed curing ovens?
    
    Additional Monitoring Information
    
    63.1184  What do I need to know about the design specifications, 
    installation, and operation of a bag leak detection system?
    63.1185  How do I establish the average operating temperature of an 
    incinerator?
    63.1186  How may I change the compliance levels of monitored 
    parameters?
    63.1187  What do I need to know about operations, maintenance, and 
    monitoring plans?
    
    Performance Tests and Methods
    
    63.1188  What performance test requirements must I meet?
    63.1189  What test methods do I use?
    63.1190  How do I determine compliance?
    
    Notification, Recordkeeping, and Reporting
    
    63.1191  What notifications must I submit?
    63.1192  What recordkeeping requirements must I meet?
    63.1193  What reports must I submit?
    
    Other Requirements and Information
    
    63.1194  Which general provisions apply?
    63.1195  Who enforces this subpart?
    63.1196  What definitions should I be aware of?
    63.1197-63.1199  [Reserved]
    Table 1 to Subpart DDD of Part 63--Applicability of General 
    Provisions (40 CFR Part 63, Subpart A) to Subpart DDD of Part 63.
    Appendix A to Subpart DDD of Part 63--Free Formaldehyde Analysis of 
    Insulation Resins by the Hydroxylamine Hydrochloride Method.
    
    Subpart DDD--National Emission Standards for Hazardous Air 
    Pollutants for Mineral Wool Production
    
    
    Sec. 63.1175  What is the purpose of this subpart?
    
        This subpart establishes national emission standards for hazardous 
    air pollutants emitted from existing, new, and reconstructed cupolas 
    and curing ovens at facilities that produce mineral wool.
    
    
    Sec. 63.1176  Where can I find definitions of key words used in this 
    subpart?
    
        The definitions of key words used in this subpart are in the Clean 
    Air Act (Act), in Sec. 63.2 of the general provisions in subpart A of 
    this part, and in Sec. 63.1196 of this subpart.
    
    
    Sec. 63.1177  Am I subject to this subpart?
    
        You are subject to this subpart if you own or operate an existing, 
    new, or reconstructed mineral wool production facility that is located 
    at a plant site that is a major source of hazardous air pollutant (HAP) 
    emissions, meaning the plant emits or has the potential to emit any 
    single HAP at a rate of 9.07 megagrams (10 tons) or more per year or 
    any combination of HAPs at a rate of 22.68 megagrams (25 tons) or more 
    per year.
    
    Standards
    
    
    Sec. 63.1178  For cupolas, what standards must I meet?
    
        (a) You must control emissions from each cupola as follows:
        (1) Limit emissions of particulate matter (PM) from each existing, 
    new, or reconstructed cupola to 0.05 kilograms (kg) of PM per megagram 
    (MG) (0.10 pound [lb] of PM per ton) of melt or less.
        (2) Limit emissions of carbon monoxide (CO) from each new or 
    reconstructed cupola to either of the following:
        (i) 0.05 kg of CO per MG (0.10 lb of CO per ton) of melt or less.
        (ii) A reduction of uncontrolled CO emissions by at least 99 
    percent.
        (b) You must meet the following operating limits for each cupola:
        (1) Begin within one hour after the alarm on a bag leak detection 
    system sounds, and complete in a timely manner, corrective actions as 
    specified in your operations, maintenance, and monitoring plan required 
    by Sec. 63.1187 of this subpart.
        (2) When the alarm on a bag leak detection system sounds for more 
    than five percent of the total operating time in a six-month reporting 
    period, develop and implement a written quality improvement plan (QIP) 
    consistent with the compliance assurance monitoring requirements of 
    Sec. 64.8(b)-(d) of 40 CFR part 64.
        (3) Additionally, for each new or reconstructed cupola, maintain 
    the operating temperature of the incinerator so that the average 
    operating temperature for each three-hour block period never falls 
    below the average temperature established during the performance test.
    
    
    Sec. 63.1179  For curing ovens, what standards must I meet?
    
        (a) You must control emissions from each existing, new, or 
    reconstructed curing oven by limiting emissions of formaldehyde to 
    either of the following:
        (1) 0.03 kg of formaldehyde per MG (0.06 lb of formaldehyde per 
    ton) of melt or less.
        (2) A reduction of uncontrolled formaldehyde emissions by at least 
    80 percent.
        (b) You must meet the following operating limits for each curing 
    oven:
        (1) Maintain the free-formaldehyde content of each resin lot and 
    the formaldehyde content of each binder formulation at or below the 
    specification ranges of the resin and binder used during the 
    performance test.
        (2) Maintain the operating temperature of each incinerator so that
    
    [[Page 29504]]
    
    the average operating temperature for each three-hour block period 
    never falls below the average temperature established during the 
    performance test.
    
    
    Sec. 63.1180  When must I meet these standards?
    
        (a) Existing cupolas and curing ovens. You must install any control 
    devices and monitoring equipment necessary to meet the standards in 
    this subpart, complete performance testing, and demonstrate compliance 
    with all requirements of this subpart no later than the following:
        (1) June 2, 2002; or
        (2) June 3, 2003 if you apply for and receive a one-year extension 
    under section 112(i)(3)(B) of the Act.
        (b) New and reconstructed cupolas and curing ovens. You must 
    install any control devices or monitoring equipment necessary to meet 
    the standards in this subpart, complete performance testing, and 
    demonstrate compliance with all requirements of this subpart by the 
    dates in Sec. 63.7 of the general provisions in subpart A of this part.
        (c) You must comply with the standards in Secs. 63.1178 and 63.1179 
    of this subpart on and after the dates in paragraphs (a) and (b) of 
    this section.
        (d) You must comply with these standards at all times except during 
    periods of startup, shutdown, or malfunction.
    
    Compliance With Standards
    
    
    Sec. 63.1181  How do I comply with the particulate matter standards for 
    existing, new, and reconstructed cupolas?
    
        To comply with the PM standards, you must meet all of the 
    following:
        (a) Install, adjust, maintain, and continuously operate a bag leak 
    detection system for each fabric filter.
        (b) Do a performance test as specified in Sec. 63.1188 of this 
    subpart and show compliance with the PM emission limits while the bag 
    leak detection system is installed, operational, and properly adjusted.
        (c) Begin corrective actions specified in your operations, 
    maintenance, and monitoring plan required by Sec. 63.1187 of this 
    subpart within one hour after the alarm on a bag leak detection system 
    sounds. Complete the corrective actions in a timely manner.
        (d) Develop and implement a written QIP consistent with compliance 
    assurance monitoring requirements of 40 CFR 64.8(b) through (d) when 
    the alarm on a bag leak detection system sounds for more than five 
    percent of the total operating time in a six-month reporting period.
    
    
    Sec. 63.1182  How do I comply with the carbon monoxide standards for 
    new and reconstructed cupolas?
    
        To comply with the CO standards, you must meet all of the 
    following:
        (a) Install, calibrate, maintain, and operate a device that 
    continuously measures the operating temperature in the firebox of each 
    thermal incinerator.
        (b) Do a performance test as specified in Sec. 63.1188 of this 
    subpart and show compliance with the CO emission limits while the 
    device for measuring incinerator operating temperature is installed, 
    operational, and properly calibrated. Establish the average operating 
    temperature as specified in Sec. 63.1185(a) of this subpart.
        (c) Following the performance test, measure and record the average 
    operating temperature of the incinerator as specified in 
    Sec. 63.1185(b) of this subpart.
        (d) Maintain the operating temperature of the incinerator so that 
    the average operating temperature for each three-hour block period 
    never falls below the average temperature established during the 
    performance test.
        (e) Operate and maintain the incinerator as specified in your 
    operations, maintenance, and monitoring plan required by Sec. 63.1187 
    of this subpart.
    
    
    Sec. 63.1183  How do I comply with the formaldehyde standards for 
    existing, new, and reconstructed curing ovens?
    
        To comply with the formaldehyde standards, you must meet all of the 
    following:
        (a) Install, calibrate, maintain, and operate a device that 
    continuously measures the operating temperature in the firebox of each 
    thermal incinerator.
        (b) Do a performance test as specified in Sec. 63.1188 of this 
    subpart while manufacturing the product that requires a binder 
    formulation made with the resin containing the highest free-
    formaldehyde content specification range. Show compliance with the 
    formaldehyde emission limits while the device for measuring incinerator 
    operating temperature is installed, operational, and properly 
    calibrated. Establish the average operating temperature as specified in 
    Sec. 63.1185(a) of this subpart.
        (c) During the performance test that uses the binder formulation 
    made with the resin containing the highest free-formaldehyde content 
    specification range, record the free-formaldehyde content specification 
    range of the resin used, and the formulation of the binder used, 
    including the formaldehyde content and binder specification.
        (d) Following the performance test, monitor and record the free-
    formaldehyde content of each resin lot and the formulation of each 
    batch of binder used, including the formaldehyde content.
        (e) Maintain the free-formaldehyde content of each resin lot and 
    the formaldehyde content of each binder formulation at or below the 
    specification ranges established during the performance test.
        (f) Following the performance test, measure and record the average 
    operating temperature of the incinerator as specified in 
    Sec. 63.1185(b) of this subpart.
        (g) Maintain the operating temperature of the incinerator so that 
    the average operating temperature for each three-hour block period 
    never falls below the average temperature established during the 
    performance test.
        (h) Operate and maintain the incinerator as specified in your 
    operations, maintenance, and monitoring plan required by Sec. 63.1187 
    of this subpart.
        (i) With prior approval from the Administrator, you may do short-
    term experimental production runs using resin where the free-
    formaldehyde content, or binder formulations where the formaldehyde 
    content, is higher than the specification ranges of the resin and 
    binder used during previous performance tests, or using experimental 
    pollution prevention process modifications without first doing 
    additional performance tests. Notification of intent to perform a 
    short-term experimental production run must include the following 
    information:
        (1) The purpose of the experimental run.
        (2) The affected production process.
        (3) How the resin free-formaldehyde content or binder formulation 
    will deviate from previously approved levels or what the experimental 
    pollution prevention process modifications are.
        (4) The duration of the experimental run.
        (5) The date and time of the experimental run.
        (6) A description of any emissions testing to be done during the 
    experimental run.
    
    Additional Monitoring Information
    
    
    Sec. 63.1184   What do I need to know about the design specifications, 
    installation, and operation of a bag leak detection system?
    
        A bag leak detection system must meet the following requirements:
        (a) The bag leak detection system must be certified by the 
    manufacturer to be capable of detecting PM emissions at concentrations 
    of 10 milligrams per actual cubic meter (0.0044 grains per actual cubic 
    foot) or less.
    
    [[Page 29505]]
    
        (b) The sensor on the bag leak detection system must provide output 
    of relative PM emissions.
        (c) The bag leak detection system must have an alarm that will 
    sound automatically when it detects an increase in relative PM 
    emissions greater than a preset level.
        (d) The alarm must be located in an area where appropriate plant 
    personnel will be able to hear it.
        (e) For a positive-pressure fabric filter, each compartment or cell 
    must have a bag leak detector. For a negative-pressure or induced-air 
    fabric filter, the bag leak detector must be installed downstream of 
    the fabric filter. If multiple bag leak detectors are required (for 
    either type of fabric filter), detectors may share the system 
    instrumentation and alarm.
        (f) Each triboelectric bag leak detection system must be installed, 
    operated, adjusted, and maintained so that it follows EPA's ``Fabric 
    Filter Bag Leak Detection Guidance'' (EPA-454/R-98-015, September 
    1997). Other bag leak detection systems must be installed, operated, 
    adjusted, and maintained so that they follow the manufacturer's written 
    specifications and recommendations.
        (g) At a minimum, initial adjustment of the system must consist of 
    establishing the baseline output in both of the following ways:
        (1) Adjust the range and the averaging period of the device.
        (2) Establish the alarm set points and the alarm delay time.
        (h) After initial adjustment, the range, averaging period, alarm 
    set points, or alarm delay time may not be adjusted except as specified 
    in the operations, maintenance, and monitoring plan required by 
    Sec. 63.1187 of this subpart. In no event may the range be increased by 
    more than 100 percent or decreased by more than 50 percent over a 365 
    day period unless a responsible official as defined in Sec. 63.2 of the 
    general provisions in subpart A of this part certifies in writing to 
    the Administrator that the fabric filter has been inspected and found 
    to be in good operating condition.
    
    
    Sec. 63.1185  How do I establish the average operating temperature of 
    an incinerator?
    
        (a) During the performance test, you must establish the average 
    operating temperature of an incinerator as follows:
        (1) Continuously measure the operating temperature of the 
    incinerator.
        (2) Determine and record the average temperatures in consecutive 
    15-minute blocks.
        (3) Determine and record the arithmetic average of the recorded 
    average temperatures measured in consecutive 15-minute blocks for each 
    of the one-hour performance test runs.
        (4) Determine and record the arithmetic average of the three one-
    hour average temperatures during the performance test runs. The average 
    of the three one-hour performance test runs establishes the temperature 
    level to use to monitor compliance.
        (b) To comply with the requirements for maintaining the operating 
    temperature of an incinerator after the performance test, you must 
    measure and record the average operating temperature of the incinerator 
    as required by Secs. 63.1182 and 63.1183 of this subpart. This average 
    operating temperature of the incinerator is based on the arithmetic 
    average of the one-hour average temperatures for each consecutive 
    three-hour period and is determined in the same manner described in 
    paragraphs (a)(1) through (a)(4) of this section.
    
    
    Sec. 63.1186  How may I change the compliance levels of monitored 
    parameters?
    
        You may change control device and process operating parameter 
    levels established during performance tests and used to monitor 
    compliance if you do the following:
        (a) You must notify the Administrator of your desire to expand the 
    range of a control device or process operating parameter level.
        (b) Upon approval from the Administrator, you must conduct 
    additional performance tests at the proposed new control device or 
    process operating parameter levels. Before operating at these levels, 
    the performance test results must verify that, at the new levels, you 
    comply with the emission limits in Secs. 63.1178 and 63.1179 of this 
    subpart.
    
    
    Sec. 63.1187  What do I need to know about operations, maintenance, and 
    monitoring plans?
    
        (a) An operations, maintenance, and monitoring plan must be 
    submitted to the Administrator for review and approval as part of your 
    application for the title V permit.
        (b) The operations, maintenance, and monitoring plan must include 
    the following:
        (1) Process and control device parameters you will monitor to 
    determine compliance, along with established operating levels or ranges 
    for each process or control device.
        (2) A monitoring schedule.
        (3) Procedures for properly operating and maintaining control 
    devices used to meet the standards in Secs. 63.1178 and 63.1179 of this 
    subpart. These procedures must include an inspection of each 
    incinerator at least once per year. At a minimum, you must do the 
    following as part of an incinerator inspection:
        (i) Inspect all burners, pilot assemblies, and pilot sensing 
    devices for proper operation. Clean pilot sensor if necessary.
        (ii) Ensure proper adjustment of combustion air, and adjust if 
    necessary.
        (iii) Inspect, when possible, all internal structures (such as 
    baffles) to ensure structural integrity per the design specifications.
        (iv) Inspect dampers, fans, and blowers for proper operation.
        (v) Inspect motors for proper operation.
        (vi) Inspect, when possible, combustion chamber refractory lining. 
    Clean, and repair or replace lining if necessary.
        (vii) Inspect incinerator shell for proper sealing, corrosion, and/
    or hot spots.
        (viii) For the burn cycle that follows the inspection, document 
    that the incinerator is operating properly and make any necessary 
    adjustments.
        (ix) Generally observe whether the equipment is maintained in good 
    operating condition.
        (x) Complete all necessary repairs as soon as practicable.
        (4) Procedures for keeping records to document compliance.
        (5) Corrective actions you will take if process or control device 
    parameters vary from the levels established during performance testing. 
    For bag leak detection system alarms, example corrective actions that 
    may be included in the operations, maintenance, and monitoring plan 
    include:
        (i) Inspecting the fabric filter for air leaks, torn or broken bags 
    or filter media, or any other condition that may cause an increase in 
    emissions.
        (ii) Sealing off defective bags or filter media.
        (iii) Replacing defective bags or filter media, or otherwise 
    repairing the control device.
        (iv) Sealing off a defective fabric filter compartment.
        (v) Cleaning the bag leak detection system probe, or otherwise 
    repairing the bag leak detection system.
        (vi) Shutting down the process producing the particulate emissions.
    
    Performance Tests and Methods
    
    
    Sec. 63.1188  What performance test requirements must I meet?
    
        You must meet the following performance test requirements:
    
    [[Page 29506]]
    
        (a) All monitoring systems and equipment must be installed, 
    operational, and properly calibrated before the performance tests.
        (b) Do a performance test, consisting of three test runs, for each 
    cupola and curing oven subject to this subpart at the maximum 
    production rate to demonstrate compliance with each of the applicable 
    emission limits in Secs. 63.1178 and 63.1179 of this subpart.
        (c) Measure emissions of PM from each existing cupola.
        (d) Measure emissions of PM and CO from each new or reconstructed 
    cupola.
        (e) Measure emissions of formaldehyde from each existing, new or 
    reconstructed curing oven.
        (f) Measure emissions at the outlet of the control device if 
    complying with a numerical emission limit for PM, CO, or formaldehyde, 
    or at the inlet and outlet of the control device if complying with a 
    percent reduction emission limit for CO or formaldehyde.
        (g) To determine the average melt rate, measure and record the 
    amount of raw materials, excluding coke, charged into and melted in 
    each cupola during each performance test run. Determine and record the 
    average hourly melt rate for each performance test run. Determine and 
    record the arithmetic average of the average hourly melt rates 
    associated with the three performance test runs. The average hourly 
    melt rate of the three performance test runs is used to determine 
    compliance with the applicable emission limits.
        (h) Compute and record the average emissions of the three 
    performance test runs and use the equations in Sec. 63.1190 of this 
    subpart to determine compliance with the applicable emission limits.
        (i) Comply with control device and process operating parameter 
    monitoring requirements for performance testing as specified in this 
    subpart.
    
    
    Sec. 63.1189  What test methods do I use?
    
        You must use the following test methods to determine compliance 
    with the applicable emission limits:
        (a) Method 1 in appendix A to part 60 of this chapter for the 
    selection of the sampling port locations and number of sampling ports.
        (b) Method 2 in appendix A to part 60 of this chapter for stack gas 
    velocity and volumetric flow rate.
        (c) Method 3 or 3A in appendix A to part 60 of this chapter for 
    oxygen and carbon dioxide for diluent measurements needed to correct 
    the concentration measurements to a standard basis.
        (d) Method 4 in appendix A to part 60 of this chapter for moisture 
    content of the stack gas.
        (e) Method 5 in appendix A to part 60 of this chapter for the 
    concentration of PM. Each PM test run must consist of a minimum run 
    time of three hours and a minimum sample volume of 3.75 dscm (135 
    dscf).
        (f) Method 10 in appendix A to part 60 of this chapter for the 
    concentration of CO, using the continuous sampling option described in 
    section 7.1.1 of the method. Each CO test run must consist of a minimum 
    run time of one hour.
        (g) Method 318 in appendix A to this part for the concentration of 
    formaldehyde or CO.
        (h) Method to determine the free-formaldehyde content of each resin 
    lot in appendix A of this subpart.
    
    
    Sec. 63.1190  How do I determine compliance?
    
        (a) Using the results of the performance tests, you must use the 
    following equation to determine compliance with the PM emission limit:
    [GRAPHIC] [TIFF OMITTED] TR01JN99.015
    
    where:
    E = Emission rate of PM, kg/Mg (lb/ton) of melt.
    C = Concentration of PM, g/dscm (gr/dscf).
    Q = Volumetric flow rate of exhaust gases, dscm/hr (dscf/hr).
    K 51 = Conversion factor, 1 kg/1,000 g (1 lb/7,000 gr).
    P = Average melt rate, Mg/hr (ton/hr).
    
        (b) Using the results of the performance tests, you must use the 
    following equation to determine compliance with the CO and formaldehyde 
    numerical emission limits:
    [GRAPHIC] [TIFF OMITTED] TR01JN99.016
    
    where:
    E = Emission rate of measured pollutant, kg/Mg (lb/ton) of melt.
    C = Measured volume fraction of pollutant, ppm.
    MW = Molecular weight of measured pollutant, g/g-mole:
    CO = 28.01, Formaldehyde = 30.03.
    Q = Volumetric flow rate of exhaust gases, dscm/hr (dscf/hr).
    K1 = Conversion factor, 1 kg/1,000 g (1 lb/453.6 g).
    K2 = Conversion factor, 1,000 L/m3 (28.3 L/
    ft3).
    K3 = Conversion factor, 24.45 L/g-mole.
    P = Average melt rate, Mg/hr (ton/hr).
    
        (c) Using the results of the performance tests, you must use the 
    following equation to determine compliance with the CO and formaldehyde 
    percent reduction performance standards:
    [GRAPHIC] [TIFF OMITTED] TR01JN99.017
    
    where:
    %R = Percent reduction, or collection efficiency of the control device.
    Li = Inlet loading of pollutant, kg/Mg (lb/ton).
    Lo = Outlet loading of pollutant, kg/Mg (lb/ton).
    
    Notification, Recordkeeping, and Reporting
    
    
    Sec. 63.1191  What notifications must I submit?
    
        You must submit written notifications to the Administrator as 
    required by Sec. 63.9(b)-(h) of the general provisions in subpart A of 
    this part. These notifications include, but are not limited to, the 
    following:
        (a) Notification that the following types of sources are subject to 
    the standard:
        (1) An area source that increases its emissions so that it becomes 
    a major source.
        (2) A source that has an initial startup before the effective date 
    of the standard.
        (3) A new or reconstructed source that has an initial startup after 
    the effective date of the standard and doesn't require an application 
    for approval of construction or reconstruction under Sec. 63.5(d) of 
    the general provisions in subpart A of this part.
        (b) Notification of intention to construct a new major source or 
    reconstruct a major source where the initial startup of the new or 
    reconstructed source occurs after the effective date of the standard 
    and an application for approval of construction or reconstruction under 
    Sec. 63.5(d) of the general provisions in subpart A of this part is 
    required.
        (c) Notification of special compliance obligations for a new source 
    that is subject to special compliance requirements in Sec. 63.6(b)(3) 
    and (4) of the general provisions in subpart A of this part.
        (d) Notification of a performance test at least 60 calendar days 
    before the performance test is scheduled to begin.
        (e) Notification of compliance status.
    
    
    Sec. 63.1192  What recordkeeping requirements must I meet?
    
        You must meet the following recordkeeping requirements:
        (a) Maintain files of all information required by Sec. 63.10(b) of 
    the general provisions in subpart A of this part, including all 
    notifications and reports.
        (b) Maintain records of the following information also:
        (1) Cupola production (melt) rate (Mg/hr (tons/hr) of melt).
    
    [[Page 29507]]
    
        (2) All bag leak detection system alarms. Include the date and time 
    of the alarm, when corrective actions were initiated, the cause of the 
    alarm, an explanation of the corrective actions taken, and when the 
    cause of the alarm was corrected.
        (3) The free-formaldehyde content of each resin lot and the binder 
    formulation, including formaldehyde content, of each binder batch used 
    in the manufacture of bonded products.
        (4) Incinerator operating temperature and results of incinerator 
    inspections. For all periods when the average temperature in any three-
    hour block period fell below the average temperature established during 
    the performance test, and all periods when the inspection identified 
    incinerator components in need of repair or maintenance, include the 
    date and time of the problem, when corrective actions were initiated, 
    the cause of the problem, an explanation of the corrective actions 
    taken, and when the cause of the problem was corrected.
        (c) Retain each record for at least five years following the date 
    of each occurrence, measurement, corrective action, maintenance, 
    record, or report. The most recent two years of records must be 
    retained at the facility. The remaining three years of records may be 
    retained off site.
        (d) Retain records on microfilm, on a computer, on computer disks, 
    on magnetic tape disks, or on microfiche.
        (e) Report the required information on paper or on a labeled 
    computer disk using commonly available and compatible computer 
    software.
    
    
    Sec. 63.1193  What reports must I submit?
    
        You must prepare and submit reports to the Administrator as 
    required by this subpart and Sec. 63.10 of the general provisions in 
    subpart A of this part. These reports include, but are not limited to, 
    the following:
        (a) A performance test report, as required by Sec. 63.10(d)(2) of 
    the general provisions in subpart A of this part, that documents the 
    process and control equipment operating parameters during the test 
    period, the test methods and procedures, the analytical procedures, all 
    calculations, and the results of the performance tests.
        (b) A startup, shutdown, and malfunction plan, as described in 
    Sec. 63.6(e)(3) of the general provisions in subpart A of this part, 
    that contains specific procedures for operating and maintaining the 
    source during periods of startup, shutdown, and malfunction and a 
    program of corrective action for malfunctioning process and control 
    systems used to comply with the emission standards. In addition to the 
    information required by Sec. 63.6(e)(3), your plan must include the 
    following:
        (1) Procedures to determine and record what caused the malfunction 
    and when it began and ended.
        (2) Corrective actions you will take if a process or control device 
    malfunctions, including procedures for recording the actions taken to 
    correct the malfunction or minimize emissions.
        (3) An inspection and maintenance schedule for each process and 
    control device that is consistent with the manufacturer's instructions 
    and recommendations for routine and long-term maintenance.
        (c) A report of each event as required by Sec. 63.10(b) of the 
    general provisions in subpart A of this part, including a report if an 
    action taken during a startup, shutdown, or malfunction is inconsistent 
    with the procedures in the plan as described in Sec. 63.6(e)(3) of the 
    general provisions in subpart A of this part.
        (d) An operations, maintenance, and monitoring plan as specified in 
    Sec. 63.1187 of this subpart.
        (e) A semiannual report as required by Sec. 63.10(e)(3) of the 
    general provisions in subpart A of this part if measured emissions 
    exceed the applicable standard or a monitored parameter varies from the 
    level established during performance testing. The report must contain 
    the information specified in Sec. 63.10(c) of the general provisions, 
    as well as the relevant records required by Sec. 63.1192(b) of this 
    subpart.
        (f) A semiannual report stating that no excess emissions or 
    deviations of monitored parameters occurred during the reporting period 
    as required by Sec. 63.10(e)(3)(v) of the general provisions in subpart 
    A of this part if no deviations have occurred.
    
    Other Requirements and Information
    
    
    Sec. 63.1194  Which general provisions apply?
    
        The general provisions in subpart A of this part define 
    requirements applicable to all owners and operators affected by NESHAP 
    in part 63. See Table 1 of this subpart for general provisions that 
    apply (or don't apply) to you as an owner or operator subject to the 
    requirements of this subpart.
    
    
    Sec. 63.1195  Who enforces this subpart?
    
        If the Administrator has delegated authority to your State, then 
    the State, along with the EPA, enforces this regulation. If the 
    Administrator has not delegated authority to your State, then the EPA 
    enforces this regulation.
    
    
    Sec. 63.1196  What definitions should I be aware of?
    
        Terms used in this subpart are defined in the Act, in Sec. 63.2 of 
    the general provisions in subpart A of this part, and in this section 
    as follows:
        Bag leak detection system means a monitoring device for a fabric 
    filter that identifies an increase in particulate matter emissions 
    resulting from a broken filter bag or other malfunction and sounds an 
    alarm.
        Bonded product means mineral wool to which a hazardous air 
    pollutant-based binder (containing such hazardous air pollutants as 
    phenol or formaldehyde) has been applied.
        CO means, for the purposes of this subpart, emissions of carbon 
    monoxide that serve as a surrogate for emissions of carbonyl sulfide, a 
    compound included on the list of hazardous air pollutants in section 
    112 of the Act.
        Cupola means a large, water-cooled metal vessel to which is charged 
    a mixture of fuel, rock and/or slag, and additives. As the fuel is 
    burned, the charged mixture is heated to a molten state for later 
    processing to form mineral wool.
        Curing oven means a chamber in which heat is used to thermoset a 
    binder on the mineral wool fiber used to make bonded products.
        Fabric filter means an air pollution control device used to capture 
    particulate matter by filtering gas streams through fabric bags. It 
    also is known as a baghouse.
        Formaldehyde means, for the purposes of this subpart, emissions of 
    formaldehyde that, in addition to being a HAP itself, serve as a 
    surrogate for organic compounds included on the list of hazardous air 
    pollutants in section 112 of the Act, including but not limited to 
    phenol.
        Hazardous air pollutant means any air pollutant listed in or 
    pursuant to section 112(b) of the Act.
        I means the owner or operator of a mineral wool production 
    facility.
        Incinerator means an enclosed air pollution control device that 
    uses controlled flame combustion to convert combustible materials to 
    noncombustible gases.
        Melt means raw materials, excluding coke, that are charged into the 
    cupola, heated to a molten state, and discharged to the fiber forming 
    and collection process.
        Melt rate means the mass of molten material discharged from a 
    single cupola over a specified time period.
        Mineral wool means a fibrous glassy substance made from natural 
    rock (such as basalt), blast furnace slag or other slag, or a mixture 
    of rock and slag. It
    
    [[Page 29508]]
    
    may be used as a thermal or acoustical insulation material or in the 
    making of other products to provide structural strength, sound 
    absorbency, fire resistance, or other required properties.
        New source means any affected source the construction or 
    reconstruction of which is commenced after May 8, 1997.
        PM means, for the purposes of this subpart, emissions of 
    particulate matter that serve as a surrogate for metals (in particulate 
    or volatile form) on the list of hazardous air pollutants in section 
    112 of the Act, including but not limited to: antimony, arsenic, 
    beryllium, cadmium, chromium, lead, manganese, nickel, and selenium.
        You means the owner or operator of a mineral wool production 
    facility.
    
      Table 1 to Subpart DDD of Part 63--Applicability of General Provisions (40 CFR Part 63, Subpart A) to Subpart
                                                     DDD of Part 63
    ----------------------------------------------------------------------------------------------------------------
        General provisions  citation            Requirement         Applies to subpart DDD?        Explanation
    ----------------------------------------------------------------------------------------------------------------
    63.1(a)(1)-(a)(4)...................  General Applicability..  Yes.....................
    63.1(a)(5)..........................                           No......................  [Reserved].
    63.1(a)(6)-(a)(8)...................                           Yes.....................
    63.1(a)(9)..........................                           No......................  [Reserved].
    63.1(a)(10)-(a)(14).................                           Yes.....................
    63.1(b).............................  Initial Applicability    Yes.....................
                                           Determination.
    63.1(c)(1)..........................  Applicability After      Yes.....................
                                           Standard Established.
    63.1(c)(2)..........................                           Yes.....................  Some plants may be area
                                                                                              sources.
    63.1(c)(3)..........................                           No......................  [Reserved].
    63.1(c)(4)-(c)(5)...................                           Yes.....................
    63.1(d).............................                           No......................  [Reserved].
    63.1(e).............................  Applicability of Permit  Yes.....................
                                           Program.
    63.2................................  Definitions............  Yes.....................  Additional definitions
                                                                                              in Sec.  63.1196.
    63.3................................  Units and Abbreviations  Yes.....................
    63.4(a)(1)-(a)(3)...................  Prohibited Activities..  Yes.....................
    63.4(a)(4)..........................                           No......................  [Reserved].
    63.4(a)(5)..........................                           Yes.....................
    63.4(b)-(c).........................  Circumvention/           Yes.....................
                                           Severability.
    63.5(a).............................  Construction/            Yes.....................
                                           Reconstruction
                                           Applicability.
    63.5(b)(1)..........................  Existing, New,           Yes.....................
                                           Reconstructed Sources
                                           Requirements.
    63.5(b)(2)..........................                           No......................  [Reserved].
    63.5(b)(3)-(b)(6)...................                           Yes.....................
    63.5(c).............................                           No......................  [Reserved].
    63.5(d).............................  Application for          Yes.....................
                                           Approval of
                                           Construction/
                                           Reconstruction.
    63.5(e).............................  Approval of              Yes.....................
                                           Construction/
                                           Reconstruction.
    63.5(f).............................  Approval of              Yes.....................
                                           Construction/
                                           Reconstruction Based
                                           on State Review.
    63.6(a).............................  Compliance with          Yes.....................
                                           Standards and
                                           Maintenance
                                           Applicability.
    63.6(b)(1)-(b)(5)...................  New and Reconstructed    Yes.....................
                                           Sources Dates.
    63.6(b)(6)..........................                           No......................  [Reserved].
    63.6(b)(7)..........................                           Yes.....................
    63.6(c)(1)..........................  Existing Sources Dates.  Yes.....................  Sec.  63.1180 specifies
                                                                                              compliance dates.
    63.6(c)(2)..........................  .......................  Yes.....................
    63.6(c)(3)-(c)(4)...................  .......................  No......................  [Reserved].
    63.6(c)(5)..........................  .......................  Yes.....................
    63.6(d).............................  .......................  No......................  [Reserved].
    63.6(e)(1)-(e)(2)...................  Operation & Maintenance  Yes.....................  Sec.  63.1187 specifies
                                           Requirements.                                      additional
                                                                                              requirements.
    63.6(e)(3)..........................  Startup, Shutdown, and   Yes.....................
                                           Malfunction Plan.
    63.6(f).............................  Compliance with          Yes.....................
                                           Emission Standards.
    63.6(g).............................  Alternative Standard...  Yes.....................
    63.6(h).............................  Compliance with Opacity/ No......................  Subpart DDD does not
                                           VE Standards.                                      include VE/opacity
                                                                                              standards.
    63.6(i)(1)-(i)(14)..................  Extension of Compliance  Yes.....................  Sec.  63.1180 specifies
                                                                                              date.
    63.6(i)(15).........................  .......................  No......................  [Reserved].
    63.6(i)(16).........................  .......................  Yes.....................
    63.6(j).............................  Exemption from           Yes.....................
                                           Compliance.
    63.7(a).............................  Performance Test         Yes.....................
                                           Requirements
                                           Applicability.
    63.7(b).............................  Notification...........  Yes.....................
    63.7(c).............................  Quality Assurance/Test   Yes.....................
                                           Plan.
    63.7(d).............................  Testing Facilities.....  Yes.....................
    63.7(e).............................  Conduct of Tests.......  Yes.....................  Sec.  63.1188 specifies
                                                                                              additional
                                                                                              requirements.
    63.7(f).............................  Alternative Test Method  Yes.....................
    63.7(g).............................  Data Analysis..........  Yes.....................
    63.7(h).............................  Waiver of Tests........  Yes.....................
    
    [[Page 29509]]
    
     
    63.8(a)(1)..........................  Monitoring Requirements  Yes.....................
                                           Applicability.
    63.8(a)(2)..........................  .......................  No......................  Subpart DDD does not
                                                                                              require CMS
                                                                                              performance
                                                                                              specifications.
    63.8(a)(3)..........................  .......................  No......................  [Reserved].
    63.8(a)(4)..........................  .......................  Yes.....................
    63.8(b).............................  Conduct of Monitoring..  Yes.....................
    63.8(c)(1)-(c)(3)...................  CMS Operation/           Yes.....................
                                           Maintenance.
    63.8(c)(4)-(c)(8)...................  .......................  No......................  Subpart DDD does not
                                                                                              require COMS or CMS
                                                                                              performance
                                                                                              specifications.
    63.8(d).............................  Quality Control........  No......................  Subpart DDD does not
                                                                                              require a CMS quality
                                                                                              control program.
    63.8(e).............................  CMS Performance          No......................  Subpart DDD does not
                                           Evaluation.                                        require CMS
                                                                                              performance
                                                                                              evaluations.
    63.8(f)(1)-(f)(5)...................  Alternative Monitoring   Yes.....................
                                           Method.
    63.8(f)(6)..........................  Alternative to RATA      No......................  Subpart DDD does not
                                           Test.                                              require CEMS.
    63.8(g)(1)..........................  Data Reduction.........  Yes.....................
    63.8(g)(2)..........................  .......................  No......................  Subpart DDD does not
                                                                                              require COMS or CEMS.
    63.8(g)(3)-(g)(5)...................  .......................  Yes.....................
    63.9(a).............................  Notification             Yes.....................
                                           Requirements
                                           Applicability.
    63.9(b).............................  Initial Notifications..  Yes.....................
    63.9(c).............................  Request for Compliance   Yes.....................
                                           Extension.
    63.9(d).............................  New Source Notification  Yes.....................
                                           for Special Compliance
                                           Requirements.
    63.9(e).............................  Notification of          Yes.....................
                                           Performance Test.
    63.9(f).............................  Notification of VE/      No......................  Subpart DDD does not
                                           Opacity Test.                                      include VE/opacity
                                                                                              standards.
    63.9(g).............................  Additional CMS           No......................  Subpart DDD does not
                                           Notifications.                                     require CMS
                                                                                              performance
                                                                                              evaluation, COMS, or
                                                                                              CEMS.
    63.9(h)(1)-(h)(3)...................  Notification of          Yes.....................
                                           Compliance Status.
    63.9(h)(4)..........................  .......................  No......................  [Reserved].
    63.9(h)(5)-(h)(6)...................  .......................  Yes.....................
    63.9(i).............................  Adjustment of Deadlines  Yes.....................
    63.9(j).............................  Change in Previous       Yes.....................
                                           Information.
    63.10(a)............................  Recordkeeping/Reporting- Yes.....................
                                           Applicability.
    63.10(b)............................  General Recordkeeping    Yes.....................  Sec.  63.1192 includes
                                           Requirements.                                      additional
                                                                                              requirements.
    63.10(c)(1).........................  Additional CMS           Yes.....................
                                           Recordkeeping.
    63.10(c)(2)-(c)(4)..................  .......................  No......................  [Reserved].
    63.10(c)(5).........................  .......................  Yes.....................
    63.10(c)(6).........................  .......................  No......................  Subpart DDD does not
                                                                                              require CMS
                                                                                              performance
                                                                                              specifications.
    63.10(c)(7)-(c)(8)..................  .......................  Yes.....................
    63.10(c)(9).........................  .......................  No......................  [Reserved].
    63.10(c) (10)-(c)(13)...............  .......................  Yes.....................
    63.10(c)(14)........................  .......................  No......................  Subpart DDD does not
                                                                                              require a CMS quality
                                                                                              control program.
    63.10(c)(15)........................  .......................  Yes.....................
    63.10(d)(1).........................  General Reporting        Yes.....................  Additional requirements
                                           Requirements.                                      in Sec.  63.1193.
    63.10(d)(2).........................  Performance Test         Yes.....................
                                           Results.
    63.10(d)(3).........................  Opacity or VE            No......................  Subpart DDD does not
                                           Observations.                                      include VE/opacity
                                                                                              standards.
    63.10(d)(4)-(d)(5)..................  Progress Reports/        Yes.....................
                                           Startup, Shutdown, and
                                           Malfunction Reports.
    63.10(e)(1)-(e)(2)..................  Additional CMS Reports.  No......................  Subpart DDD does not
                                                                                              require CEMS or CMS
                                                                                              performance
                                                                                              evaluations.
    63.10(e)(3).........................  Excess Emissions/CMS     Yes.....................
                                           Performance Reports.
    63.10(e)(4).........................  COMS Data Reports......  No......................  Subpart DDD does not
                                                                                              require COMS.
    63.10(f)............................  Recordkeeping/Reporting  Yes.....................
                                           Waiver.
    63.11(a)............................  Control Device           Yes.....................
                                           Requirements
                                           Applicability.
    63.11(b)............................  Flares.................  No......................  Flares not applicable.
    63.12...............................  State Authority and      Yes.....................
                                           Delegations.
    63.13...............................  Addresses..............  Yes.....................
    63.14...............................  Incorporation by         Yes.....................
                                           Reference.
    63.15...............................  Information              Yes.....................
                                           Availability/
                                           Confidentiality.
    ----------------------------------------------------------------------------------------------------------------
    
    
    [[Page 29510]]
    
    Appendix A to Subpart DDD of Part 63--Free Formaldehyde Analysis of 
    Insulation Resins by the Hydroxylamine Hydrochloride Method
    
    1. Scope
    
        The method in this appendix was specifically developed for 
    water-soluble phenolic resins that have a relatively high free-
    formaldehyde (FF) content such as insulation resins. It may also be 
    suitable for other phenolic resins, especially those with a high FF 
    content.
    
    2. Principle
    
        2.1  a. The basis for this method is the titration of the 
    hydrochloric acid that is liberated when hydroxylamine hydrochloride 
    reacts with formaldehyde to form formaldoxine:
    
    HCHO + NH2OH:HCl  CH2:NOH + H2O + HCl
    
        b. Free formaldehyde in phenolic resins is present as monomeric 
    formaldehyde, hemiformals, polyoxymethylene hemiformals, and 
    polyoxymethylene glycols. Monomeric formaldehyde and hemiformals 
    react rapidly with hydroxylamine hydrochloride, but the polymeric 
    forms of formaldehyde must hydrolyze to the monomeric state before 
    they can react. The greater the concentration of free formaldehyde 
    in a resin, the more of that formaldehyde will be in the polymeric 
    form. The hydrolysis of these polymers is catalyzed by hydrogen 
    ions.
        2.2  The resin sample being analyzed must contain enough free 
    formaldehyde so that the initial reaction with hydroxylamine 
    hydrochloride will produce sufficient hydrogen ions to catalyze the 
    depolymerization of the polymeric formaldehyde within the time 
    limits of the test method. The sample should contain approximately 
    0.3 grams (g) free formaldehyde to ensure complete reaction within 5 
    minutes.
    
    3. Apparatus
    
        3.1  Balance, readable to 0.01 g or better.
        3.2  pH meter, standardized to pH 4.0 with pH 4.0 buffer and pH 
    7 with pH 7.0 buffer.
        3.3  50-mL burette for 1.0 N sodium hydroxide.
        3.4  Magnetic stirrer and stir bars.
        3.5  250-mL beaker.
        3.6  50-mL graduated cylinder.
        3.7  100-mL graduated cylinder.
        3.8  Timer.
    
    4. Reagents
    
        4.1  Standardized 1.0 N sodium hydroxide solution.
        4.2  Hydroxylamine hydrochloride solution, 100 grams per liter, 
    pH adjusted to 4.00.
        4.3  Hydrochloric acid solution, 1.0 N and 0.1 N.
        4.4  Sodium hydroxide solution, 0.1 N.
        4.5  50/50 v/v mixture of distilled water and methyl alcohol.
    
    5. Procedure
    
        5.1  Determine the sample size as follows:
        a. If the expected FF is greater than 2 percent, go to Part A in 
    5.1.c to determine sample size.
        b. If the expected FF is less than 2 percent, go to Part B in 
    5.1.d to determine sample size.
        c. Part A: Expected FF 2 percent.
    
    Grams resin = 60/expected percent FF
    
        I. The following table shows example levels:
    
    ------------------------------------------------------------------------
                                                                    Sample
                 Expected percent free formaldehyde              size, grams
    ------------------------------------------------------------------------
    2..........................................................         30.0
    5..........................................................         12.0
    8..........................................................          7.5
    10.........................................................          6.0
    12.........................................................          5.0
    15.........................................................          4.0
    ------------------------------------------------------------------------
    
        ii. It is very important to the accuracy of the results that the 
    sample size be chosen correctly. If the milliliters of titrant are 
    less than 15 mL or greater than 30 mL, reestimate the needed sample 
    size and repeat the tests.
        d. Part B: Expected FF < 2="" percent="" grams="" resin="30/expected" percent="" ff="" i.="" the="" following="" table="" shows="" example="" levels:="" ------------------------------------------------------------------------="" sample="" expected="" percent="" free="" formaldehyde="" size,="" grams="" ------------------------------------------------------------------------="" 2..........................................................="" 15="" 1..........................................................="" 30="" 0.5........................................................="" 60="" ------------------------------------------------------------------------="" ii.="" if="" the="" milliliters="" of="" titrant="" are="" less="" than="" 5="" ml="" or="" greater="" than="" 30="" ml,="" reestimate="" the="" needed="" sample="" size="" and="" repeat="" the="" tests.="" 5.2="" weigh="" the="" resin="" sample="" to="" the="" nearest="" 0.01="" grams="" into="" a="" 250-ml="" beaker.="" record="" sample="" weight.="" 5.3="" add="" 100="" ml="" of="" the="" methanol/water="" mixture="" and="" stir="" on="" a="" magnetic="" stirrer.="" confirm="" that="" the="" resin="" has="" dissolved.="" 5.4="" adjust="" the="" resin/solvent="" solution="" to="" ph="" 4.0,="" using="" the="" prestandardized="" ph="" meter,="" 1.0="" n="" hydrochloric="" acid,="" 0.1="" n="" hydrochloric="" acid,="" and="" 0.1="" n="" sodium="" hydroxide.="" 5.5="" add="" 50="" ml="" of="" the="" hydroxylamine="" hydrochloride="" solution,="" measured="" with="" a="" graduated="" cylinder.="" start="" the="" timer.="" 5.6="" stir="" for="" 5="" minutes.="" titrate="" to="" ph="" 4.0="" with="" standardized="" 1.0="" n="" sodium="" hydroxide.="" record="" the="" milliliters="" of="" titrant="" and="" the="" normality.="" 6.="" calculations="" [graphic]="" [tiff="" omitted]="" tr01jn99.018="" 7.="" method="" precision="" and="" accuracy="" test="" values="" should="" conform="" to="" the="" following="" statistical="" precision:="" variance="0.005" standard="" deviation="0.07" 95%="" confidence="" interval,="" for="" a="" single="" determination="0.2" 8.="" author="" this="" method="" was="" prepared="" by="" k.k.="" tutin="" and="" m.l.="" foster,="" tacoma="" r&d="" laboratory,="" georgia-pacific="" resins,="" inc.="" (principle="" written="" by="" r.="" r.="" conner.)="" 9.="" references="" 9.1="" gpam="" 2221.2.="" 9.2="" pr&c="" tm="" 2.035.="" 9.3="" project="" report,="" comparison="" of="" free="" formaldehyde="" procedures,="" january="" 1990,="" k.="" tutin.="" [fr="" doc.="" 99-12585="" filed="" 5-28-99;="" 8:45="" am]="" billing="" code="" 6560-50-p="">

Document Information

Published:
06/01/1999
Department:
Environmental Protection Agency
Entry Type:
Rule
Action:
Final rule.
Document Number:
99-12585
Dates:
June 1, 1999. See the SUPPLEMENTARY INFORMATION section concerning judicial review.
Pages:
29490-29510 (21 pages)
Docket Numbers:
FRL-6345-4
RINs:
2060-AE08: NESHAP: Mineral Wool Production Industry
RIN Links:
https://www.federalregister.gov/regulations/2060-AE08/neshap-mineral-wool-production-industry
PDF File:
99-12585.pdf
CFR: (158)
40 CFR 63.1(a)(9)
40 CFR 63.1185(a)
40 CFR 63.1(a)(5)
40 CFR 63.5(a)
40 CFR 63.4(a)(4)
More ...